CN107779320A - A kind of green peel of walnut clean skin product and preparation method thereof - Google Patents

A kind of green peel of walnut clean skin product and preparation method thereof Download PDF

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Publication number
CN107779320A
CN107779320A CN201710959243.1A CN201710959243A CN107779320A CN 107779320 A CN107779320 A CN 107779320A CN 201710959243 A CN201710959243 A CN 201710959243A CN 107779320 A CN107779320 A CN 107779320A
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China
Prior art keywords
walnut
green peel
powder
parts
preparation
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CN201710959243.1A
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Chinese (zh)
Inventor
周建华
尹梦晗
周晨
王文佳
丁秋月
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Shandong Normal University
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Shandong Normal University
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Priority to CN201710959243.1A priority Critical patent/CN107779320A/en
Publication of CN107779320A publication Critical patent/CN107779320A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/005Synthetic soaps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/007Preparations for dry skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • C11D2111/12

Abstract

The invention discloses a kind of green peel of walnut clean skin product and preparation method thereof, the green peel of walnut clean skin product that the present invention is prepared is without chemical compositions such as antiseptic, preservatives, natural environmental-protective, without harmful components, properties of product are gentle, it is non-foaming, there is the multi-efficiencies such as significant cleaning, itch-stopping bactericidal, anti-inflammatory, whitening, anti-oxidant, heat-clearing, moisturizing.Green peel of walnut clean skin product is raw materials used to be included in parts by weight:90~110 parts of soap base, 8~12 parts of green peel of walnut powder, 3~7 parts of needles of pinus massoniana powder, 3~7 parts of licorice powder, 0.5~1.5 part of Chinese mugwort ash, 0.4~0.6 part of luffa;Wherein, the soap base is the mixture of olive oil and rilanit special, and the ratio of weight and number of the specific olive oil and rilanit special is 7~8:2~3.

Description

A kind of green peel of walnut clean skin product and preparation method thereof
Technical field
The present invention relates to wash shield cleaning supplies technical field, and in particular to a kind of green peel of walnut clean skin product and its preparation Method.
Background technology
In recent years, as China's major part urban environment pollutes by the haze of getting worse, the skin of people becomes to get over Come more fragile, frequently occur the problems such as itch, acne, skin sensitivity, annoying people.Therefore need of the people to washing product Ask in terms of not only resting on cleaning, be more desirable to it and have go acne, sterilization, anti-inflammatory, antipruritic, anti-oxidant, moist, moisturizing etc. Multiple functions, can more fully integrate improves various skin problems, lifts quality of life.
Perfumed soap is the general name of fatty acid metal salts, can be dissolved in water, has washing decontamination, wherein soap is by various Grease is generated with aqueous slkali by saponification.Perfumed soap wide variety at present, to clean based on clean effect, and in order to be lifted The functions such as reparation of the perfumed soap to skin, maintenance, often add related functionality raw material in perfumed soap, including chemically additive, plant The additive in thing source etc..It is such as the sterilizing function of lifting perfumed soap, adds phenolic compound, such perfumed soap Chang Chenghong thereto Color, the stimulation to skin is stronger, for for skin sensitivity and having the people of minor cut or wound and does not apply to.Therefore pure natural plant is used Feature Traditional Chinese medicine perfumed soap that the Chinese herbal medicine in thing source is prepared, because it had both had the cleaning force of conventional toilet soaps, while have again The health-care efficacy of medicine composition, turn into practical in daily life and life washing product with Chinese characteristics.
Chinese patent CN10270323A discloses a kind of degerming soap of natural plant, mainly with Radix Isatidis, ginger, Radix scutellariae, cordate houttuynia, dandelion, honeysuckle, Chinese prickly ash are main waste concentrate and a certain proportion of cleaning, decontamination composition Mixing, is made with decontamination, antiviral, bactericidal effect health care fancy soap by modernization process.But the perfumed soap skin care energy Power is low, and traditional Chinese medicine ingredients flavour of a drug are strong, makes us being difficult to receive, while Chinese medicine can destroy or lose part when concentrate is made Active ingredient, influence its function.
Chinese patent CN103666890B discloses a kind of Traditional Chinese medicinal liquid soap, by laruyl alcohol sodium sulfovinate 40-60 parts, Lanolin 6-10 parts, dioecious balanophora herb 2-4 parts, cat hair grass 2-4 parts composition, the Traditional Chinese medicinal liquid soap have good foaming and antibacterial Effect.But the patent soap is liquid form, and do not have the effect of physics is antipruritic.
The content of the invention
For above-mentioned the deficiencies in the prior art, inventor is through long-term technology and practical exploration, there is provided a kind of green peel of walnut Clean skin product and preparation method thereof.The green peel of walnut clean skin product that the present invention is prepared is without chemistry such as antiseptic, preservatives Composition, natural environmental-protective, no harmful components, properties of product are gentle, have significant cleaning, sterilization, anti-inflammatory, it is antipruritic, anti-oxidant, The multi-efficiencies such as moist, moisturizing.
Specifically, the present invention relates to following technical scheme:
The first aspect of the invention, there is provided a kind of green peel of walnut clean skin product, its is raw materials used to wrap in parts by weight Include:90~110 parts of soap base, 8~12 parts of green peel of walnut powder, 3~7 parts of needles of pinus massoniana powder, 3~7 parts of licorice powder, Chinese mugwort ash 0.5~ 1.5 parts, 0.4~0.6 part of luffa;
Wherein, soap base is the basic material for making soap, and the present invention is especially from vegetative grease with sodium hydroxide through saponification institute Soap base must be used as, it is further preferred that the vegetative grease is the mixture of olive oil and rilanit special, the olive The ratio of weight and number of oil and rilanit special is 7~8:2~3;
The preparation method of the green peel of walnut powder is:The selection fresh green peel of walnut of this season is dried, and 180 purposes are crossed after crushing Sieve;
The needles of pinus massoniana powder, preparation method thereof is:The fresh Pineneedles of Pinus Massoniana Lamb of selection this season is dried after cleaning, after crushing, mistake 80 mesh sieves;
The preparation method of the licorice powder is:Selection has good quality, and without the radix glycyrrhizae to go mouldy, is directly crushed after cutting small pieces, mistake 140 mesh sieves;
The grey preparation method of the Chinese mugwort is:Selection has good quality, and without the wormwood to go mouldy, burns into ash, i.e. Chinese mugwort ash, crosses 140 mesh Sieve;
The luffa preparation method is:The sponge gourd that selection full maturity is dried, luffa obtained by peeling remove seed, according to Specification is cut into segment, is put into after soaking in mould, standby;
Preferably, the green peel of walnut clean skin product, its is raw materials used to be in parts by weight:100 parts of soap base, walnut are blue or green 10 parts of skin powder, 5 parts of needles of pinus massoniana powder, 5 parts of licorice powder, 1 part of Chinese mugwort ash, 0.5 part of luffa;
Wherein, the soap base is the mixture and sodium hydroxide of olive oil and rilanit special through saponification gained, the olive Olive oil and rilanit special ratio of weight and number are 7:2.8;
The second aspect of the invention, discloses the preparation method of the green peel of walnut clean skin product, and specific method is:
(1) pretreatment of raw material:
The selection fresh green peel of walnut of this season is dried, and the sieve of 180 mesh is crossed after crushing;
Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh sieves are crossed after crushing;
Selection has good quality, and without the radix glycyrrhizae to go mouldy, is directly crushed after cutting small pieces, crosses 140 mesh sieves;
Selection has good quality, and without the wormwood to go mouldy, burns into ash, i.e. Chinese mugwort ash, crosses 140 mesh sieves;
The sponge gourd that selection full maturity is dried, luffa obtained by peeling remove seed, is cut into segment according to specification, is put after soaking Enter in mould, it is standby;
(2) preparation of mixed powder:Green peel of walnut powder, needles of pinus massoniana powder, licorice powder, Chinese mugwort ash are fully mixed in proportion;
(3) grease is handled:
Rilanit special is placed in into 45 DEG C of heating water baths makes its thawing be liquid, by olive oil and rilanit special 7~8: 2~3 (be preferably 7:2.8) part by weight mixing, is placed in 50~60 DEG C of (be preferably 50 DEG C) heating water baths, keep olive oil, Rilanit special mixes oils temperature stabilization at 50 DEG C;
(4) according to a conventional method according to olive oil, rilanit special saponification value to olive oil, rilanit special miscella Middle addition sodium oxide molybdena carries out saponification;
Preferably, it is 50 DEG C to control saponification temperature, and the saponification time is 1.5~2.5h (being most preferably 2h);
(5) mould, cooled and solidified are entered:
In the lotion after the mixed powder in proportion preparing step (2) before entering mould adds saponification, quick stirring Poured into after uniformly in the mould equipped with the luffa soaked, cooled and solidified processing.
Preferably, in the step (5), quick mixing time is 1~2min (be most preferably 1.5min), rotating speed 80~ 120rpm (be most preferably 100rpm), the cooled and solidified processing time be:Below 10 DEG C of temperature, 2~3d is stood.
Preferably, the preparation method of the green peel of walnut clean skin product also includes step (6) demoulding, packaging, specifically, Demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, is slightly repaired, and assists profile Adjust consistent.The soap product of taking-up is put into preprepared packaging bag, sealing preserves.
The third aspect of the invention, disclose application of the above-mentioned preparation method in green peel of walnut clean skin product is prepared.
The fourth aspect of the invention, the application method of the green peel of walnut clean skin product is disclosed, specifically, using It is preceding with warm water moistening skin, after green peel of walnut clean skin product completely immersion, the gently rubbing on itch skin, reach physics With the dual antipruritic purpose of chemistry, then massaged and cleaned with palm part, rinsed well with clear water, finally with quality soft texture Dry towel by dry.
Preferably, palm massage scavenging period determines according to skin oil dryness, and the Oily time is 1min, dryness skin Skin is 0.5min.
Green peel of walnut clean skin product of the present invention is as follows from the specific effect of plant material:
Green peel of walnut is also known as " pericarpium juglandis ", is the thick green pericarp of a thickness outside walnut.It is its bitter, puckery, it is mild-natured, return Liver, spleen, stomach, it is good Chinese medicine.Contain abundant volatile oil, aliphatic acid, mineral matter, polysaccharide, quinone in green peel of walnut The materials such as class, flavonoids, have inhibiting bacteria and diminishing inflammation, antitumor, hypotensive, it is anti-oxidant, ease pain, relieving asthma and other effects.Wherein contain Hydro carbons, ketone, alcohols etc. volatilize oil substances, based on sesquiterpenoids, have relieving asthma, be antibacterial, antitumor action;All kinds of fat Acid content is enriched, the aliphatic acid as necessary to containing leukotrienes, linoleic acid human body, has softening blood vessel, preventing and treating hypertension and the heart The special efficacies such as popular name for;Quinones substance has obvious inhibitory action to a variety of transplanted tumors in vivo, Cytotoxicity in vitro cell Act on stronger, and toxicity is relatively low;Flavonoid substances have antitumor, resisting cardiovascular disease, anti-oxidant, scavenging activated oxygen With the extensive curative effect such as anti-aging, anti-inflammatory and antalgic;In addition containing abundant natural pigment.
Containing abundant amino acid in Pineneedles of Pinus Massoniana Lamb, a variety of fat-soluble and water soluble vitamin, more than 40 kinds of macroelement and Various trace elements and crude fibre, have anti-aging, it is anti-oxidant, relieving asthma, protect angiocarpy, inhibiting bacteria and diminishing inflammation, antitumor, Adjust-blood lipid, The functions such as hypotensive.Its lignanoid contained, shikimic acid have the function that antiphlogistic antibacterial, can alleviate cutaneous pruritus.
Radix glycyrrhizae is a kind of important help Chinese herbal medicine, often enters various Chinese herbal medicine prescriptions for adjutant.Its property sweet taste, the thoughts of returning home, Lung, spleen, stomach, there is the effect of invigorating the lung and benefiting vital QI, clearing heat and detoxicating, antiasthmatic-antitussive, pain of alleviation, coordinating the drug actions of a prescription, while have anti- The pharmacological action such as bacterium, anti-inflammatory, antitumor, anti-AIDS.Glycyrrhizic acid composition therein can effectively treat allergic dermatitis, Such as itch, dermatocyst and eczema;Radix glycyrrhizae flavane can suppress platelet activating factor acetyl transferase activity in vitro, tool There is anti-inflammatory activity, natural anti-inflammatory drug can be used as;Contained licoflavone constituents, glabridin, isoliquiritigenin etc. have Anti-inflammatory power.In addition, licorice has whitening function, chromocor compound composition therein has sun-proof efficiency.
Wormwood can be ended obtained by the moxa that ash dries with all herbal medicine, had anti-inflammation and sterilization, hemostasis and pain-relieving, drying Wound, anti-acne, beautifying whitening, treatment wet sore, tinea pedis and other effects are protected, end grey or natural effective eliminating smell agent, drying in addition Agent and fertilizer.
Luffa also known as day trailing plants muscle or sponge gourd net, it is the vascular bundle of the ripening fruits of sponge gourd or Guangdong sponge gourd.It is sweet, it is mild-natured, Return lung, liver, stomach, have it is clearing heat and detoxicating, it is living through dredging collateral, inducing diuresis to remove edema, hemostasis and other effects, there is medicine-food two-purpose effect.Luffa It is flexible, it is not easily broken, there is netted gap again, smoothing effect can be played, and have good massage effect, energy to skin Antipruritic anti-acne.
Beneficial effects of the present invention:
(1) green peel of walnut clean skin product of the invention is a kind of with green peel of walnut, needles of pinus massoniana, radix glycyrrhizae, Chinese mugwort ash and sponge gourd Network is new, the practical product of natural material, and material adapted is reasonable, using luffa as natural support body, retains luffa Natural shape, the effect of assigning the unique physics of product and dual antipruritic chemistry, while can give full play to and utilize luffa Massage, cleaning and whitening function;
(2) green peel of walnut clean skin product raw materials of the invention have a variety of compositions mutually cooperateed with and effect.Core The volatilization oil substances that peach rascal contains have anti-inflammation, oxidation resistant beneficial effect;The lignanoid contained in needles of pinus massoniana, Shikimic acid has the function that antiphlogistic antibacterial, can alleviate cutaneous pruritus, and have antioxidant effect;Glycyrrhizic acid in radix glycyrrhizae and Radix glycyrrhizae flavane is natural anti-inflammatory drug, and has antibacterial action;Wormwood has the effect of anti-inflammation and sterilization.Four kinds of materials of the above are equal The effect of with anti-inflammation, complement each other, fully and more effectively enhance the antipruritic effect of anti-inflammation, luffa Friction can play the effect of physics is antipruritic.Therefore, the present invention has the dual itching-relieving action of physics and chemistry simultaneously.
(3) green peel of walnut of the present invention, Pineneedles of Pinus Massoniana Lamb, radix glycyrrhizae contain Flavonoid substances.Flavonoid substances With the extensive curative effect such as antitumor, resisting cardiovascular disease, anti-oxidant, scavenging activated oxygen and anti-aging, anti-inflammatory and antalgic. Chromocor compound in other licorice also has whitening sun protection function, and green peel of walnut and Pineneedles of Pinus Massoniana Lamb can be anti-ageing Always, it is anti-oxidant.Chromocor compound composition, Chinese mugwort ash, luffa in licorice all have white-skinned face function, with reference to luffa Physical massage, product is enhanced cleaning, whitening and antipruritic effect.
(4) raw material of the present invention also have a variety of collaboration facilitations pharmacologically.Green peel of walnut, horse hair Loosely pin, radix glycyrrhizae are respectively provided with antitumor, antiasthmatic effect, and wormwood also has antiasthmatic-antitussive effect;Green peel of walnut, Pineneedles of Pinus Massoniana Lamb All there is the effect of hypotensive, Adjust-blood lipid, protection cardiovascular and cerebrovascular disease;Green peel of walnut and radix glycyrrhizae have analgesic efficacy;Chinese mugwort ash and Luffa can stop blooding;Pine needle and radix glycyrrhizae can improve immunity;Radix glycyrrhizae and luffa can be clearing heat and detoxicating.These associations pharmacologically Clinical and medicine is can be applied to facilitation, strengthens drug effect;Meanwhile further to play drug effect, the present invention uses direct powder Broken technology is by each raw material pulverization process, based on each material composition because quality, density differ, therefore using the sieve of different meshes Son carries out sieving processing, so as to which each raw material maximum effect be brought into play;, will in preparation process meanwhile inventor has found Each plant material mixed powder, which is added in the lotion after saponification, carries out under certain rotating speed stir process for a period of time, by The raw material powder mill pressure of different-grain diameter so that the soap product crystalline phase being finally prepared wholly or largely is changed into β crystalline substances Phase, therefore the soap product solubility prepared by the present invention is higher, and it is fine and smooth gentle to wash sense.
(5) the manufacture special olive oil of raw material of the present invention, contained abundant monounsaturated fatty acids in olive oil With vitamin E, K, A, D etc. and phenols polyphenoils, it can smooth away wrinkles, prevent skin aging, there is good skin care work( Effect;Olive oil is rich in the squalene and essential fatty acid splendid with skin affinity, absorbs rapidly, can effectively keep skin Skin is elastic and moist, moistens and maintains skin, increases the gloss and elasticity of skin;In olive oil and material containing flavonoids etc. its He plays synergy by composition, has efficient antiinflammation.
(6) present invention solves the problems, such as environmental pollution and the wasting of resources caused by the superfluous accumulation of green peel of walnut, by core Peach rascal is turned waste into wealth, and environmental protection, adds farmers' income, improves the utilization rate of walnut byproduct, there is provided it is abundant and The raw material being readily available, while provide a kind of green peel of walnut clean skin product and preparation method thereof for people.Each equal nothing of medicinal material Toxic side effect, it is safe to use, there is light medicinal herbs delicate fragrance taste.
Brief description of the drawings
Fig. 1 is the green peel of walnut clean skin finished product figure that the present invention is prepared.
Embodiment
It is noted that described further below is all exemplary, it is intended to provides further instruction to the application.Unless Otherwise indicated, all technologies used herein and scientific terminology have and the application person of an ordinary skill in the technical field The identical meanings being generally understood that.
It should be noted that term used herein above is merely to describe embodiment, and be not intended to restricted root According to the illustrative embodiments of the application.As used herein, unless the context clearly indicates otherwise, otherwise odd number shape Formula is also intended to include plural form, additionally, it should be understood that, when in this manual use term "comprising" and/or During " comprising ", it indicates existing characteristics, step, operation, device, component and/or combinations thereof.
In the exemplary embodiment of the present invention, there is provided a kind of green peel of walnut clean skin product, its is raw materials used by weight Number includes:90~110 parts of soap base, 8~12 parts of green peel of walnut powder, 3~7 parts of needles of pinus massoniana powder, 3~7 parts of licorice powder, Chinese mugwort ash 0.5~1.5 part, 0.4~0.6 part of luffa;
Wherein, soap base is the basic material for making soap, and the present invention especially selects vegetative grease as soap base, further excellent Choosing, the vegetative grease is the mixture of olive oil and rilanit special, the weight of the olive oil and rilanit special Portion rate is 7~8:2~3;
The preparation method of the green peel of walnut powder is:The selection fresh green peel of walnut of this season is dried, and 180 purposes are crossed after crushing Sieve;
The needles of pinus massoniana powder, preparation method thereof is:Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh are crossed after crushing Sieve;
The preparation method of the licorice powder is:Selection has good quality, and without the radix glycyrrhizae to go mouldy, is directly crushed after cutting small pieces, mistake 140 mesh sieves;
The grey preparation method of the Chinese mugwort is:Selection has good quality, and without the wormwood to go mouldy, burns into ash, i.e. Chinese mugwort ash, crosses 140 mesh Sieve;
The luffa preparation method is:The sponge gourd that selection full maturity is dried, luffa obtained by peeling remove seed, according to Specification is cut into segment, is put into after soaking in mould, standby;
In the another exemplary embodiment of the present invention, the green peel of walnut clean skin product, its is raw materials used in parts by weight For:100 parts of soap base, 10 parts of green peel of walnut powder, 5 parts of needles of pinus massoniana powder, 5 parts of licorice powder, 1 part of Chinese mugwort ash, 0.5 part of luffa;
Wherein, the soap base gets for the mixture of olive oil and rilanit special with sodium hydroxide saponification, the olive Oil and rilanit special ratio of weight and number are 7:2.8;
In another embodiment of the invention, there is provided the preparation method of the green peel of walnut clean skin product, specific method For:
(1) pretreatment of raw material:
The selection fresh green peel of walnut of this season is dried, and the sieve of 180 mesh is crossed after crushing;
Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh sieves are crossed after crushing;
Selection has good quality, and without the radix glycyrrhizae to go mouldy, is directly crushed after cutting small pieces, crosses 140 mesh sieves;
Selection has good quality, and without the wormwood to go mouldy, burns into ash, i.e. Chinese mugwort ash, crosses 140 mesh sieves;
The sponge gourd that selection full maturity is dried, luffa obtained by peeling remove seed, is cut into segment according to specification, is put after soaking Enter in mould, it is standby.
(2) preparation of mixed powder:By green peel of walnut powder, needles of pinus massoniana powder, licorice powder, Chinese mugwort ash ratio in parts by weight Fully mix.
(3) grease is handled:
Rilanit special is placed in into 45 DEG C of heating water baths makes its thawing be liquid, by olive oil and rilanit special 7~8: 2~3 (be preferably 7:2.8) part by weight mixing, is placed in 50~60 DEG C of (be preferably 50 DEG C) heating water baths, keep olive oil, Rilanit special mixes oils temperature stabilization at 50 DEG C.
(4) according to a conventional method according to olive oil, rilanit special saponification value to olive oil, rilanit special miscella Middle addition sodium hydroxide carries out saponification.
Preferably, it is 50 DEG C to control saponification temperature, and the saponification time is 1.5~2.5h (being most preferably 2h);
(5) mould, cooled and solidified are entered:
In the lotion after the mixed powder in proportion preparing step (2) before entering mould adds saponification, quick stirring Poured into after uniformly in the mould equipped with the luffa soaked, cooled and solidified processing.
In another embodiment of the invention, in the step (5), quick mixing time is that 1~2min (is most preferably 1.5min), 80~120rpm of rotating speed (being most preferably 100rpm), the cooled and solidified processing time are:Below 10 DEG C of temperature, Stand 2~3d.
In another embodiment of the invention, the preparation method of the green peel of walnut clean skin product also includes step (6) and taken off Mould, packaging:Specifically, demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, slightly Add finishing, make profile harmonious.The soap product of taking-up is put into preprepared packaging bag, sealing preserves.
In another embodiment of the invention, there is provided above-mentioned preparation method is in green peel of walnut clean skin product is prepared Using.
In another embodiment of the invention, there is provided the application method of the green peel of walnut clean skin product, specifically, Using preceding with warm water moistening skin, after green peel of walnut clean skin product is soaked, the gently rubbing on itch skin, reach physics With the dual antipruritic purpose of chemistry, then massaged and cleaned with palm part, rinsed well with clear water, finally with quality soft texture Dry towel by dry.
Wherein, palm massage scavenging period determines according to skin oil dryness, and the Oily time is 1min, Dry For 0.5min.
The present invention is further elaborated with experimental example with reference to embodiments.
Embodiment 1
A kind of green peel of walnut clean skin product and preparation method thereof:
(1) pretreatment of raw material
The selection fresh rascal of this season is dried, and the sieve of 180 mesh is crossed after crushing;Rascal grinds increase its specific surface area, favorably In the dissolving and leaching of active ingredient, curative effect and bioavilability are improved;Also allowing for each composition can be well mixed.
Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh sieves are crossed after crushing, it is standby;
The radix glycyrrhizae that selection is had good quality, nothing is gone mouldy, directly crushes after cutting small pieces, crosses 140 mesh sieves, standby;
Selection wormwood is dried, the ash burnt till, i.e. Chinese mugwort ash, crosses 140 mesh sieves, standby;
Select full maturity sponge gourd, dry peeling remove seed obtained by luffa, be cut into the thick segments of 3cm, diameter 6cm, completely It is put into after soaking in silica gel mould, it is standby.
The parts by weight proportioning of required raw material is olive oil:Rilanit special:Green peel of walnut powder:Needles of pinus massoniana powder:Radix glycyrrhizae Powder:Chinese mugwort ash=70:28:10:5:5:1.
(2) preparation of mixed powder
Ratio of weight and number is green peel of walnut powder:Needles of pinus massoniana powder:Licorice powder:Chinese mugwort ash=10:5:5:1, fully mix, obtain Mixed powder.
(3) processing of grease
Rilanit special makes its thawing be liquid in 45 DEG C of heating water baths.By olive oil:Rilanit special=70:28 Ratio mixes, and is placed in water-bath in 50 DEG C of water-baths, keeps olive oil, rilanit special mixing oils stable at 50 DEG C.
(4) saponification
It is about 0.134mg/g according to olive oil saponification value, rilanit special saponification value is about 0.129mg/g, is claimed in proportion Sodium hydrate solid is measured, is dissolved in a certain proportion of deionized water, reaches saturation, treats that sodium hydroxide solution temperature cools down During to room temperature and clarification, saturation sodium hydroxide solution is slowly fallen in miscella by several times, control temperature is at 50 DEG C, side bevelling Stirring, saponification 2h.By 1h stirring, saponification, temperature is maintained at 50 DEG C, and saponification occurs for mixture, and oils is in gradually lemon Lemon yellow paste, draw 8-shaped on surface and do not disappear, bottom does not have oils remaining until saponification is complete.
(5) mould, cooled and solidified are entered
In the lotion after mixed powder addition saponification is terminated in proportion before entering mould, quickly stirred with 100rpm rotating speeds Poured into after mixing 1.5min in the silica type mould equipped with the luffa soaked, be put in cooled and solidified at low-temperature aeration drying, temperature Less than 10 DEG C, setting time 2h, place 2d.
(6) it is stripped, packs
Demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, is slightly repaired, Make profile harmonious.The soap of taking-up is put into preprepared packaging bag, sealing preserves.
Embodiment 2
A kind of green peel of walnut clean skin product and preparation method thereof:
(1) pretreatment of raw material
The selection fresh rascal of this season is dried, and the sieve of 180 mesh is crossed after crushing;Rascal grinds increase its specific surface area, favorably In the dissolving and leaching of active ingredient, curative effect and bioavilability are improved;Also allowing for each composition can be well mixed.
Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh sieves are crossed after crushing, it is standby;
The radix glycyrrhizae that selection is had good quality, nothing is gone mouldy, directly crushes after cutting small pieces, crosses 140 mesh sieves, standby;
Selection wormwood is dried, the ash burnt till, i.e. Chinese mugwort ash, crosses 140 mesh sieves, standby;
Select full maturity sponge gourd, dry peeling remove seed obtained by luffa, be cut into the thick segments of 3cm, diameter 6cm, completely It is put into after soaking in silica gel mould, it is standby.
The parts by weight proportioning of required raw material is olive oil:Rilanit special:Green peel of walnut powder:Needles of pinus massoniana powder:Radix glycyrrhizae Powder:Chinese mugwort ash=80:20:12:4:5:0.5.
(2) preparation of mixed powder
Ratio of weight and number is green peel of walnut powder:Needles of pinus massoniana powder:Licorice powder:Chinese mugwort ash=12:4:5:0.5, fully mix, Obtain mixed powder.
(3) processing of grease
Rilanit special makes its thawing be liquid in 45 DEG C of heating water baths.By olive oil:Rilanit special=4:1 ratio Example mixing, is placed in water-bath in 50 DEG C of water-baths, keeps olive oil, rilanit special mixing oils stable at 50 DEG C.
(4) saponification
It is about 0.134mg/g according to olive oil saponification value, rilanit special saponification value is about 0.129mg/g, is claimed in proportion Sodium hydrate solid is measured, is dissolved in a certain proportion of deionized water, reaches saturation, treats that sodium hydroxide solution temperature cools down During to room temperature and clarification, saturation sodium hydroxide solution is slowly fallen in miscella by several times, control temperature is at 50 DEG C, side bevelling Stirring, saponification 2h.By 1h stirring, saponification, temperature is maintained at 50 DEG C, and saponification occurs for mixture, and oils is in gradually lemon Lemon yellow paste, draw 8-shaped on surface and do not disappear, bottom does not have oils remaining until saponification is complete.
(5) mould, cooled and solidified are entered
In the lotion after mixed powder addition saponification is terminated in proportion before entering mould, quickly stirred with 80rpm rotating speeds Poured into after 2min in the silica type mould equipped with luffa, be put in cooled and solidified at low-temperature aeration drying, below 10 DEG C of temperature, Setting time 2h, place 2d.
(6) it is stripped, packs
Demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, is slightly repaired, Make profile harmonious.The soap of taking-up is put into preprepared packaging bag, sealing preserves.
Embodiment 3
A kind of green peel of walnut clean skin product and preparation method thereof:
(1) pretreatment of raw material
The selection fresh rascal of this season is dried, and the sieve of 180 mesh is crossed after crushing;Rascal grinds increase its specific surface area, favorably In the dissolving and leaching of active ingredient, curative effect and bioavilability are improved;Also allowing for each composition can be well mixed.
Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh sieves are crossed after crushing, it is standby;
The radix glycyrrhizae that selection is had good quality, nothing is gone mouldy, directly crushes after cutting small pieces, crosses 140 mesh sieves, standby;
Selection wormwood is dried, the ash burnt till, i.e. Chinese mugwort ash, crosses 140 mesh sieves, standby;
Select full maturity sponge gourd, dry peeling remove seed obtained by luffa, be cut into the thick segments of 3cm, diameter 6cm, completely It is put into after soaking in silica gel mould, it is standby.
The parts by weight proportioning of required raw material is olive oil:Rilanit special:Green peel of walnut powder:Needles of pinus massoniana powder:Radix glycyrrhizae Powder:Chinese mugwort ash=80:30:8:7:5:0.5.
(2) preparation of mixed powder
Ratio of weight and number is green peel of walnut powder:Needles of pinus massoniana powder:Licorice powder:Chinese mugwort ash=8:7:5:0.5, fully mix, obtain Mixed powder.
(3) processing of grease
Rilanit special makes its thawing be liquid in 45 DEG C of heating water baths.By olive oil:Rilanit special=8:3 ratio Example mixing, is placed in water-bath in 50 DEG C of water-baths, keeps olive oil, rilanit special mixing oils stable at 50 DEG C.
(4) saponification
It is about 0.134mg/g according to olive oil saponification value, rilanit special saponification value is about 0.129mg/g, is claimed in proportion Sodium hydrate solid is measured, is dissolved in a certain proportion of deionized water, reaches saturation, treats that sodium hydroxide solution temperature cools down During to room temperature and clarification, saturation sodium hydroxide solution is slowly fallen in miscella by several times, control temperature is at 50 DEG C, side bevelling Stirring, saponification 2h.By 1h stirring, saponification, temperature is maintained at 50 DEG C, and saponification occurs for mixture, and oils is in gradually lemon Lemon yellow paste, draw 8-shaped on surface and do not disappear, bottom does not have oils remaining until saponification is complete.
(5) mould, cooled and solidified are entered
In the lotion after mixed powder addition saponification is terminated in proportion before entering mould, quickly stirred with 120rpm rotating speeds Poured into after mixing 1min in the silica type mould equipped with luffa, be put in cooled and solidified at low-temperature aeration drying, 10 DEG C of temperature with Under, setting time 2h, place 2d.
(6) it is stripped, packs
Demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, is slightly repaired, Make profile harmonious.The soap of taking-up is put into preprepared packaging bag, sealing preserves.
Experimental example 1
A kind of green peel of walnut clean skin product and preparation method thereof:
(1) pretreatment of raw material
The selection fresh rascal of this season is dried, and the sieve of 180 mesh is crossed after crushing;Rascal grinds increase its specific surface area, favorably In the dissolving and leaching of active ingredient, curative effect and bioavilability are improved;Also allowing for each composition can be well mixed.
Select the fresh Pineneedles of Pinus Massoniana Lamb of this season to clean drying, 80 mesh sieves are crossed after crushing, it is standby;
The radix glycyrrhizae that selection is had good quality, nothing is gone mouldy, directly crushes after cutting small pieces, crosses 140 mesh sieves, standby;
Selection wormwood is dried, the ash burnt till, i.e. Chinese mugwort ash, crosses 140 mesh sieves, standby;
Select full maturity sponge gourd, dry peeling remove seed obtained by luffa, be cut into the thick segments of 3cm, diameter 6cm, completely It is put into after soaking in silica gel mould, it is standby.
The parts by weight proportioning of required raw material is olive oil:Rilanit special:Green peel of walnut powder:Needles of pinus massoniana powder:Radix glycyrrhizae Powder:Chinese mugwort ash=70:30:9:6:5:1.
(2) preparation of mixed powder
Ratio of weight and number is green peel of walnut powder:Needles of pinus massoniana powder:Licorice powder:Chinese mugwort ash=9:6:5:1, fully mix, obtain mixed Close powder.
(3) processing of grease
Rilanit special makes its thawing be liquid in 45 DEG C of heating water baths.By olive oil:Rilanit special=7:3 ratio Example mixing, is placed in water-bath in 50 DEG C of water-baths, keeps olive oil, rilanit special mixing oils stable at 50 DEG C.
(4) saponification
It is about 0.134mg/g according to olive oil saponification value, rilanit special saponification value is about 0.129mg/g, is claimed in proportion Sodium hydrate solid is measured, is dissolved in a certain proportion of deionized water, reaches saturation, treats that sodium hydroxide solution temperature cools down During to room temperature and clarification, saturation sodium hydroxide solution is slowly fallen in miscella by several times, control temperature is at 50 DEG C, side bevelling Stirring, saponification 2h.By 1h stirring, saponification, temperature is maintained at 50 DEG C, and saponification occurs for mixture, and oils is in gradually lemon Lemon yellow paste, draw 8-shaped on surface and do not disappear, bottom does not have oils remaining until saponification is complete.
(5) mould, cooled and solidified are entered
In the lotion after mixed powder addition saponification is terminated in proportion before entering mould, stirred with 50rpm rotating speeds Poured into after 1.5min in the silica type mould equipped with luffa, be put in cooled and solidified at low-temperature aeration drying, 10 DEG C of temperature with Under, setting time 2h, place 2d.
(6) it is stripped, packs
Demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, is slightly repaired, Make profile harmonious.The soap of taking-up is put into preprepared packaging bag, sealing preserves.Green peel of walnut clean skin product Effect experiment
1st, zoopery
Green peel of walnut clean skin product of the present invention presses the Ministry of Public Health《Cosmetics health specification》(2007 editions) " acute dermal toxicity Once limit the quantity test method(s) " healthy adult rat is given, 180~220g of body weight, 20, male and female half and half, once percutaneously smear dosage 5000mg/kg body weight, observe 14 days, experiment rat body situation, diet, drinking-water, body weight increase are normal, do not occur obvious Intoxicating phenomenon and the phenomena of mortality, locate post mortem Non Apparent Abnormality, judge the nontoxic level in the true border of the product.
2nd, human trial
Skin sensitivity is selected from student crowd, has slight itch patient as volunteer, wherein man 20, female 20, Two groups are randomly divided into, applies the green peel of walnut clean skin product of embodiment 1 and the preparation of experimental example 1 at the itching of skin respectively.Make With being evaluated after 7 days, evaluation result is as follows:
Wherein, using in the volunteer (20 people) of embodiment 1,
Think that the product of embodiment 1 washes temperature-sensitive and rub the fine and smooth people of person 15, it is believed that product is washed temperature-sensitive and rubbed compared with general person 5 people;
Think to feel salubrious after washing, no people of tight feeling person 18;
Think there is antipruritic effect the people of person 18;
Volunteer's overall merit thinks that the product taste of embodiment 1 is light, moderate performance, and friction is fine and smooth, has preferably antipruritic Effect, acceptance level are high.
Using in the volunteer (20 people) of experimental example 1,
Think that the product of experimental example 1 washes temperature-sensitive and rub the fine and smooth people of person 10, it is believed that product is washed temperature-sensitive and rubbed compared with general person 8 people, it is believed that product washes temperature-sensitive and rub the rougher people of person 2;
Think to feel salubrious after washing, no people of tight feeling person 15;
Think there is the antipruritic people of whitening effect person 17;
Volunteer's overall merit thinks that the product taste of experimental example 1 is light, moderate performance, there is preferable antipruritic effect, receives Degree is higher.
The preferred embodiment of the application is the foregoing is only, is not limited to the application, for the skill of this area For art personnel, the application can have various modifications and variations.It is all within spirit herein and principle, made it is any Modification, equivalent substitution, improvement etc., should be included within the protection domain of the application.

Claims (10)

1. a kind of green peel of walnut clean skin product, it is characterised in that raw materials used to include in parts by weight:90~110 parts of soap base, core 8~12 parts of peach rascal powder, 3~7 parts of needles of pinus massoniana powder, 3~7 parts of licorice powder, 0.5~1.5 part of Chinese mugwort ash, luffa 0.4~0.6 Part;
Wherein, the soap base is the mixture and sodium hydroxide of olive oil and rilanit special through obtained by saponification.
2. a kind of green peel of walnut clean skin product as claimed in claim 1, it is characterised in that the olive oil and rilanit special Ratio of weight and number be 7~8:2~3.
A kind of 3. green peel of walnut clean skin product as claimed in claim 1, it is characterised in that the preparation side of the green peel of walnut powder Method is:The selection fresh green peel of walnut of this season is dried, and the sieve of 180 mesh is crossed after crushing;
The needles of pinus massoniana powder, preparation method thereof is:The fresh Pineneedles of Pinus Massoniana Lamb of selection selection this season cleans drying, and 80 mesh are crossed after crushing Sieve;
The preparation method of the licorice powder is:Selection has good quality, and without the radix glycyrrhizae to go mouldy, is directly smashed after cutting small pieces, crosses 140 mesh Sieve;
The grey preparation method of the Chinese mugwort is:Selection has good quality, and without the wormwood to go mouldy, burns into ash, i.e. Chinese mugwort ash, crosses 140 mesh sieves;
The luffa preparation method is:Full ripe sponge gourd is selected, remove seed gained luffa is removed the peel after drying, is cut into small Section, is put into mould after soaking water.
4. a kind of green peel of walnut clean skin product as claimed in claim 1, it is characterised in that raw materials used to be in parts by weight: 100 parts of soap base, 10 parts of green peel of walnut powder, 5 parts of needles of pinus massoniana powder, 5 parts of licorice powder, 1 part of Chinese mugwort ash, 0.5 part of luffa;
Wherein, the soap base is the mixture and sodium hydroxide of olive oil and rilanit special through saponification gained, the olive oil It is 7 with rilanit special ratio of weight and number:2.8.
5. the preparation method of any one of the claim 1-4 green peel of walnut clean skin products, it is characterised in that specific method is:
(1) pretreatment of raw material:
The selection fresh green peel of walnut of this season is dried, and the sieve of 180 mesh is crossed after crushing;
The fresh Pineneedles of Pinus Massoniana Lamb of selection selection this season cleans drying, and 80 mesh sieves are crossed after crushing;
Selection has good quality, and without the radix glycyrrhizae to go mouldy, is directly smashed after cutting small pieces, crosses 140 mesh sieves;
Selection has good quality, and without the wormwood to go mouldy, burns into ash, i.e. Chinese mugwort ash, crosses 140 mesh sieves;
Full ripe sponge gourd is selected, remove seed gained luffa is removed the peel after drying, segment is cut into, is put into after soaking water in mould;
(2) preparation of mixed powder:Green peel of walnut powder, needles of pinus massoniana powder, licorice powder, Chinese mugwort ash ratio in parts by weight is fully mixed It is even;
(3) grease is handled:
Rilanit special is placed in into 45 DEG C of heating water baths makes its thawing be liquid, by olive oil and rilanit special 7~8:2~3 (it is preferably 7:2.8) part by weight mixing, 50~60 DEG C of (being preferably 50 DEG C) heating water baths is placed in, keep olive oil, hydrogenation Castor oil mixes oils temperature stabilization at 50 DEG C;
(4) added according to a conventional method according to the saponification value of olive oil, rilanit special into olive oil, rilanit special miscella Sodium hydroxide carries out saponification;
Preferably, it is 50 DEG C to control saponification temperature, and the saponification time is 1.5~2.5h (being most preferably 2h);
(5) mould, cooled and solidified are entered:
In the lotion after the mixed powder in proportion preparing step (2) before entering mould adds saponification, quickly stir Pour into afterwards in the mould equipped with the luffa soaked, cooled and solidified processing.
6. preparation method as claimed in claim 5, it is characterised in that quick mixing time is 1~2min in the step (5) (be most preferably 1.5min), rotating speed are 80~120rpm (being most preferably 100rpm), and the cooled and solidified processing time is:Temperature Less than 10 DEG C, stand 2~3d.
7. preparation method as claimed in claim 5, it is characterised in that the preparation method of the green peel of walnut clean skin product also includes Step (6) demoulding, packaging:Demoulding processing is carried out to the soaps after solidification, the soap body after solidification is combined together with luffa, slightly Add finishing, make profile harmonious;The soap product of taking-up is put into preprepared packaging bag, sealing preserves.
8. application of any one of the claim 5-7 preparation methods in green peel of walnut clean skin product is prepared.
9. the application method of any one of the claim 1-5 green peel of walnut clean skin products, it is characterised in that with warm water before using Moistening skin, after green peel of walnut clean skin product is soaked, the rubbing on skin, reach physics and the dual antipruritic purpose of chemistry, then Massaged and cleaned with palm part, rinsed well with clear water, finally with the dry towel of quality soft texture by dry.
10. method as claimed in claim 9, it is characterised in that the palm massage scavenging period foundation skin oil dryness determination, The Oily time is 1min, Dry 0.5min.
CN201710959243.1A 2017-10-16 2017-10-16 A kind of green peel of walnut clean skin product and preparation method thereof Pending CN107779320A (en)

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CN109971570A (en) * 2019-04-22 2019-07-05 荆楚理工学院 A kind of functional luffa skeleton handmade soap and preparation method thereof
CN114525181A (en) * 2022-01-13 2022-05-24 安徽师范大学 Bathing bean soap and preparation method thereof

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CN109971570A (en) * 2019-04-22 2019-07-05 荆楚理工学院 A kind of functional luffa skeleton handmade soap and preparation method thereof
CN114525181A (en) * 2022-01-13 2022-05-24 安徽师范大学 Bathing bean soap and preparation method thereof

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