CN104721121B - A kind of skin-care cosmetics - Google Patents
A kind of skin-care cosmetics Download PDFInfo
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- CN104721121B CN104721121B CN201510146755.7A CN201510146755A CN104721121B CN 104721121 B CN104721121 B CN 104721121B CN 201510146755 A CN201510146755 A CN 201510146755A CN 104721121 B CN104721121 B CN 104721121B
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Abstract
A kind of skin-care cosmetics, belong to cosmetic technical field.By papaya extractives, kamuning and shaddock bark extract, cactus glue polysaccharide, okra pectin, royal jelly according to weight ratio 10 20:20‑40:10‑40:10‑30:10 20 ratio is made.A kind of skin-care cosmetics, reasonable mixture ratio of components, improve wrinkle of skin, anti-oxidant radiation protection, remove free radical, lighten the stain, decomposes melanin in terms of show it is good act synergistically and it is excellent the effect of.
Description
Technical field
The invention belongs to cosmetic technical field, specially a kind of skin-care cosmetics.
Background technology
Cosmetics and skin care item play an important role to the beautification and skin care of the mankind, and it is big that beauty has become 21 century ten
One of popular industry.During rapid economic development, from small to large, from weak to strong, brand is Chinese Cosmetic Market
It emerges in an endless stream, the Cosmetic Market of China has become the market of global maximum at present.Along with domestic consumer to cosmetics
Etc. the cognition of daily use chemicals industry be familiar with, more and more consumers focus more on safe and healthy, effective care method, especially
It is the appearance of plants herb class skin care item, further promotes the fast development of cosmetic industry.China possess it is abundant in
Herbal medicine resource, therefore the cosmetics of natural plant kind will have the development potentiality and the market space of bigger from now on.Natural makeup
Product are extracted from natural plants, the effects that playing nutrition protection and beauty treatment to the skin of human body, and will not be to skin
Skin causes the functional component that irritation is damaged.Therefore the vegetalization cosmetic for natural component being extracted from plant be opposite science and
The method of environmental protection.
Invention content
For the above-mentioned problems in the prior art, it is an object of the invention to design to provide a kind of skin-care cosmetics
Technical solution, reasonable mixture ratio of components, improve wrinkle of skin, anti-oxidant radiation protection, remove free radical, lighten the stain, point
Good the effect of acting synergistically and is excellent is shown in terms of solution melanin.
A kind of skin-care cosmetics, it is characterised in that by papaya extractives, kamuning and shaddock bark extract, celestial being
People slaps glue polysaccharide, okra pectin, royal jelly according to weight ratio 10-20: 20-40 : 10-40 : 10-30 : 10-20
Ratio be made；
The papaya extractives are prepared using following methods：Low temperature drying after pawpaw is sliced, by dried pawpaw
Piece is put in the container of smashing extractor, and it is aqueous to add in 60%-80% according to the pawpaw weight 1kg ratios that then hydrous ethanol 5-8 rises
Ethyl alcohol carries out crushing extraction 1-2 times, and each extraction time is 1-3 minutes, and extracting solution is filtered, discards filter residue, is merged
Extracting solution carries out flash concentration to the 1/6-1/10 of original volume below 70 DEG C using Reduced Pressure Concentration Device, continues to concentrate
Liquid is dried in vacuo into dry powder, with mortar it is finely ground after obtain papaya extractives dry powder；
The kamuning and shaddock bark extract is prepared using following methods：Take dry Murraya jasminorage leaf and dry shaddock
Sub- pericarp, according to weight ratio 1:1-2 is mixed, and is then put in the container of smashing extractor, according to raw material weight 1kg then hydrous ethanols
The ratio that 6-8 rises adds in 70%-100% ethyl alcohol and carries out crushing extraction 2-3 times, and each extraction time is 1-4 minutes, by extracting solution
It filters, discards filter residue, the extracting solution merged carries out flash concentration to original below 60 DEG C using Reduced Pressure Concentration Device
The 1/7-1/9 of volume continues concentrate being dried in vacuo into dry powder, with mortar it is finely ground after kamuning and pomelo peel extract
Object dry powder；
The cactus glue polysaccharide is prepared using following methods：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into
Fritter is weighed, and is put in the container of smashing extractor, adds in cactus 4-8 times of distilled water measured of fresh weight, is carried out high-speed stirred and is crushed
1-3 minutes, broken cactus mucilage is transferred out of, is centrifuged at a high speed, takes supernatant, supernatant is depressurized
The 1/3-1/6 of original volume is concentrated into, adds in absolute ethyl alcohol, stirring while adding, static alcohol analysis, is centrifuged at a high speed, abandons at 1-4 DEG C
Supernatant is removed, after sediment low temperature drying, obtains cactus glue polysaccharide；
The okra pectin is prepared using following methods：The okra okra fruit cleaned and dried is taken, is sliced with crosspiece face
Okra fruit after drying is placed in extraction vessel by low temperature drying afterwards, according to dosage of the raw material weight for 1kg then distilled water
Distillation water boiling and extraction is added in for the 6-10 ratios risen 2-3 times, it is 30-90 minutes each, it is centrifuged at a high speed, takes supernatant
Liquid；Obtained supernatant carries out flash concentration to the 1/6- of original volume under the conditions of 60-70 DEG C using Reduced Pressure Concentration Device
1/10, the ethyl alcohol of 92-95% is then added in into concentrate so that alcohol content reaches less than 80%, 1-4 DEG C static alcohol analysis, occurs
A large amount of precipitation, is centrifuged at a high speed, and discards supernatant liquid, collects sediment, and 40 DEG C of -50 DEG C of drying obtain okra pectin.
A kind of skin-care cosmetics, it is characterised in that papaya extractives, kamuning and shaddock bark extract, celestial being
Slap glue polysaccharide, okra pectin, royal jelly weight ratio be 12-18: 25-35 : 15-35 : 15-25 : 12-18.
A kind of skin-care cosmetics, it is characterised in that papaya extractives, kamuning and shaddock bark extract, celestial being
Slap glue polysaccharide, okra pectin, royal jelly weight ratio be 14-16: 28-32 : 18-30 : 18-22 : 15-16.
A kind of skin-care cosmetics, it is characterised in that in the preparation method of the papaya extractives：According to pawpaw
The weight 1kg ratios that then hydrous ethanol 6-7 rises add in 65%-75% hydrous ethanols and carry out crushing extraction 1 time, each extraction time
It is 2 minutes, the 1/7-1/9 of flash concentration to original volume.
A kind of skin-care cosmetics, it is characterised in that the preparation of the kamuning and shaddock bark extract extract
In method：The weight ratio 1 of Murraya jasminorage leaf and dry shaddock pericarp:1.5 mixing, according to raw material weight 1kg then 7 liters of hydrous ethanol
Ratio add in 80%-90% ethyl alcohol and carry out broken extraction, each extraction time is 2-3 minutes, extracting solution flash concentration to original
The 1/8 of volume.
A kind of skin-care cosmetics, it is characterised in that in the preparation method of the cactus glue polysaccharide：It adds in
The distilled water that 5-7 times of cactus fresh weight is measured carries out high-speed stirred and crushes 2 minutes, supernatant is carried out to be concentrated under reduced pressure into original volume
1/4-1/5.
A kind of skin-care cosmetics, it is characterised in that in the preparation method of the okra pectin：According to raw material
Weight is that the dosage of 1kg then distilled water is that the ratio that 7-9 rises adds in distillation water boiling and extraction, 50-60 minute each, supernatant sudden strain of a muscle
Inspissation is reduced to the 1/7-1/9 of original volume, and 42 DEG C of -45 DEG C of drying obtain okra pectin.
Pawpaw is the drying almost ripe fruit of rosaceous plant chaenomeles lagenaria.Summer, two season of autumn fruit it is greenish-yellow when harvest, put boiling
It is scalded in water to crust canescence, double of vertical profile dries.Pawpaw is warm-natured, sour, enters liver, the spleen channel；It is killed with reinforcing spleen to promote digestion, anti-epidemic disease
The effect of worm, promoting lactation anticancer, heat-clearing wind-dispelling；Cure mainly stomachache, indigestion, lung heat dry cough, alactation, eczema, parasitic disease,
The illnesss such as anti-spasm, trick spasm pain.Contain large quantity of moisture, carbohydrate, protein, fat, a variety of dimension lifes in pawpaw
Plain and a variety of amino acid needed by human can effectively supplement the nutrient of human body, enhance the disease resistance of body.
Kamuning be Rutaceae Murraya evergreen shrubs plant, also known as nine autumns perfume, nine tree perfume, murraya paniculataJack, Caulis et folium gaultheriae yunnanensis, mistake
Bee saage can grow up to dungarunga sample sometimes, and strain appearance is graceful, and branches and leaves are beautiful, and the fragrance of flowers is strong.Root, stem, chemical composition and a thousand li contained by leaf
It is fragrant similar, originate from the south such as Fujian, Guangdong, Hainan, Guangxi.Be common in the level land not far from seashore, gentle slope, hillock bushes
In.Murraya jasminorage leaf contains a variety of Coumarins compounds, and such as isomexoticin, murpanidin, murpanicin, come into leaves kamuning
Aldehyde separately containing flavonoids, amino acid, separately containing volatile oil, is aromatics plant, has removing blood stasis and analgesics；The effect of removing toxicity for detumescence, cures mainly
Treating rheumatic ostealgia is had a stomachache, toothache, lockjaw, tumbling and swelling；Sore carbuncle；Snakebite and bugbite.For having a stomachache, arthralgia pain due to rheumatism；Toothache is controlled outside,
Tumbling and swelling, worm snake bite.
Shaddock also known as pomelo, crust is very thick, is picked mostly in the 10-11 months.Shaddock is grown on south more, with Fujian, Xiamen
Produced shaddock is the most famous.Its fruit fresh food sweet acid is tasty, refreshing, makes us being profuse in praise, and pomelo peel has very high medicine
With value and edible value.And can be used as medicine, pomelo peel is warm-natured, bitter, pungent, containing ingredients such as flavonoids, volatile oil in pomelo peel,
It is eliminating dampness and eliminating phlegm with cold dispelling qi-regulating, the work of relax bowel, reduce blood viscosity, prevention headstroke, cold dispelling eliminating dampness etc.
With.
For cactus containing abundant protein, vitamin, carrotene, l0 several mineral materials and l8 kind amino acid, human body must
Must amino acid nearly all wherein, also containing organic acid, carbohydrate, flavonoids, alkaloids, sterols, terpene etc. have compared with
The chemical composition of strong pharmacological action.Cactus has extremely strong removing free radical anti-aging ability.Cactus polyoses have apparent
It is hypoglycemic, enhance immune function.The functions such as self-protection and radioresistance and effect.Cactus contains triterpenoid saponin, can be directly
It adjusts human secretory function and adjusts the activity of lipase, superabundant fats is promoted to decompose rapidly and are down to normally, and can effectively hinder
Only fat inhibits fat to be synthesized in liver, to anti-cholesterol, the deposition of blood vessel, incremental mitigation in intestinal absorption
Weight does not suffer tremendous loss in strength or resources not only, supplements the nutrients instead, increases human body energy.Glue polysaccharide in cactus includes mucilaginous substance, fruit
The heteromeric polysaccharide such as glue, arabogalactan, cellulose and starch etc., glue polysaccharide in cactus have heat-clearing, removing toxic substances,
Moisturizing, it is sun-proof the effect of.
Okra is annual herb plant, has the plantation of okra in China the South and the North various regions.It is rich in okra
Protein, fat, vitamin, minerals, dietary fiber, flavones, pectin, polysaccharide and other functional ingredient, particularly okra it is tender
The mucoid material being rich in fruit is the mixture by poly galactolipin, galactan and araban and pectin, wherein fruit
Glue is a kind of Soluble Fiber, it can promote the excretion of internal organic substance, reduces the accumulation of toxin, reduces blood glucose and cholesterol
Content.Glutinous sliding juice can help digest, and prevent constipation.With the works such as cancer anticancer, tonifying kidney and strengthening yang, strengthen immunity, aid digestion
With, while the water-soluble fibre pectin in okra has skin good health-care effect, okra pectin also has uniqueness
Beautifying face and moistering lotion, increase skin elasticity and anti-aging, dispel pigmentation and whitening function.
A kind of above-mentioned skin-care cosmetics, have the advantages that：
1. the present invention is the plant extract composition formula in pure plant source, environmentally protective, safe and healthy；Pawpaw is extracted
Use is improving skin while object, kamuning and shaddock bark extract, cactus glue polysaccharide, okra pectin and royal jelly
Wrinkle increases skin elasticity, removes free radical, lightens the stain, decomposing good act synergistically and excellent is shown in terms of melanin
The effect of different, is far longer than the effect that one of which is used alone.
It, should 2. the papaya extractives and Folium Et Cacumen Murrayae extract that contain in inventive formulation have certain antisepsis and sterilization effect
The addition of extract makes the product have good Antimicrobial preservative effect, ensure that microbiological indicator meets wanting for Cosmetic Manufacture
It asks；Contain flavones ingredient in the shaddock bark extract and okra pectin extraction object that contain in inventive formulation, belong to natural
Antioxidant, without additionally adding antioxidant with regard to the scavenging effect to free radical can be played.
3. being extracted in the present invention to pawpaw, kamuning and pomelo peel using room temperature Smashing extraction method, that is, utilize high speed rotation
Special tool raw material crushed into shearing to fine particle, by high-speed stirred, vibration, mixing, infiltration, impregnate, homogenize
Combination makes the active ingredient inside medicinal material be rapidly achieved dissolution balance；The extracting method realizes raw material and crushes and extract
It is completed while process, eliminates the process that medicinal material individually crushes, broken extraction time is extremely short, and primary extraction only needs a few minutes,
Extraction process avoids possibility of the thermo-labile component by heat damage, remains original battalion to the maximum extent without heating simultaneously
Foster and functional component has and extracts quick, complete, energy-efficient, easy to operate, working efficiency is high advantage；Obtain extracting solution
Low with concentrate heating temperature using Reduced Pressure Concentration Device progress flash concentration, heated time is extremely short, effective protection heat
Quick property ingredient is not destroyed, and the rate of recovery of solvent is high, and concentration speed is fast, efficient, easy to operate, easy to use, energy conservation and environmental protection
Etc. advantages.
Percentage composition involved in present patent application unless otherwise indicated outer, remaining is the pure material of active ingredient
Weight percentage.
Specific embodiment
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
The skin-care cosmetics are by papaya extractives, kamuning and shaddock bark extract, cactus glue polysaccharide, okra
Pectin, royal jelly are according to weight ratio 10: 40 :20 : 20 :10 ratio is made；
The preparation of papaya extractives：Dried papaya tablet is put smashing extractor by low temperature drying after pawpaw is sliced
In container, add in than 8 times 70% hydrous ethanols of amount of equivalent raw material weight and carry out crushing extraction 2 times, each extraction time is 2 points
Clock filters extracting solution, discards filter residue, and the extracting solution merged is dodged below 70 DEG C using Reduced Pressure Concentration Device
Inspissation is reduced to the 1/8 of original volume, continues concentrate vacuum drying into dry powder, with mortar it is finely ground after obtain papaya extractives and do
Powder, papaya extractives yield reach 25.9%；
The preparation of kamuning and shaddock bark extract：Dry Murraya jasminorage leaf and dry shaddock pericarp are taken, according to weight
Than 1:1 mixing, then puts in the container of smashing extractor, adds in equivalent 7 times of 95% ethyl alcohol of amount of mixed raw material weight ratio and is broken
It is broken extraction 2 times, each extraction time be 2 minutes, extracting solution is filtered, discards filter residue, the extracting solution merged 60 DEG C with
It is lower that flash concentration is carried out to the 1/6 of original volume using Reduced Pressure Concentration Device, continue concentrate being dried in vacuo into dry
Powder, with mortar it is finely ground after kamuning and shaddock bark extract dry powder, extract yield reach 18.4%.
The preparation of cactus glue polysaccharide：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into small pieces, weighs, put broken
In the container of extractor, the distilled water of 6 times of amounts of cactus fresh weight is added in, high-speed stirred is carried out and crushes 3 minutes, by broken celestial being
People slaps mucilage and is transferred out of, and is centrifuged at a high speed, takes supernatant.Supernatant is carried out to be concentrated under reduced pressure into the 1/6 of original volume, is added
Enter absolute ethyl alcohol, stirring while adding, less than 4 DEG C static alcohol analysis are centrifuged at a high speed, discard supernatant liquid, sediment low temperature drying
Afterwards, cactus glue polysaccharide is obtained, the yield of cactus glue polysaccharide reaches 29.6%.
The preparation of okra pectin：The okra okra fruit cleaned and dried is taken, low temperature drying after being sliced with crosspiece face.It will drying
Okra fruit afterwards is placed in extraction vessel, adds in distillation water boiling and extraction 3,60 minutes every time, be 1kg according to raw material weight
Then the dosage of distilled water is 8 liters of ratio.It is centrifuged at a high speed, takes supernatant, obtained supernatant is under the conditions of 70 DEG C
Using Reduced Pressure Concentration Device progress flash concentration to the 1/8 of original volume, 95% ethyl alcohol is then added in into concentrate, is made
It obtains alcohol content and reaches 80%, less than 4 DEG C static alcohol analysis a large amount of precipitation occur, are centrifuged at a high speed, discard supernatant liquid, collection is heavy
Starch, 40 DEG C of -50 DEG C of drying, obtains okra pectin, the yield of okra pectin reaches 33.5%.
Embodiment 2
The skin-care cosmetics are by papaya extractives, kamuning and shaddock bark extract, cactus glue polysaccharide, okra
Pectin, royal jelly are according to weight ratio 15:35:20 : 15 :15 ratio is made；
The preparation of papaya extractives：Low temperature drying after pawpaw is sliced.Dried papaya tablet is put into smashing extractor
In container, add in than 5 times 60% hydrous ethanols of amount of equivalent raw material weight and carry out crushing extraction 2 times, each extraction time is 3 points
Clock filters extracting solution, discards filter residue, and the extracting solution merged is dodged below 70 DEG C using Reduced Pressure Concentration Device
Inspissation is reduced to the 1/6 of original volume, continues concentrate vacuum drying into dry powder, with mortar it is finely ground after obtain papaya extractives and do
Powder, papaya extractives yield reach 18.4%.
The preparation of kamuning and shaddock bark extract：Dry Murraya jasminorage leaf and dry shaddock pericarp are taken, according to weight
Than 1:1 mixing, then puts in the container of smashing extractor, adds in equivalent 8 times of 90% ethyl alcohol of amount of mixed raw material weight ratio and is broken
Broken to extract 3 times, each extraction time is 1 minute.Extracting solution is filtered, discards filter residue, the extracting solution merged 60 DEG C with
It is lower that flash concentration is carried out to the 1/8 of original volume using Reduced Pressure Concentration Device, continue concentrate being dried in vacuo into dry
Powder, with mortar it is finely ground after kamuning and shaddock bark extract dry powder, extract yield reach 20.3%.
The preparation of cactus glue polysaccharide：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into small pieces, weighs, put broken
In the container of extractor, the distilled water of 7 times of amounts of cactus fresh weight is added in, high-speed stirred is carried out and crushes 2 minutes, by broken celestial being
People slaps mucilage and is transferred out of, and is centrifuged at a high speed, takes supernatant, supernatant is carried out to be concentrated under reduced pressure into the 1/7 of original volume, is added
Enter absolute ethyl alcohol, stirring while adding, less than 4 DEG C static alcohol analysis are centrifuged at a high speed, discard supernatant liquid, sediment low temperature drying
Afterwards, cactus glue polysaccharide is obtained, the yield of cactus glue polysaccharide reaches 28.4%-37.8%.
The preparation of okra pectin：The okra okra fruit cleaned and dried is taken, low temperature drying after being sliced with crosspiece face.It will drying
Okra fruit afterwards is placed in extraction vessel, adds in distillation water boiling and extraction 2 times, 90 minutes every time, is according to raw material weight
The dosage of 1kg then distilled water is 10 liters of ratio, is centrifuged at a high speed, takes supernatant, obtained supernatant is in 70 DEG C of items
Using Reduced Pressure Concentration Device progress flash concentration to the 1/10 of original volume under part, 95% second is then added in into concentrate
Alcohol so that alcohol content reaches 80%, and less than 4 DEG C static alcohol analysis a large amount of precipitation occur, are centrifuged at a high speed, discard supernatant liquid,
Sediment is collected, 40 DEG C of -50 DEG C of drying obtain okra pectin, the yield of okra pectin reaches 38.4%.
Embodiment 3
The skin-care cosmetics are by papaya extractives, kamuning and shaddock bark extract, cactus glue polysaccharide, okra
Pectin, royal jelly are according to weight ratio 20:30:30 : 10 :10 ratio is made；
The preparation of papaya extractives：Low temperature drying after pawpaw is sliced.Dried papaya tablet is put into smashing extractor
In container, add in than 6 times 75% hydrous ethanols of amount of equivalent raw material weight and carry out crushing extraction 2 times, each extraction time is 3 points
Clock filters extracting solution, discards filter residue, and the extracting solution merged is dodged below 70 DEG C using Reduced Pressure Concentration Device
Inspissation is reduced to the 1/7 of original volume, continues concentrate vacuum drying into dry powder, with mortar it is finely ground after obtain papaya extractives and do
Powder, papaya extractives yield reach 23.7%.
The preparation of kamuning and shaddock bark extract：Dry Murraya jasminorage leaf and dry shaddock pericarp are taken, according to weight
Than 1:1 mixing, then puts in the container of smashing extractor, adds in equivalent 6 times of 100% ethyl alcohol of amount of mixed raw material weight ratio and is broken
It is broken extraction 2 times, each extraction time be 3 minutes, extracting solution is filtered, discards filter residue, the extracting solution merged 60 DEG C with
It is lower that flash concentration is carried out to the 1/7 of original volume using Reduced Pressure Concentration Device, continue concentrate being dried in vacuo into dry
Powder, with mortar it is finely ground after kamuning and shaddock bark extract dry powder, extract yield reach 17.4%.
The preparation of cactus glue polysaccharide：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into small pieces, weighs, put broken
In the container of extractor, the distilled water of 5 times of amounts of cactus fresh weight is added in, high-speed stirred is carried out and crushes 3 minutes, by broken celestial being
People slaps mucilage and is transferred out of, and is centrifuged at a high speed, takes supernatant.Supernatant is carried out to be concentrated under reduced pressure into the 1/5 of original volume, is added
Enter absolute ethyl alcohol, stirring while adding, less than 4 DEG C static alcohol analysis.It is centrifuged at a high speed, discards supernatant liquid, sediment low temperature drying
Afterwards, cactus glue polysaccharide is obtained, the yield of cactus glue polysaccharide reaches 30.4%.
The preparation of okra pectin：The okra okra fruit cleaned and dried is taken, low temperature drying after being sliced with crosspiece face.It will drying
Okra fruit afterwards is placed in extraction vessel, adds in distillation water boiling and extraction 3 times, 70 minutes every time, is according to raw material weight
The dosage of 1kg then distilled water is 9 liters of ratio.It is centrifuged at a high speed, takes supernatant, obtained supernatant is in 70 DEG C of conditions
It is lower that flash concentration is carried out to the 1/9 of original volume using Reduced Pressure Concentration Device, 95% ethyl alcohol is then added in into concentrate,
So that alcohol content reaches 80%, there is a large amount of precipitation, are centrifuged at a high speed, discard supernatant liquid, collect in less than 4 DEG C static alcohol analysis
Sediment, 40 DEG C of -50 DEG C of drying, obtains okra pectin, the yield of okra pectin reaches 34.2%.
Embodiment 4
The skin-care cosmetics are by papaya extractives, kamuning and shaddock bark extract, cactus glue polysaccharide, okra
Pectin, royal jelly are according to weight ratio 15:30:20 : 25 :10 ratio is made；
The preparation of papaya extractives：Dried papaya tablet is put smashing extractor by low temperature drying after pawpaw is sliced
In container, add in than 7 times 80% hydrous ethanols of amount of equivalent raw material weight and carry out crushing extraction 2 times, each extraction time is 1 point
Clock filters extracting solution, discards filter residue, and the extracting solution merged is dodged below 70 DEG C using Reduced Pressure Concentration Device
Inspissation is reduced to the 1/7 of original volume, continues concentrate vacuum drying into dry powder, with mortar it is finely ground after obtain papaya extractives and do
Powder, papaya extractives yield reach 24.1%.
The preparation of kamuning and shaddock bark extract：Dry Murraya jasminorage leaf and dry shaddock pericarp are taken, according to weight
Than 1:1 mixing, then puts in the container of smashing extractor, adds in equivalent 6 times of 80% ethyl alcohol of amount of mixed raw material weight ratio and is broken
It is broken extraction 2 times, each extraction time be 2 minutes, extracting solution is filtered, discards filter residue, the extracting solution merged 60 DEG C with
It is lower that flash concentration is carried out to the 1/7 of original volume using Reduced Pressure Concentration Device, continue concentrate being dried in vacuo into dry
Powder, with mortar it is finely ground after kamuning and shaddock bark extract dry powder, extract yield reach 20.3%.
The preparation of cactus glue polysaccharide：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into small pieces, weighs, put broken
In the container of extractor, the distilled water of 8 times of amounts of cactus fresh weight is added in, high-speed stirred is carried out and crushes 2 minutes, by broken celestial being
People slaps mucilage and is transferred out of, and is centrifuged at a high speed, takes supernatant.Supernatant is carried out to be concentrated under reduced pressure into the 1/5 of original volume, is added
Enter absolute ethyl alcohol, stirring while adding, less than 4 DEG C static alcohol analysis.It is centrifuged at a high speed, discards supernatant liquid, sediment low temperature drying
Afterwards, cactus glue polysaccharide is obtained, the yield of cactus glue polysaccharide reaches 32.1%.
The preparation of okra pectin：The okra okra fruit cleaned and dried is taken, low temperature drying after being sliced with crosspiece face will dry
Okra fruit afterwards is placed in extraction vessel, adds in distillation water boiling and extraction 3 times, 30 minutes every time, is according to raw material weight
The dosage of 1kg then distilled water is 6 liters of ratio.It is centrifuged at a high speed, takes supernatant.Obtained supernatant is in 70 DEG C of conditions
It is lower that flash concentration is carried out to the 1/6 of original volume using Reduced Pressure Concentration Device, 95% ethyl alcohol is then added in into concentrate,
So that alcohol content reaches 80%, there is a large amount of precipitation, are centrifuged at a high speed, discard supernatant liquid, collect in less than 4 DEG C static alcohol analysis
Sediment, 40 DEG C of -50 DEG C of drying, obtains okra pectin, the yield of okra pectin reaches 28.7%.
Except more than plant extract beyond the region of objective existence is contained in the cosmetic composition of the present invention, auxiliary agent and carrier are further included, is contained
Cosmetic additive and carrier can include preservative, antioxidant, thickener, stabilizer, flavouring agent, forming agent, emulsifier, alcohol
Class and esters solvent, oils, polymer water etc.；Specific auxiliary agent and carrier can be polyethylene glycol, polysorbate, stearic acid,
Cyclodextrin, lauryl sodium sulfate, hydroxyethyl cellulose, ethyl acetate, Ergol, ethyl alcohol, propylene glycol, dimethyl-silicon
Oil, glycerine, castor oil etc., the preparation that cosmetic composition of the invention can be fabricated to, including face breast, skin cream, skin-tendering cream,
Face cream, facial mask etc., specific preparation process belong to routine techniques.
A kind of production technology of skin-care cosmetics of the present invention is, first according to the weight hundred of the formula in embodiment
Point ratio weighs each component, obtains mixed material, then mixes various auxiliary agents and carrier, under 70-80 DEG C or so of heating
Magnetic agitation, mixing, homogeneity and emulsification are carried out, 50 DEG C -60 DEG C is then cooled the temperature to, adds in prepared material and continue to stir
Mix mixing, homogeneity and emulsification, it is ensured that addition is mutually completely dissolved so that subject to emulsion bubble-free occurs, stop heating stirring,
It places to room temperature and obtains finished product.
The advantageous effect further illustrated the present invention below in conjunction with corresponding test data.
Experiment 1：Increase the soothing effect experiment of skin elasticity
To prove its soothing effect to skin of face, soothing effect experiment is carried out using embodiment 1-4.Smearing position is
Face, subjects are 50-60 Sui, and skin elasticity is poor, the women of dry skin.After each face cleaning, daily in the facial morning and evening
It is smeared twice, while carries out softly, adhering to trying out 1 month, the soothing effect of follow-up subjects face with hand.
Embodiment 1-4 increases the soothing effect experiment of skin elasticity
| Embodiment | Tested number | Significant effective | Effectively | In vain | It is efficient |
| Embodiment 1 | 8 | 4 | 4 | 0 | 100% |
| Embodiment 2 | 8 | 5 | 3 | 0 | 100% |
| Embodiment 3 | 8 | 3 | 5 | 0 | 100% |
| Embodiment 4 | 8 | 4 | 4 | 0 | 100% |
Experiment 2：Improve the wrinkle-proof effect experiment of wrinkle of skin
To prove that it improves the effect of face skin wrinkle, using embodiment 1-4 improve the wrinkle resistant effect of wrinkle of skin
Fruit is tested.Position is smeared as face, subjects are 50-60 Sui, the more women of wrinkle of skin.After each face cleaning, in face
And eyes edge daily sooner or later smeared twice, while with hand carries out softly with massage, massage time 3-4 minute,
Adhere to 2 months on probation, the improvement situation of follow-up subjects face and eye part skin wrinkle.
Embodiment 1-4 improves the wrinkle-proof effect experiment of wrinkle of skin
| Embodiment | Tested number | Significant effective | Effectively | In vain | It is efficient |
| Embodiment 1 | 10 | 4 | 5 | 1 | 90% |
| Embodiment 2 | 10 | 3 | 6 | 1 | 90% |
| Embodiment 3 | 12 | 5 | 5 | 2 | 83.3% |
| Embodiment 4 | 12 | 4 | 6 | 2 | 83.3% |
Experiment 3：The sun-proof result experiment of anti-oxidant radiation protection
To prove that its is anti-oxidant, removes the sun-proof result of free radical, the anti-of anti-oxidant radiation protection is carried out using embodiment 1-4
Shine effect test.Position is smeared as face, subjects are the women of 20-40 Sui.After each face cleaning, in facial progress early daily
It smears, tries out 1 month, follow-up subjects try out rear radioresistance, sun-proof application effect.
The sun-proof result experiment of the anti-oxidant radiation protections of embodiment 1-4
| Embodiment | Tested number | Significant effective | Effectively | In vain | It is efficient |
| Embodiment 1 | 6 | 3 | 3 | 0 | 100% |
| Embodiment 2 | 6 | 3 | 3 | 0 | 100% |
| Embodiment 3 | 6 | 2 | 3 | 1 | 83.3% |
| Embodiment 4 | 6 | 2 | 3 | 1 | 83.3% |
Experiment 4：Lighten the stain, decompose the freckle effect experiment of melanin
For prove its desalinate facial colour spot, decompose melanin freckle effect, lightened the stain using embodiment 1-4,
Decompose the freckle effect experiment of melanin.Position is smeared as face, subjects are 30-45 Sui, face has the women of color spot.Often
It after secondary face cleaning, is smeared twice sooner or later daily in entire face, while soft to there is color spot position emphasis to smear, adheres to trying out
2 months, follow-up subjects tried out rear freckle effect.
Embodiment 1-4 lightens the stain, decomposes the freckle effect experiment of melanin
| Embodiment | Tested number | Significant effective | Effectively | In vain | It is efficient |
| Embodiment 1 | 10 | 3 | 6 | 1 | 90% |
| Embodiment 2 | 10 | 4 | 5 | 1 | 90% |
| Embodiment 3 | 10 | 4 | 4 | 2 | 80% |
| Embodiment 4 | 10 | 3 | 5 | 2 | 80% |
Claims (2)
1. a kind of skin-care cosmetics, it is characterised in that by papaya extractives, kamuning and shaddock bark extract, cactus mucus
Polysaccharide, okra pectin, royal jelly are according to weight ratio 10: 40 :20 : 20 :10 ratio is made；
The preparation of papaya extractives：Dried papaya tablet is put the container of smashing extractor by low temperature drying after pawpaw is sliced
In, it adds in than 8 times 70% hydrous ethanols of amount of equivalent raw material weight and carries out crushing extraction 2 times, each extraction time is 2 minutes, will
Extracting solution filters, and discards filter residue, the extracting solution merged using Reduced Pressure Concentration Device flash dense below 70 DEG C
Be reduced to the 1/8 of original volume, continue concentrate vacuum drying into dry powder, with mortar it is finely ground after obtain papaya extractives dry powder；
The preparation of kamuning and shaddock bark extract：Dry Murraya jasminorage leaf and dry shaddock pericarp are taken, according to weight ratio 1:1
Mixing, then puts in the container of smashing extractor, adds in equivalent 7 times of 95% ethyl alcohol of amount of mixed raw material weight ratio and carries out broken extraction
2 times, each extraction time is 2 minutes, and extracting solution is filtered, discards filter residue, the extracting solution merged uses below 60 DEG C
Reduced Pressure Concentration Device carries out flash concentration to the 1/6 of original volume, continues concentrate being dried in vacuo into dry powder, with grinding
Kamuning and shaddock bark extract dry powder are obtained after alms bowl is finely ground；
The preparation of cactus glue polysaccharide：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into small pieces, weighs, put broken extraction
In the container of device, the distilled water of 6 times of amounts of cactus fresh weight is added in, high-speed stirred is carried out and crushes 3 minutes, by broken cactus
Mucilage is transferred out of, and is centrifuged at a high speed, and takes supernatant, and supernatant is carried out to be concentrated under reduced pressure into the 1/6 of original volume, adds in nothing
Water-ethanol, stirring while adding, less than 4 DEG C static alcohol analysis are centrifuged at a high speed, discard supernatant liquid, after sediment low temperature drying, obtain
To cactus glue polysaccharide；
The preparation of okra pectin：The okra okra fruit cleaned and dried is taken, low temperature drying after being sliced with crosspiece face, after drying
Okra fruit is placed in extraction vessel, is added in distillation water boiling and extraction 3,60 minutes every time, is then steamed for 1kg according to raw material weight
The dosage of distilled water is 8 liters of ratio, is centrifuged at a high speed, takes supernatant, obtained supernatant uses under the conditions of 70 DEG C
Reduced Pressure Concentration Device carries out flash concentration to the 1/8 of original volume, 95% ethyl alcohol is then added in into concentrate so that contain
Alcohol amount reaches 80%, and less than 4 DEG C static alcohol analysis a large amount of precipitation occur, are centrifuged at a high speed, discard supernatant liquid, collect precipitation
Object, 40 DEG C of -50 DEG C of drying, obtains okra pectin.
2. a kind of skin-care cosmetics, it is characterised in that by papaya extractives, kamuning and shaddock bark extract, cactus mucus
Polysaccharide, okra pectin, royal jelly are according to weight ratio 15:35:20 : 15 :15 ratio is made；
The preparation of papaya extractives：Dried papaya tablet is put the container of smashing extractor by low temperature drying after pawpaw is sliced
In, it adds in than 5 times 60% hydrous ethanols of amount of equivalent raw material weight and carries out crushing extraction 2 times, each extraction time is 3 minutes, will
Extracting solution filters, and discards filter residue, the extracting solution merged using Reduced Pressure Concentration Device flash dense below 70 DEG C
Be reduced to the 1/6 of original volume, continue concentrate vacuum drying into dry powder, with mortar it is finely ground after obtain papaya extractives dry powder；
The preparation of kamuning and shaddock bark extract：Dry Murraya jasminorage leaf and dry shaddock pericarp are taken, according to weight ratio 1:1
Mixing, then puts in the container of smashing extractor, adds in equivalent 8 times of 90% ethyl alcohol of amount of mixed raw material weight ratio and carries out broken extraction
3 times, each extraction time is 1 minute, and extracting solution is filtered, discards filter residue, the extracting solution merged uses below 60 DEG C
Reduced Pressure Concentration Device carries out flash concentration to the 1/8 of original volume, continues concentrate being dried in vacuo into dry powder, with grinding
Kamuning and shaddock bark extract dry powder are obtained after alms bowl is finely ground；
The preparation of cactus glue polysaccharide：Fresh cactus is taken to clean, except thorn is removed the peel, is cut into small pieces, weighs, put broken extraction
In the container of device, the distilled water of 7 times of amounts of cactus fresh weight is added in, high-speed stirred is carried out and crushes 2 minutes, by broken cactus
Mucilage is transferred out of, and is centrifuged at a high speed, and takes supernatant, and supernatant is carried out to be concentrated under reduced pressure into the 1/7 of original volume, adds in nothing
Water-ethanol, stirring while adding, less than 4 DEG C static alcohol analysis are centrifuged at a high speed, discard supernatant liquid, after sediment low temperature drying, obtain
To cactus glue polysaccharide；
The preparation of okra pectin：The okra okra fruit cleaned and dried is taken, low temperature drying after being sliced with crosspiece face, after drying
Okra fruit is placed in extraction vessel, adds in distillation water boiling and extraction 2 times, 90 minutes every time, according to raw material weight for 1kg then
The dosage of distilled water is 10 liters of ratio, is centrifuged at a high speed, takes supernatant, obtained supernatant is adopted under the conditions of 70 DEG C
Flash concentration is carried out to the 1/10 of original volume with Reduced Pressure Concentration Device, and 95% ethyl alcohol is then added in into concentrate so that
Alcohol content reaches 80%, and less than 4 DEG C static alcohol analysis a large amount of precipitation occur, are centrifuged at a high speed, discard supernatant liquid, collect precipitation
Object, 40 DEG C of -50 DEG C of drying, obtains okra pectin.
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| CN201510146755.7A Expired - Fee Related CN104721121B (en) | 2015-03-31 | 2015-03-31 | A kind of skin-care cosmetics |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055299A (en) * | 2015-09-27 | 2015-11-18 | 龚灿锋 | Whitening and skin protecting emulsion |
| CN109700724A (en) * | 2019-03-05 | 2019-05-03 | 陈伟伟 | A kind of cosmetic face cream and preparation method thereof added with camellia flower extract |
| CN110538113A (en) * | 2019-09-27 | 2019-12-06 | 广州环亚化妆品科技有限公司 | Traditional Chinese medicine composition with moisturizing and hydrating effects and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102727630A (en) * | 2012-06-29 | 2012-10-17 | 河南中医学院 | Plant extract dripping pill |
| CN104042538A (en) * | 2014-05-31 | 2014-09-17 | 青岛博泓海洋生物技术有限公司 | Whitening and firming mask |
| CN104288061A (en) * | 2014-11-09 | 2015-01-21 | 陈佩诗 | Skin-beautifying health massage solution |
| CN104434617A (en) * | 2014-07-22 | 2015-03-25 | 程远韶 | Pawpaw nutritional mask |
| CN104435240A (en) * | 2014-05-19 | 2015-03-25 | 南京正亮医药科技有限公司 | Kamuning massaging emulsion |
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2015
- 2015-03-31 CN CN201510146755.7A patent/CN104721121B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102727630A (en) * | 2012-06-29 | 2012-10-17 | 河南中医学院 | Plant extract dripping pill |
| CN104435240A (en) * | 2014-05-19 | 2015-03-25 | 南京正亮医药科技有限公司 | Kamuning massaging emulsion |
| CN104042538A (en) * | 2014-05-31 | 2014-09-17 | 青岛博泓海洋生物技术有限公司 | Whitening and firming mask |
| CN104434617A (en) * | 2014-07-22 | 2015-03-25 | 程远韶 | Pawpaw nutritional mask |
| CN104288061A (en) * | 2014-11-09 | 2015-01-21 | 陈佩诗 | Skin-beautifying health massage solution |
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| CN104721121A (en) | 2015-06-24 |
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Inventor after: Cai Rongrong Inventor after: Yuan Ke Inventor after: Wang Guanghua Inventor after: Yang Zhonghan Inventor after: Niu Yingpeng Inventor after: Jia Panpan Inventor before: Yuan Ke Inventor before: Wang Guanghua Inventor before: Yang Zhonghan Inventor before: Niu Yingpeng Inventor before: Jia Panpan |
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Effective date of registration: 20190718 Address after: Building No. 1899 Shangshu Road, Fengxian District, Shanghai, 201414 Patentee after: Shanghai Aiying Health Technology Co.,Ltd. Address before: 311800, No. 77, Puyang Road, Zhuji, Zhejiang, Shaoxing Patentee before: JIYANG COLLEGE OF ZHEJIANG A&F UNIVERSITY |
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Denomination of invention: A kind of skin care cosmetics Effective date of registration: 20210323 Granted publication date: 20180615 Pledgee: Pacific Anxin Agricultural Insurance Co.,Ltd. Shanghai Fengxian Branch Pledgor: Shanghai Aiying Health Technology Co.,Ltd. Registration number: Y2021310000018 |
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