CN111139152B - Vinegar residue mature vinegar cold-made soap and preparation method thereof - Google Patents
Vinegar residue mature vinegar cold-made soap and preparation method thereof Download PDFInfo
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- CN111139152B CN111139152B CN202010060221.3A CN202010060221A CN111139152B CN 111139152 B CN111139152 B CN 111139152B CN 202010060221 A CN202010060221 A CN 202010060221A CN 111139152 B CN111139152 B CN 111139152B
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- vinegar
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/48—Superfatting agents
Abstract
The invention relates to a cold soap of vinegar residue mature vinegar and a preparation method thereof, wherein the cold soap comprises the following raw materials: cold pressing olive oil, avocado oil, hazelnut oil, coconut oil, palm oil, shea butter, grape seed oil, distilled water, mature vinegar, caustic soda, and vinegar residue powder; the vinegar residue powder is prepared by performing enzymolysis on vinegar residue after vinegar leaching, drying and crushing, wherein the enzymolysis is to perform enzymolysis on the vinegar residue by adding cellulase and beta-mannase, so that the content of soluble cellulose in the vinegar residue is 25-45%, and the content of insoluble solids is 55-75%; adding mature vinegar and vinegar residue powder when the soap solution is nearly thick, stirring uniformly, and solidifying and saponifying; the cold-processed handmade soap of the mature vinegar and vinegar residue, which is manufactured by the invention, not only can deeply clean the skin, but also has the effects of moisturizing, nourishing the skin, removing cutin and the like, and reduces the stimulation to the skin.
Description
Technical Field
The invention relates to the technical field of daily-use cleaning products, in particular to a handmade soap, and more particularly relates to a cold-made soap of vinegar residue and mature vinegar and a preparation method thereof.
Background
At present, most of the facial soap sold in the market contains some chemical components, and the facial soap containing the chemical components can cause certain irritation to the skin after long-term use. The cold soap is a natural soap rich in glycerin and obtained by low-temperature saponification of vegetable oil and alkali, and has good skin care effect.
The vinegar residue is residue after mature vinegar brewing, and amino acids and organic acids contained in the vinegar residue have effects of nourishing skin, and can be pulverized to remove dead skin on skin. Mature vinegar is rich in amino acids and organic acids, but has been used only for seasoning, but is gradually applied to daily cleaning such as face washing and foot washing along with the deep knowledge of the public on the mature vinegar.
Disclosure of Invention
The invention overcomes the defects in the prior art and provides a cold soap made of vinegar residue and mature vinegar and a preparation method thereof.
The invention is realized by the following technical scheme.
The cold soap made of vinegar residue and mature vinegar specifically comprises the following raw materials in percentage by mass: 17% -21% of cold-pressed olive oil, 8% -10% of avocado oil, 7% -11% of hazelnut oil, 8% -10% of coconut oil, 5% -8% of palm oil, 5% -8% of shea butter, 2% -6% of grape seed oil, 15% -19% of distilled water, 8% -10% of mature vinegar, 7% -11% of caustic soda and 2% -5% of vinegar residue powder.
Preferably, the mature vinegar is vinegar which is obtained by performing solid state fermentation and ageing on sorghum, barley, peas, bran and bran coat.
Preferably, the ageing time is 2-5 years.
Preferably, the vinegar residue powder is prepared by performing enzymolysis on vinegar residue after vinegar leaching, drying and crushing, wherein the enzymolysis is to perform enzymolysis on the vinegar residue by adding cellulase and beta-mannase, so that the content of soluble cellulose in the vinegar residue is 25-45%, and the content of insoluble solids is 55-75%.
A preparation method of a vinegar residue mature vinegar cold soap comprises the following specific steps:
1) preparing vinegar residue powder: taking vinegar residue after vinegar leaching, pulverizing to 20-50 mesh, adding cellulase 0.5-1.5% of the weight of the vinegar residue and beta-mannase 0.2-0.8% of the weight of the vinegar residue for enzymolysis, drying after enzymolysis, and pulverizing to 80-100 mesh.
2) Dissolving oil and alkali liquor, and mixing the oil and the alkali liquor to prepare soap liquid;
3) adding the aged vinegar and the vinegar residue powder when the soap solution is nearly thick, and continuously stirring until the mixture is uniformly mixed;
4) coagulating and saponifying.
Further, the enzymolysis temperature is 25-35 ℃, and the enzymolysis time is 8-12 h.
Further, the alkali liquor is prepared by pouring water into caustic soda to be fully dissolved and cooling to room temperature.
Further, the solidification and saponification is to slowly pour the uniformly mixed soap liquid into a clean mould for several times, and standing to solidify the soap liquid; placing the soap after being molded into a constant temperature incubator at 25 ℃ for heat preservation for 24 hours; placing the heat-preserved soap at room temperature for 1-2 days, and taking out the soap from the mold; placing the taken-out soap in a dry and ventilated room, and saponifying for 60-90 days to obtain the soap.
Compared with the prior art, the invention has the following beneficial effects:
the cold soap is a natural soap body rich in glycerin obtained by saponifying various different vegetable oils and alkali at low temperature, wherein the glycerin can play a role in moisturizing and nourishing the skin; the solid-state fermentation and aging of the mature vinegar result in increased contents of non-volatile acids and ester phenolic substances, increased contents of antioxidant components, amino acids and organic acids in the soap body, the amino acids can relieve skin sensitivity and effectively protect skin surface sebum, the addition of the organic acids can neutralize incompletely saponified alkali liquor, reduce the damage of residual alkali liquor to skin, and the ester component has the function of blending vegetable oil.
Tyrosinase is a key enzyme for synthesizing melanin in a human body, and when the activity of tyrosinase is inhibited, the synthesis amount of melanin in the body is reduced, so that the tyrosinase has the effects of removing freckles and whitening the skin. Experiments show that the inhibition rates of Shanxi mature vinegar aged for 3 years and 5 years on tyrosinase are 18% and 10% respectively. Therefore, the Shanxi mature vinegar can inhibit the activity of tyrosinase and reduce the synthesis of melanin, thereby achieving the effects of whitening and removing freckles.
The addition of the vinegar residue powder can achieve the effect of removing cutin, and on the other hand, as the vinegar residue is subjected to enzymolysis, one part of the vinegar residue is converted into soluble fibers, and covalent bonds are formed between the soluble fibers and water molecules, so that the effect of moisturizing can be fully achieved, bran components with higher roughness in the vinegar residue are further soft, and the stimulation to skin in the process of removing cutin is reduced, so that the cold-made handmade soap with the aged vinegar residue can deeply clean the skin, and has the effects of moisturizing, nourishing the skin, removing the cutin and the like.
Detailed Description
In order to make the technical problems, technical solutions and advantageous effects to be solved by the present invention more clearly apparent, the present invention is further described in detail with reference to the embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention. The technical solutions of the present invention are described in detail below with reference to examples, but the scope of protection is not limited thereto.
Example 1
The cold soap made of vinegar residue and mature vinegar specifically comprises the following raw materials in percentage by mass: 17% of cold-pressed olive oil, 8% of avocado oil, 10% of hazelnut oil, 8% of coconut oil, 5% of palm oil, 8% of shea butter, 4% of grape seed oil, 19% of distilled water, 8% of mature vinegar with 5 ° of total acid, 8% of caustic soda and 5% of vinegar residue powder.
The mature vinegar is vinegar prepared by fermenting sorghum, barley, pea, bran and bran coat in solid state and aging for 3 years.
The vinegar residue powder is prepared by performing enzymolysis on vinegar residues after vinegar spraying, drying and crushing, wherein the enzymolysis is to perform enzymolysis on the vinegar residues by adding cellulase and beta-mannase, so that the content of soluble cellulose in the vinegar residues is 30%, and the content of insoluble solids is 55%.
The preparation method of the vinegar residue cold soap comprises the following specific steps:
preparing vinegar residue powder: taking vinegar residue after vinegar pouring, crushing into 50 meshes, adding cellulase accounting for 1 percent of the weight of the vinegar residue and beta-mannase accounting for 0.8 percent of the weight of the vinegar residue, adding distilled water accounting for 10 percent of the weight of the vinegar residue, carrying out enzymolysis, drying after the enzymolysis, and crushing into 80 meshes. The enzymolysis temperature is 35 ℃, and the enzymolysis time is 12 h.
1. Weighing cold-pressed olive oil, avocado oil, hazelnut oil, coconut oil, palm oil, shea butter and grape seed oil according to a formula, wherein each oil is weighed twice, so that each oil is accurately weighed.
2. Caustic soda is accurately weighed, and the remaining distilled water is poured into the caustic soda to be sufficiently dissolved and cooled to room temperature.
3. Mixing the weighed grease, and dissolving the mixture on a small fire.
4. Heating the mixed oil and the dissolved alkali liquor, slowly adding the alkali liquor into the oil when the temperature of the oil reaches 35 ℃ and the temperature of the alkali liquor is close to 40 ℃, and fully stirring.
5. Adding old mature vinegar and vinegar residue powder which is crushed by a crusher and then sieved by a 80-mesh sieve when the soap solution is nearly thick, and continuously stirring until the soap solution and the mature vinegar are uniformly mixed.
6. Slowly pouring the soap liquid added with the mature vinegar into a clean mould for several times, and standing for solidification.
7. And placing the soap after being molded into a constant temperature incubator at 25 ℃ for heat preservation for 24 hours.
8. The soap after the heat preservation was left at room temperature for 1 day, and then taken out of the mold.
9. The soap taken out is placed in a dry and ventilated room, and is used after being saponified for 90 days.
Example 2
The cold soap made of vinegar residue and mature vinegar specifically comprises the following raw materials in percentage by mass: 20% of cold-pressed olive oil, 10% of avocado oil, 10% of hazelnut oil, 8% of coconut oil, 5% of palm oil, 5% of shea butter, 6% of grape seed oil, 15% of distilled water, 8% of mature vinegar with 5-degree total acid, 9% of caustic soda and 2% of vinegar residue powder.
The mature vinegar is vinegar prepared by fermenting sorghum, barley, pea, bran and bran coat in solid state and aging for 5 years.
The vinegar residue powder is prepared by performing enzymolysis on vinegar residues after vinegar spraying, drying and crushing, wherein the enzymolysis is to perform enzymolysis on the vinegar residues by adding cellulase and beta-mannase, so that the content of soluble cellulose in the vinegar residues is 30%, and the content of insoluble solids is 55%.
The preparation method of the vinegar residue cold soap comprises the following specific steps:
preparing vinegar residue powder: taking vinegar residue after vinegar pouring, crushing to 40 meshes, adding cellulase and beta-mannase which are 0.5 percent and 0.5 percent of the weight of the vinegar residue, adding distilled water which is 10 percent, carrying out enzymolysis, drying after the enzymolysis, and crushing to 80 meshes. The enzymolysis temperature is 30 ℃, and the enzymolysis time is 8 h.
1. Weighing cold-pressed olive oil, avocado oil, hazelnut oil, coconut oil, palm oil, shea butter and grape seed oil according to a formula, wherein each oil is weighed twice, so that each oil is accurately weighed.
2. Caustic soda is accurately weighed, and the remaining distilled water is poured into the caustic soda to be sufficiently dissolved and cooled to room temperature.
3. Mixing the weighed grease, and dissolving the mixture on a small fire.
4. Heating the mixed oil and the dissolved alkali liquor, slowly adding the alkali liquor into the oil when the temperature of the oil reaches 35 ℃ and the temperature of the alkali liquor is close to 40 ℃, and fully stirring.
5. Adding old mature vinegar and vinegar residue powder which is crushed by a crusher and then sieved by a 80-mesh sieve when the soap solution is nearly thick, and continuously stirring until the soap solution and the mature vinegar are uniformly mixed.
6. Slowly pouring the soap liquid added with the mature vinegar into a clean mould for several times, and standing for solidification.
7. And placing the soap after being molded into a constant temperature incubator at 25 ℃ for heat preservation for 24 hours.
8. The soap after the heat preservation was left at room temperature for 2 days, and then taken out of the mold.
9. The soap taken out is placed in a dry and ventilated room, and the soap can be used after being saponified for 70 days.
Example 3
The cold soap made of vinegar residue and mature vinegar specifically comprises the following raw materials in percentage by mass: 21% of cold-pressed olive oil, 8% of avocado oil, 8% of hazelnut oil, 9% of coconut oil, 8% of palm oil, 7% of shea butter, 5% of grape seed oil, 15% of distilled water, 8% of mature vinegar with 6-degree total acid, 9% of caustic soda and 2% of vinegar residue powder.
The mature vinegar is vinegar prepared by fermenting sorghum, barley, pea, bran and bran coat in solid state and aging for 5 years.
The vinegar residue powder is prepared by performing enzymolysis on vinegar residues after vinegar spraying, drying and crushing, wherein the enzymolysis is to perform enzymolysis on the vinegar residues by adding cellulase and beta-mannase, so that the content of soluble cellulose in the vinegar residues is 30%, and the content of insoluble solids is 55%.
The preparation method of the vinegar residue cold soap comprises the following specific steps:
preparing vinegar residue powder: taking vinegar residue after vinegar pouring, crushing to 40 meshes, adding cellulase accounting for 0.8 percent of the weight of the vinegar residue and beta-mannase accounting for 0.5 percent of the weight of the vinegar residue, adding distilled water accounting for 10 percent of the weight of the vinegar residue, carrying out enzymolysis, drying after the enzymolysis, and crushing to 80 meshes. The enzymolysis temperature is 30 ℃, and the enzymolysis time is 8 h.
1. Weighing cold-pressed olive oil, avocado oil, hazelnut oil, coconut oil, palm oil, shea butter and grape seed oil according to a formula, wherein each oil is weighed twice, so that each oil is accurately weighed.
2. Caustic soda is accurately weighed, and the remaining distilled water is poured into the caustic soda to be sufficiently dissolved and cooled to room temperature.
3. Mixing the weighed grease, and dissolving the mixture on a small fire.
4. Heating the mixed oil and the dissolved alkali liquor, slowly adding the alkali liquor into the oil when the temperature of the oil reaches 35 ℃ and the temperature of the alkali liquor is close to 40 ℃, and fully stirring.
5. Adding old mature vinegar and vinegar residue powder which is crushed by a crusher and then sieved by a 80-mesh sieve when the soap solution is nearly thick, and continuously stirring until the soap solution and the mature vinegar are uniformly mixed.
6. Slowly pouring the soap liquid added with the mature vinegar into a clean mould for several times, and standing for solidification.
7. And placing the soap after being molded into a constant temperature incubator at 25 ℃ for heat preservation for 24 hours.
8. The soap after the heat preservation was left at room temperature for 2 days, and then taken out of the mold.
9. The soap taken out is placed in a dry and ventilated room, and the soap can be used after being saponified for 70 days.
The above description is provided for further details of the present invention with reference to specific preferred embodiments, which should not be construed as limiting the present invention, and all soap products produced by brewing vinegar or vinegar residue from food are within the technical scope of the present invention. Numerous and varied other arrangements can be devised by those skilled in the art without departing from the invention, and it is intended that the present invention cover all modifications and equivalents of the embodiments disclosed and claimed herein as fall within the scope of the appended claims.
Claims (4)
1. The preparation method of the cold soap of vinegar residue aged mature vinegar is characterized by comprising the following raw materials in percentage by mass: 17% -21% of cold-pressed olive oil, 8% -10% of avocado oil, 7% -11% of hazelnut oil, 8% -10% of coconut oil, 5% -8% of palm oil, 5% -8% of shea butter, 2% -6% of grape seed oil, 15% -19% of distilled water, 8% -10% of mature vinegar, 7% -11% of caustic soda and 2% -5% of vinegar residue powder; the vinegar residue powder is prepared by performing enzymolysis on vinegar residue after vinegar spraying, drying and crushing, wherein the enzymolysis is to perform enzymolysis on the vinegar residue by adding cellulase and beta-mannase, so that the content of soluble cellulose in the vinegar residue is 25-45%, and the content of insoluble solids is 55-75%; the method comprises the following specific steps:
1) preparing vinegar residue powder: taking vinegar residue after vinegar leaching, pulverizing to 20-50 mesh, adding cellulase 0.5-1.5% of the weight of the vinegar residue and beta-mannase 0.2-0.8% of the weight of the vinegar residue for enzymolysis, drying after enzymolysis, and pulverizing to 80-100 mesh;
2) dissolving oil and alkali liquor, and mixing the oil and the alkali liquor to prepare soap liquid;
3) adding the aged vinegar and the vinegar residue powder when the soap solution is nearly thick, and continuously stirring until the mixture is uniformly mixed;
4) coagulating and saponifying.
2. The method for preparing the cold soap of vinegar residue mature vinegar as claimed in claim 1, wherein the enzymolysis temperature is 25-35 ℃, and the enzymolysis time is 8-12 h.
3. The method for preparing the cold soap of vinegar residue and mature vinegar as claimed in claim 1, wherein the alkali solution is prepared by pouring water into caustic soda to dissolve fully and cooling to room temperature.
4. The method for preparing the cold soap of vinegar residue and mature vinegar as claimed in claim 1, wherein the solidification and saponification is to gradually pour the uniformly mixed soap liquid into a clean mold, and to let the mold stand for solidification; placing the soap after being molded into a constant temperature incubator at 25 ℃ for heat preservation for 24 hours; placing the heat-preserved soap at room temperature for 1-2 days, and taking out the soap from the mold; placing the taken-out soap in a dry and ventilated room, and saponifying for 60-90 days to obtain the soap.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010060221.3A CN111139152B (en) | 2020-01-19 | 2020-01-19 | Vinegar residue mature vinegar cold-made soap and preparation method thereof |
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| CN202010060221.3A CN111139152B (en) | 2020-01-19 | 2020-01-19 | Vinegar residue mature vinegar cold-made soap and preparation method thereof |
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| CN111139152A CN111139152A (en) | 2020-05-12 |
| CN111139152B true CN111139152B (en) | 2021-02-26 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883957A (en) * | 2017-04-17 | 2017-06-23 | 帝善圆农业科技（苏州）有限公司 | A kind of soap and preparation method thereof |
| CN107440998A (en) * | 2017-09-06 | 2017-12-08 | 山西大学 | Application of the Shanxi mature vinegar extract in nti-freckle, skin-lightening cosmetic is prepared |
| CN109694787A (en) * | 2018-12-07 | 2019-04-30 | 西北农林科技大学 | A kind of precipitate handmade soap and preparation method thereof |
| CN110194998A (en) * | 2019-07-03 | 2019-09-03 | 河南牧业经济学院 | Natural plants craft cold process soap and preparation method thereof |
-
2020
- 2020-01-19 CN CN202010060221.3A patent/CN111139152B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883957A (en) * | 2017-04-17 | 2017-06-23 | 帝善圆农业科技（苏州）有限公司 | A kind of soap and preparation method thereof |
| CN107440998A (en) * | 2017-09-06 | 2017-12-08 | 山西大学 | Application of the Shanxi mature vinegar extract in nti-freckle, skin-lightening cosmetic is prepared |
| CN109694787A (en) * | 2018-12-07 | 2019-04-30 | 西北农林科技大学 | A kind of precipitate handmade soap and preparation method thereof |
| CN110194998A (en) * | 2019-07-03 | 2019-09-03 | 河南牧业经济学院 | Natural plants craft cold process soap and preparation method thereof |
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| CN111139152A (en) | 2020-05-12 |
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