CN105238598A - Natural enzyme handmade soap and preparation method thereof - Google Patents
Natural enzyme handmade soap and preparation method thereof Download PDFInfo
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- CN105238598A CN105238598A CN201510767218.4A CN201510767218A CN105238598A CN 105238598 A CN105238598 A CN 105238598A CN 201510767218 A CN201510767218 A CN 201510767218A CN 105238598 A CN105238598 A CN 105238598A
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- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 76
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
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- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 229920000832 Cutin Polymers 0.000 description 2
- 102000004882 Lipase Human genes 0.000 description 2
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- 108090001060 Lipase Proteins 0.000 description 2
- 108091005804 Peptidases Proteins 0.000 description 2
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- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
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- 206010039792 Seborrhoea Diseases 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
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- 239000003208 petroleum Substances 0.000 description 1
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- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 description 1
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- 239000003351 stiffener Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
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Landscapes
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to natural enzyme handmade soap and a preparation method thereof. The soap is prepared from, by weight, 20-50% of olive oil, 10-30% of coconut oil, 10-30% of palm oil, 5-11% of sodium hydroxide, 0.1-4% of honey, 8-30% of enzymes and 4.5-15% of water. The soap is natural, environmentally friendly, free of harm to skin and free of damage to new cells and has effects on cleaning skin, preventing whelks and resisting aging.
Description
Technical field
The present invention relates to a kind of natural ferment handmade soap and preparation method thereof, belong to washing of daily necessities field.
Background technology
Perfumed soap is on the market cheap large again, because they are all much produce in enormous quantities, the glycerine needed most by skin detaches, and adds some and does not have helpful chemical to our skin.As added pore forming material, plaing and increasing bubble effect; Add stiffening agent, in order to more durable, not easily soft rotten; Adding preservative agent, extends the shelf-time, makes the shelf-time can reach 3 or five years.Synthesis soap on existing market, only meeting let us skin worse and worse, does not more and more have protection.The skin surface of human body has one deck sebum film, and this layer of sebum film is into weakly acidic.Perfumed soap on existing market is all alkaline, and life-time service can destroy the acid base equilibrium of skin, destroys sebum film.Perfumed soap remains on skin, and skin because being in alkaline state, will cause skin roughen gradually.
Chinese patent literature CN102329703A (application number: 201110244705.4) disclose a kind of Antibacterial soaps, it is characterized in that, the feed composition making perfumed soap comprises: Oleum Cocois: 5-15%, plam oil: 10-20%, sweet oil: 3-10%, butter: 15-30%, sodium hydroxide: 5-15%, licorice water extract: 2-8%, Sodium dodecylbenzene sulfonate: 1-3% and titanium dioxide: 3-8%.The Antibacterial soaps that the present invention obtains can be directly used in skin, effectively removes and kill the bacterium on human body skin, and energy is anti-Staphylococcus aureus, Pseudomonas aeruginosa, intestinal bacteria and Candida albicans simultaneously.This Antibacterial soaps adopts Sodium dodecylbenzene sulfonate, a large amount of tetrapropylenes can be converted into dodecylbenzene by petroleum chemicals company, quality product is high, cheap, therefore be that the washing composition of raw material instead of soap rapidly with dodecylbenzene, and Sodium dodecylbenzene sulfonate just becomes the maximum organic surface active agent of consumption very soon, although the tensio-active agent kind application performance now used is good, but the shortcoming that ubiquity one is serious, that their biodegradation rates in waste disposal plant are very low, and degraded not exclusively, very large pollution is caused to environment.
Chinese patent literature 103589537A (application number: 201310577658.4) disclose a kind of beauty treatment antibacterial toilet soap, the feed composition of this perfumed soap comprises: Oleum Cocois 10-13%, plam oil 20-23%, sweet oil 21-38.3%, sodium hydroxide 8.5-9%, water 20-23%, bighead atractylodes rhizome decocting liquid 1-3%, the ultrasonic alcohol extract 1-3% of the root of Dahurain angelica, Radix Asparagi decocting liquid 1-3%, tea tree ethereal oil 0.2-2%.Perfumed soap of the present invention not only can cleaning skin, more can antibacterial, nti-freckle, anti-acne and whitening, keeps the lubrication of skin and in vain tender.The handmade soap ph value that this formula is made about 8, should belong to alkalescence, is relatively applicable to oily skin.Obvious pungency is had to other skins.
Summary of the invention
For the deficiencies in the prior art, a kind of natural ferment handmade soap of the present invention and preparation method thereof, this natural ferment handmade soap raw material all adopts and comes from crude substance extraction refinement grinding, is easy to occurring in nature and is decomposed, noresidue, free of a burden to human body.
Technical scheme of the present invention is as follows:
A kind of natural ferment handmade soap, feed composition and weight percent composed as follows:
Sweet oil 20 ~ 50%, Oleum Cocois 10 ~ 30%, plam oil 10 ~ 30%, sodium hydroxide 5 ~ 11%, honey 0.1 ~ 4%, ferment 8 ~ 30%, water 4.5 ~ 15%,
Each weight percentages of components sum is 100%.
The present invention is preferred, described ferment obtains as follows, by fruit, honey and water according to the mixing of 1:3:10 mass ratio, obtained mixture, puts into container by mixture, the add-on of mixture is less than or equal to 80% of container volume, sealing, leaves standstill, is placed on shady and cool ventilation place and leaves standstill the 5-7 month, removing solids, gained filtrate is ferment.
Preferred further, described fruit is apple, lemon, pineapple, blueberry, without the need to peeling, directly cleans up.
Preferred according to the present invention, described honey is Mel Jujubae.
The present invention is preferred, described natural ferment handmade soap, feed composition and weight percent composed as follows:
Sweet oil 20 ~ 42%, Oleum Cocois 12 ~ 28%, plam oil 12 ~ 15%, sodium hydroxide 5 ~ 14%, honey 0.1 ~ 4%, ferment 18 ~ 22%, water 6.8 ~ 11%.
The highly preferred scheme of the present invention, described natural ferment handmade soap, feed composition and weight percent composed as follows:
Sweet oil 40%, Oleum Cocois 15%, plam oil 13%, sodium hydroxide 3%, honey 0.2%, ferment 20%, water 8.8%.
The preparation method of above-mentioned natural ferment handmade soap, step is as follows:
1) by sweet oil, Oleum Cocois, plam oil, mixing post-heating to 40-50 degree, keep 20 minutes, obtained basic grease, mixes sodium hydroxide with water, obtains alkali lye,
2) basic grease is mixed with alkali lye, stirring at room temperature 10-30 minute, add honey by clockwise mixing direction and continue to stir 10-20 minute; Then add ferment by clockwise mixing direction, continue to stir 3-8 minute; Mold forming is entered, cooling by clockwise mixing direction; After 24 hours, the demoulding; Saponification 50 days, ph value stabilization, at 7-8, obtains natural ferment handmade soap.
The present invention is preferred, and the stirring in above-mentioned steps (2) hastens as 100-200rpm.
Following table 1 is saponification value and the INS value of various vegetative grease.Use when wherein NaOH makes cold soap, use when KOH makes liquid soap, and INS value instruction handmade soap hardness, value is lower shows soap softer (INS value is more appropriate between 120 ~ 160).
Calculation formula:
Single oil product:
The quality of the weight × saponification value=required NaOH of grease
The INS value of the ratio × INS value=soap soap of grease
Oil products:
The saponification value of the saponification value+B oil quality × B of A oil quality × A+... the quality of=total NaOH for needing
The INS value of the INS value+B oil ratio example × B of A oil ratio example × A+...=handmade soap INS value
Table 1
| The oily name of Chinese | NaOH value | INS |
| Oleum Cocois | 0.19 | 258 |
| Sweet oil | 0.134 | 109 |
| Plam oil | 0.141 | 145 |
In table 1, each vegetable oil is different with the hardness of the soap of the generation after alkali reaction, and the vegetables oil of different ratios participates in reaction, finally forms the handmade soap that hardness is applicable to.
Natural ferment handmade soap formula of the present invention is through oil (natural plant grease)+alkali (water-soluble sodium hydroxide)=soap+natural glycerin, typical saponification reaction and obtaining, add more than 40 days cool time processed, make its sufficient saponification, reach alkali-free and remain.The interpolation of natural ferment, thus make its pH value more stable.
Natural ferment handmade soap formula of the present invention is through that numerous experiments obtains, and makes that the handmade soap that obtains is natural, environmental protection, to skin fanout free region, can not injure new viable cell again, thus play cleaning skin, prevention comedo and antidotal effect.Cellulose solution belongs to acid, and it can neutralize the residue alkali in handmade soap, makes to which reduce pungency.And it optionally can carry out proteolysis to skin, dissolve the useless aged cells of removing simultaneously, new viable cell can not be injured again, thus play cleaning skin, prevention comedo and antidotal effect.
The present invention obtains the every batch products of natural ferment handmade soap in strict accordance with QB/T2485-2008 standard, inspects by random samples.Without waste water in the course of processing, waste gas, industrial refuse produces, and belongs to environmental protection industry.
The present invention's excellent results compared with existing routine techniques is as follows:
1. pair skin fanout free region: in handmade soap making processes, spontaneous byproduct glycerine is real useful skin, containing abundant moisturizing composition, being the most original also the most moist, bearing skin zero, is good selection to there being the people of allergic skin.A large amount of soaps that commercially available chemical plant produces can be separated soap and glycerine, and the glycerine gone out of extraction is then as the additive of makeup.
2. natural: handmade soap be natural formula, all making processes and byproduct do not pollute the environment.Commercially available soap, containing chemical foamer, active interface agent, is bragged about and can be put 3 years, certainly also will descend sanitas.And the vitamin b6 usp e of the natural anti-oxidation that handmade soap uses, the natural compositions such as quality plant oil, ferment cannot remain so long certainly.
3. plasticity-is strong: can make one piece of exclusive soap of individual according to the fragrance moulding of individual's skin situation hobby.
4. environmental protection: the pollution problem that can not cause river, lake and water channel.So the earth protecting us unique, soap is also very noble reason by hand.
5, one of the principle of ferment beautifying skin is the aged cells digest and decompose in skin to accelerate its process that comes off normally.Its effect is gentleer than tartaric acid effectively both can remove grease by cleaning skin, eliminated comedo, desalination wrinkle.Also thoroughly can improve skin condition, make its consolidation, careful, glossy.The ferment being applied to makeup for different skin problems mainly contains three kinds, protease, lipase and antioxidative enzyme (being also called SOD).Main extraction obtains from the vegetable-protein such as pineapple, pawpaw or by microbe fermentation method and culture plant cell method.
They have different effects: protease, mainly for the bad skin of cutin metabolism, because it can remove the dirt of skin surface and hair follicle, sebiferous gland, is leniently removed aging cutin, made skin recover elasticity, become smooth exquisiteness.It is usually added on clean skin product or has in the skin care product of exfoliation effect.
Lipase then mainly acts on the vigorous skin of fat secretion, by unnecessary grease on decomposition skin and then can reach effectively clean skin, the object of prevention clogging of pores.It is also be added in clean skin product usually.
Antioxidative enzyme can resist the oxidative damage that radical pair skin causes, the aging speed of delaying skin, and to starting, aging skin is effective.
Embodiment
Below in conjunction with embodiment, the present invention will be further described, do not illustrate in detail in embodiment all by state of the art.
The raw material sweet oil used in embodiment, Oleum Cocois, plam oil are currently available products, buy by market.
Embodiment 1
Natural ferment handmade soap, feed composition and weight percent composed as follows:
Sweet oil 40%, Oleum Cocois 15%, plam oil 13%, sodium hydroxide 3%, honey 0.2%, ferment 20%, water 8.8%.
Preparation method, step is as follows:
1) by sweet oil, Oleum Cocois, plam oil, mixing post-heating to 45 degree, keep 20 minutes, obtained basic grease, mixes sodium hydroxide with water, obtained alkali lye,
2) basic grease is mixed with alkali lye, to hasten stirring at room temperature 20 minutes with the stirring of 120rpm, add honey by clockwise mixing direction and continue to hasten stirring 15 minutes with the stirring of 120rpm; Then add ferment by clockwise mixing direction, continue to hasten stirring 5 minutes with the stirring of 120rpm; Mold forming is entered, cooling by clockwise mixing direction; After 24 hours, the demoulding; Saponification 50 days, ph value stabilization, 7.2, obtains natural ferment handmade soap.
The Manual perfumed soap that the present invention obtains is different from chemical cleaner, after contact with water after about 24 hours, can be bacterially decomposed into water and carbonic acid gas.To rivers and creeks or sea water body, the pollution of environment can not be caused, also can not threaten to marine organisms.Liquid pouring bracketplant after ferment handmade soap of the present invention is washed one's hands, through 20-90 days, bracketplant is well-grown still, and the liquid pouring bracketplant after washing one's hands with commercial handmade soap, through 30 days, bracketplant jaundice was withered.
Embodiment 2
Natural ferment handmade soap, feed composition and weight percent composed as follows:
Sweet oil 20%, Oleum Cocois 25%, plam oil 15%, sodium hydroxide 10%, honey 2%, ferment 18%, water 10%.
Preparation method, step is as follows:
1) by sweet oil, Oleum Cocois, plam oil, mixing post-heating to 48 degree, keep 20 minutes, obtained basic grease, mixes sodium hydroxide with water, obtained alkali lye,
2) basic grease is mixed with alkali lye, to hasten stirring at room temperature 25 minutes with the stirring of 120rpm, add honey by clockwise mixing direction and continue to hasten stirring 12 minutes with the stirring of 120rpm; Then add ferment by clockwise mixing direction, continue to hasten stirring 4 minutes with the stirring of 120rpm; Mold forming is entered, cooling by clockwise mixing direction; After 24 hours, the demoulding; Saponification 50 days, ph value stabilization, 7.8, obtains natural ferment handmade soap.
The Manual perfumed soap that the present invention obtains is different from chemical cleaner, after contact with water after about 24 hours, can be bacterially decomposed into water and carbonic acid gas.To rivers and creeks or sea water body, the pollution of environment can not be caused, also can not threaten to marine organisms.Liquid pouring bracketplant after being washed one's hands by ferment handmade soap of the present invention, through 20-90 days, bracketplant is well-grown still.
Claims (8)
1. a natural ferment handmade soap, feed composition and weight percent composed as follows:
Sweet oil 20 ~ 50%, Oleum Cocois 10 ~ 30%, plam oil 10 ~ 30%, sodium hydroxide 5 ~ 11%, honey 0.1 ~ 4%, ferment 8 ~ 30%, water 4.5 ~ 15%,
Each weight percentages of components sum is 100%.
2. natural ferment handmade soap according to claim 1, it is characterized in that, described ferment obtains as follows, fruit, honey and water mixed according to 1:3:10 mass ratio, obtained mixture, mixture is put into container, and the add-on of mixture is less than or equal to 80% of container volume, sealing, leave standstill, be placed on shady and cool ventilation place and leave standstill the 5-7 month, removing solids, gained filtrate is ferment.
3. natural ferment handmade soap according to claim 2, is characterized in that described fruit is apple, lemon, pineapple, blueberry, without the need to peeling, directly cleans up.
4. natural ferment handmade soap according to claim 1, is characterized in that, described honey is Mel Jujubae.
5. natural ferment handmade soap according to claim 1, is characterized in that, feed composition and weight percent composed as follows:
Sweet oil 20 ~ 42%, Oleum Cocois 12 ~ 28%, plam oil 12 ~ 15%, sodium hydroxide 5 ~ 14%, honey 0.1 ~ 4%, ferment 18 ~ 22%, water 6.8 ~ 11%.
6. natural ferment handmade soap according to claim 1, is characterized in that, feed composition and weight percent composed as follows:
Sweet oil 40%, Oleum Cocois 15%, plam oil 13%, sodium hydroxide 3%, honey 0.2%, ferment 20%, water 8.8%.
7. the preparation method of natural ferment handmade soap according to claim 1, step is as follows:
1) by sweet oil, Oleum Cocois, plam oil, mixing post-heating to 40-50 degree, keep 20 minutes, obtained basic grease, mixes sodium hydroxide with water, obtains alkali lye,
2) basic grease is mixed with alkali lye, stirring at room temperature 10-30 minute, add honey by clockwise mixing direction and continue to stir 10-20 minute; Then add ferment by clockwise mixing direction, continue to stir 3-8 minute; Mold forming is entered, cooling by clockwise mixing direction; After 24 hours, the demoulding; Saponification 50 days, ph value stabilization, at 7-8, obtains natural ferment handmade soap.
8. the preparation method of natural ferment handmade soap according to claim 8, is characterized in that, the stirring in step (2) hastens as 100-200rpm.
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105524722A (en) * | 2016-02-03 | 2016-04-27 | 云南人本生物科技有限公司 | Dish detergent and preparation method thereof |
| CN105567480A (en) * | 2016-02-25 | 2016-05-11 | 青岛洁百氏科技有限公司 | Enzyme soap and preparation method thereof |
| CN105623908A (en) * | 2016-02-03 | 2016-06-01 | 云南人本生物科技有限公司 | Mild pollution-free multifunctional enzyme detergent preparation method |
| CN105754756A (en) * | 2016-02-03 | 2016-07-13 | 云南人本生物科技有限公司 | Preparation method of gentle and non-pollution enzyme laundry detergent |
| CN106047539A (en) * | 2016-06-29 | 2016-10-26 | 广州白云巨星家用品厂 | Camellia seed handmade soap and preparation method thereof |
| CN106398920A (en) * | 2016-08-30 | 2017-02-15 | 张艳 | Multipurpose ferment soap and manufacturing method thereof |
| CN106701350A (en) * | 2017-02-20 | 2017-05-24 | 国莓生物科技河北股份有限公司 | Multifunctional blueberry enzyme laundry detergent |
| CN107815366A (en) * | 2017-11-09 | 2018-03-20 | 骆志明 | Anti-acne ferment is washed one's face manual liquid soap |
| CN107904050A (en) * | 2017-11-08 | 2018-04-13 | 骆志明 | Moisturizing whitening ferment face cleaning craft liquid soap |
| CN107904052A (en) * | 2017-11-09 | 2018-04-13 | 骆志明 | Preserve youthful looks nti-freckle ferment craft liquid soap |
| CN108395948A (en) * | 2018-03-21 | 2018-08-14 | 桂林良物造日用品有限公司 | A kind of diatomite soap and preparation method thereof |
| CN108926497A (en) * | 2018-08-22 | 2018-12-04 | 海南师范大学 | A kind of profit hair black hair hair soap and preparation method thereof |
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| CN112812903A (en) * | 2021-01-29 | 2021-05-18 | 董林 | Cold-made soap and preparation method thereof |
| CN116987558A (en) * | 2023-08-01 | 2023-11-03 | 云南善源生物科技发展有限公司 | Handmade soap with acne removing effect and preparation method thereof |
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| CN105524722A (en) * | 2016-02-03 | 2016-04-27 | 云南人本生物科技有限公司 | Dish detergent and preparation method thereof |
| CN105623908A (en) * | 2016-02-03 | 2016-06-01 | 云南人本生物科技有限公司 | Mild pollution-free multifunctional enzyme detergent preparation method |
| CN105754756A (en) * | 2016-02-03 | 2016-07-13 | 云南人本生物科技有限公司 | Preparation method of gentle and non-pollution enzyme laundry detergent |
| CN105567480A (en) * | 2016-02-25 | 2016-05-11 | 青岛洁百氏科技有限公司 | Enzyme soap and preparation method thereof |
| CN106047539A (en) * | 2016-06-29 | 2016-10-26 | 广州白云巨星家用品厂 | Camellia seed handmade soap and preparation method thereof |
| CN106398920A (en) * | 2016-08-30 | 2017-02-15 | 张艳 | Multipurpose ferment soap and manufacturing method thereof |
| CN106701350A (en) * | 2017-02-20 | 2017-05-24 | 国莓生物科技河北股份有限公司 | Multifunctional blueberry enzyme laundry detergent |
| CN106701350B (en) * | 2017-02-20 | 2018-08-14 | 国莓生物科技河北股份有限公司 | A kind of multi-functional blueberry ferment laundry dew |
| CN107904050A (en) * | 2017-11-08 | 2018-04-13 | 骆志明 | Moisturizing whitening ferment face cleaning craft liquid soap |
| CN107904052A (en) * | 2017-11-09 | 2018-04-13 | 骆志明 | Preserve youthful looks nti-freckle ferment craft liquid soap |
| CN107815366A (en) * | 2017-11-09 | 2018-03-20 | 骆志明 | Anti-acne ferment is washed one's face manual liquid soap |
| CN108395948A (en) * | 2018-03-21 | 2018-08-14 | 桂林良物造日用品有限公司 | A kind of diatomite soap and preparation method thereof |
| CN108926497A (en) * | 2018-08-22 | 2018-12-04 | 海南师范大学 | A kind of profit hair black hair hair soap and preparation method thereof |
| CN109055055A (en) * | 2018-10-12 | 2018-12-21 | 合肥师范学院 | Environmental protection ferment soap and preparation method thereof |
| CN112812903A (en) * | 2021-01-29 | 2021-05-18 | 董林 | Cold-made soap and preparation method thereof |
| CN116987558A (en) * | 2023-08-01 | 2023-11-03 | 云南善源生物科技发展有限公司 | Handmade soap with acne removing effect and preparation method thereof |
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