CN109694787A - A kind of precipitate handmade soap and preparation method thereof - Google Patents

A kind of precipitate handmade soap and preparation method thereof Download PDF

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Publication number
CN109694787A
CN109694787A CN201811493578.XA CN201811493578A CN109694787A CN 109694787 A CN109694787 A CN 109694787A CN 201811493578 A CN201811493578 A CN 201811493578A CN 109694787 A CN109694787 A CN 109694787A
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China
Prior art keywords
parts
wine mud
heated
preparation
wine
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CN201811493578.XA
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房玉林
何爽
王皆行
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Northwest A&F University
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Northwest A&F University
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Priority to CN201811493578.XA priority Critical patent/CN109694787A/en
Publication of CN109694787A publication Critical patent/CN109694787A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)

Abstract

The present invention relates to wash shield technical field, and in particular to a kind of precipitate handmade soap and preparation method thereof.It has the function of anti-oxidant, anti-aging.Wine mud handmade soap of the present invention includes following raw material: 330-340 parts of olive oil, 130-135 parts of coconut oil, 80-90 parts of shea butter, 60-70 parts of Sweet Almond Oil, 60-70 parts of cocoa butter, 92-95 parts of sodium hydroxide, 140-145 parts of pure water, it 140-150 parts of wine mud, 5-10 parts of sodium lactate, is prepared using certain preparation method.

Description

A kind of precipitate handmade soap and preparation method thereof
Technical field
The present invention relates to wash shield technical field, and in particular to a kind of precipitate handmade soap and preparation method thereof.
Background technique
Wine mud is in wine production, and after fermentation, the sediment or residue obtained during storage and after filtering is main It to be made of dead saccharomycete and a small amount of tartaric acid and inorganic matter.
The a large amount of wine muds generated in the process of grape wine, are largely taken as feed or Fertilizer application, more have It is arbitrarily discharged and leads to environmental pollution.
At present for the development and utilization of grape wine wine mud, washing, shield technical field is at the early-stage, a variety of nutrition in wine mud Substance has been to be concerned by more and more people, a variety of phenols being rich in precipitate and polysaccharide etc..
It yet there are no the report that handmade soap is prepared using wine mud as primary raw material.
Summary of the invention
In view of this, the present invention provides a kind of precipitate handmade soap, has the function of anti-oxidant, anti-aging.
In order to solve the problems existing in the prior art, the technical scheme is that a kind of precipitate handmade soap, feature It is: including following raw material: 330-340 parts of olive oil, 130-135 parts of coconut oil, 80-90 parts of shea butter, sweet tea apricot 60-70 parts of benevolence oil, 60-70 parts of cocoa butter, 92-95 parts of sodium hydroxide, 140-145 parts of pure water, 140-150 parts of wine mud, lactic acid 5-10 parts of sodium.
A kind of precipitate handmade soap the preparation method comprises the following steps:
Coconut oil, shea butter, cocoa butter are put in water proof in 70~80 DEG C of hot water and are heated to liquid, it is cooled to 45~ 50 DEG C spare;
By olive oil, Sweet Almond Oil water proof is heated to 45~50 DEG C, and the coconut oil, shea butter, cocoa butter of thawing is added, Part A is obtained, keeps temperature spare;
Sodium hydroxide is added into pure water, stirs evenly, is cooled to 45 DEG C, sodium lactate is added, is stirred for uniformly, obtaining B Part keeps temperature spare;
By wine mud water proof be heated to 45 DEG C it is spare, obtain C portion;
Part B is slowly imported in part A, and is at the uniform velocity stirred 30-45 minutes, until soap lye is in thick state, it can be in soap lye Surface is marked clear trace holding 5 seconds or more, and wine mud is added and continues stirring 5 minutes, pours into mold, places 48 hours under room temperature After can demould cutting, after 4-6 weeks i.e. can be used.
The wine mud the preparation method comprises the following steps:
Grape vinasse after fermentation is stood 24 hours, extracts supernatant liquor discharge;
It takes wine mud to cross 80 meshes, is heated 30 minutes as water proof in 60 DEG C of hot water;
It is placed in subzero 20 DEG C of refrigerator stored frozens, it is 45 DEG C i.e. usable that wine mud water proof is heated to wine mud by when use.With The prior art is compared, and advantages of the present invention is as follows:
Wine mud handmade soap of the present invention is mainly used for cleaning face, keeps wet after having cleaning, a variety of natural anti-reflecting oxides Matter nourishes rough skin enhances the anti-oxidant and anti-aging ability of skin;
Wine mud ingredient accounting is high in inventive formulation, usually cold using that can reduce while wine mud since wine mud is liquid The use of moisture in handmade soap processed, makes soap lye faster reach thick state, and reduces the demoulding required time;
Wine mud is natural anti-oxidation anti-aging substance in inventive formulation, and it is such as more to contain a large amount of active material in wine mud Sugar, polyphenol, pectin, flavonoids, resveratrol etc., these substances have the function of anti-oxidant, anti-aging;Wine mud is stirred in soap lye It is added after mixing 30 minutes, destruction of the soap lye for effective component in wine mud can be reduced, so that wine mud is more stable in handmade soap, Conducive to saving and use.
Grease is 100% crude vegetal in inventive formulation, and the temperature of soapmaking is lower than 60 DEG C, far below industrial soapmaking Temperature.This technique helps utmostly to protect the anti-oxidant nutriments such as the polysaccharide in wine mud.It is natural by saponification It is condensed into soap, it is slow at the soap time.Wine mud handmade soap does not stimulate skin mildly, and pro-skin moisturizing effect is strong, and long-time service can be pre- Prevent and improves a variety of skin problems.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.
The special efficacy of each ingredient in the present invention:
Olive oil is gentle, and Cheng Zaohou foam is fine and smooth, is suitable as the basic oil of handmade soap;
Coconut oil is higher at hardness after soap, and stability is good, while can increase foam volume, enhances cleaning capacity;
Shea butter moisture-retaining capacity is strong, and can accelerate the thick speed of soap lye;
Sweet Almond Oil skin care and moisture-keeping functions are good;
Cocoa butter quality is more hard, can increase soap body hardness.
Embodiment one:
A kind of precipitate handmade soap includes following raw material: 333 parts of olive oil, 133 parts of coconut oil, and shea butter 80 parts, 60 parts of Sweet Almond Oil, 65 parts of cocoa butter, 95 parts of sodium hydroxide, 140 parts of pure water, the wine mud 150 of Cabernet Sauvignon red wine Part, 10 parts of sodium lactate.
A kind of preparation method of precipitate handmade soap:
Load weighted coconut oil, shea butter, cocoa butter are put in water proof in 70~80 DEG C of hot water and are heated to liquid, is dropped Temperature to 45~50 DEG C it is spare.
By load weighted olive oil, Sweet Almond Oil water proof is heated to 45~50 DEG C, and the wooden fruit of coconut oil, cream of thawing is added Oil, cocoa butter obtain part A, keep temperature spare.
Sodium hydroxide is added into pure water, stirs evenly, is cooled to 45 DEG C, sodium lactate is added, is stirred for uniformly, obtaining B Part keeps temperature spare.
By the wine mud water proof of Cabernet Sauvignon red wine be heated to 45 DEG C it is spare, obtain C portion.
Part B is slowly imported in part A, and is at the uniform velocity stirred 30-45 minutes, until soap lye is in thick state, it can be in soap lye Surface is marked clear trace holding 5 seconds or more, and wine mud is added and continues stirring 5 minutes, pours into mold.It is placed 48 hours under room temperature After can demould cutting, after 4-6 weeks i.e. can be used.
The wine mud the preparation method comprises the following steps:
Grape vinasse after fermentation is stood 24 hours, extracts supernatant liquor discharge;
It takes wine mud to cross 80 meshes, is heated 30 minutes as water proof in 60 DEG C of hot water;
It is placed in subzero 20 DEG C of refrigerator stored frozens, it is 45 DEG C i.e. usable that wine mud water proof is heated to wine mud by when use.
Embodiment two:
A kind of precipitate handmade soap includes following raw material: 330 parts of olive oil, 130 parts of coconut oil, and shea butter 80 parts, 60 parts of Sweet Almond Oil, 60 parts of cocoa butter, 92 parts of sodium hydroxide, 140 parts of pure water, the wine mud of rose fragrant dry white wine 140 parts, 5 parts of sodium lactate.
A kind of preparation method of precipitate handmade soap:
Load weighted coconut oil, shea butter, cocoa butter are put in water proof in 70~80 DEG C of hot water and are heated to liquid, is dropped Temperature to 45~50 DEG C it is spare.
By load weighted olive oil, Sweet Almond Oil water proof is heated to 45~50 DEG C, and the wooden fruit of coconut oil, cream of thawing is added Oil, cocoa butter obtain part A, keep temperature spare.
Sodium hydroxide is added into pure water, stirs evenly, is cooled to 45 DEG C, sodium lactate is added, is stirred for uniformly, obtaining B Part keeps temperature spare.
By the wine mud water proof of rose fragrant dry white wine be heated to 45 DEG C it is spare, obtain C portion.
Part B is slowly imported in part A, and is at the uniform velocity stirred 30-45 minutes, until soap lye is in thick state, it can be in soap lye Surface is marked clear trace holding 5 seconds or more, and wine mud is added and continues stirring 5 minutes, pours into mold.It is placed 48 hours under room temperature After can demould cutting, after 4-6 weeks i.e. can be used.
The wine mud the preparation method comprises the following steps:
Grape vinasse after fermentation is stood 24 hours, extracts supernatant liquor discharge;
It takes wine mud to cross 80 meshes, is heated 30 minutes as water proof in 60 DEG C of hot water;
It is placed in subzero 20 DEG C of refrigerator stored frozens, it is 45 DEG C i.e. usable that wine mud water proof is heated to wine mud by when use.
Embodiment three:
A kind of precipitate handmade soap includes following raw material: 340 parts of olive oil, 135 parts of coconut oil, and shea butter 90 parts, 70 parts of Sweet Almond Oil, 70 parts of cocoa butter, 95 parts of sodium hydroxide, 145 parts of pure water, the wine mud 150 of Cabernet Sauvignon red wine Part, 10 parts of sodium lactate.
A kind of preparation method of precipitate handmade soap:
Load weighted coconut oil, shea butter, cocoa butter are put in water proof in 70~80 DEG C of hot water and are heated to liquid, is dropped Temperature to 45~50 DEG C it is spare.
By load weighted olive oil, Sweet Almond Oil water proof is heated to 45~50 DEG C, and the wooden fruit of coconut oil, cream of thawing is added Oil, cocoa butter obtain part A, keep temperature spare.
Sodium hydroxide is added into pure water, stirs evenly, is cooled to 45 DEG C, sodium lactate is added, is stirred for uniformly, obtaining B Part keeps temperature spare.
By the wine mud water proof of Cabernet Sauvignon red wine be heated to 45 DEG C it is spare, obtain C portion.
Part B is slowly imported in part A, and is at the uniform velocity stirred 30-45 minutes, until soap lye is in thick state, it can be in soap lye Surface is marked clear trace holding 5 seconds or more, and wine mud is added and continues stirring 5 minutes, pours into mold.It is placed 48 hours under room temperature After can demould cutting, after 4-6 weeks i.e. can be used.
The wine mud the preparation method comprises the following steps:
Grape vinasse after fermentation is stood 24 hours, extracts supernatant liquor discharge;
It takes wine mud to cross 80 meshes, is heated 30 minutes as water proof in 60 DEG C of hot water;
It is placed in subzero 20 DEG C of refrigerator stored frozens, it is 45 DEG C i.e. usable that wine mud water proof is heated to wine mud by when use.
Example IV:
A kind of precipitate handmade soap includes following raw material: 335 parts of olive oil, 132 parts of coconut oil, and shea butter 85 parts, 65 parts of Sweet Almond Oil, 67 parts of cocoa butter, 93 parts of sodium hydroxide, 143 parts of pure water, the wine mud of rose fragrant dry white wine 148 parts, 8 parts of sodium lactate.
A kind of preparation method of precipitate handmade soap:
Load weighted coconut oil, shea butter, cocoa butter are put in water proof in 70~80 DEG C of hot water and are heated to liquid, is dropped Temperature to 45~50 DEG C it is spare.
By load weighted olive oil, Sweet Almond Oil water proof is heated to 45~50 DEG C, and the wooden fruit of coconut oil, cream of thawing is added Oil, cocoa butter obtain part A, keep temperature spare.
Sodium hydroxide is added into pure water, stirs evenly, is cooled to 45 DEG C, sodium lactate is added, is stirred for uniformly, obtaining B Part keeps temperature spare.
By the wine mud water proof of rose fragrant dry white wine be heated to 45 DEG C it is spare, obtain C portion.
Part B is slowly imported in part A, and is at the uniform velocity stirred 30-45 minutes, until soap lye is in thick state, it can be in soap lye Surface is marked clear trace holding 5 seconds or more, and wine mud is added and continues stirring 5 minutes, pours into mold.It is placed 48 hours under room temperature After can demould cutting, after 4-6 weeks i.e. can be used.
The wine mud the preparation method comprises the following steps:
Grape vinasse after fermentation is stood 24 hours, extracts supernatant liquor discharge;
It takes wine mud to cross 80 meshes, is heated 30 minutes as water proof in 60 DEG C of hot water;
It is placed in subzero 20 DEG C of refrigerator stored frozens, it is 45 DEG C i.e. usable that wine mud water proof is heated to wine mud by when use.
Ingredient wine mud in the present invention is mild to skin, can be directly used for using on skin, but directly smears wine mud and use Trouble, is not easy to operate.The effect of being fabricated to handmade soap, can be convenient effectively using wine mud to skin, is stable and easy to simultaneously Storage, waste is rationally utilized.
Handmade soap of the present invention test as follows:
1. keeping moisture of skin aptitude tests, test environment is 25 DEG C, in 30% humidity hothouse.
Test equipment is Zhongshan city than the moisture of skin tester that gloomy plastic electronic Products Co., Ltd produces, test position For the back of the hand.
Data include to repeat twice, and unit is % percentage
2. total antioxidant capacity (T-AOC) test total antioxidant capacity testing cassete is purchased from the Beijing Solarbio Suo Laibao science and technology Co., Ltd, spectrophotometer method measurement, concrete operations are as follows:
Blank tube Measurement pipe
Mixed liquor (μ L) 900μL 900μL
Sample (μ L) 30μL
Distilled water (μ L) 120μL 90μL
It mixes well, reacts 10min, distilled water zeroing, 1cm scene measures A593, calculates △ A '=A measurement-A blank Pipe.
Product oxidation resistance test result:
Group Unit
Embodiment one 86.93
Embodiment two 82.17
Embodiment three 86.31
Example IV 83.22
Note: sample total antioxidant capacity (being calculated with sample quality)=(V sample volume ÷ V sample is total by x × V reaction total volume ÷ Volume × W sample quality)=34 × x ÷ W sample quality.
Total antioxidant capacity unit are as follows: U/g fresh weight.
The contents of the present invention are not limited to cited by embodiment, and those of ordinary skill in the art are by reading description of the invention And to any equivalent replacement that technical solution of the present invention is taken, all are covered by the claims of the invention.

Claims (3)

1. a kind of precipitate handmade soap, it is characterised in that: including following raw material: 330-340 parts of olive oil, coconut oil It is 130-135 parts, 80-90 parts of shea butter, 60-70 parts of Sweet Almond Oil, 60-70 parts of cocoa butter, 92-95 parts of sodium hydroxide, pure 140-145 parts of water, 140-150 parts of wine mud, 5-10 parts of sodium lactate.
2. a kind of preparation method of precipitate handmade soap according to claim 1, it is characterised in that: the preparation side Method are as follows:
Coconut oil, shea butter, cocoa butter are put in water proof in 70 ~ 80 DEG C of hot water and are heated to liquid, be cooled to 45 ~ 50 DEG C it is standby With;
By olive oil, Sweet Almond Oil water proof is heated to 45 ~ 50 DEG C, and the coconut oil, shea butter, cocoa butter of thawing is added, obtains the portion A Point, keep temperature spare;
Sodium hydroxide is added into pure water, stirs evenly, is cooled to 45 DEG C, sodium lactate is added, is stirred for uniformly, obtaining part B, Keep temperature spare;
By wine mud water proof be heated to 45 DEG C it is spare, obtain C portion;
Part B is slowly imported in part A, and is at the uniform velocity stirred 30-45 minutes, until soap lye is in thick state, it can be on soap lye surface It marks clear trace holding 5 seconds or more, wine mud is added and continues stirring 5 minutes, pours into mold, after being placed 48 hours under room temperature i.e. Cutting can be demoulded, can be used after 4-6 weeks.
3. a kind of preparation method of precipitate handmade soap according to claim 2, it is characterised in that: the wine mud The preparation method comprises the following steps:
Grape vinasse after fermentation is stood 24 hours, extracts supernatant liquor discharge;
It takes wine mud to cross 80 meshes, is heated 30 minutes as water proof in 60 DEG C of hot water;
It is placed in subzero 20 DEG C of refrigerator stored frozens, it is 45 DEG C i.e. usable that wine mud water proof is heated to wine mud by when use.
CN201811493578.XA 2018-12-07 2018-12-07 A kind of precipitate handmade soap and preparation method thereof Pending CN109694787A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811493578.XA CN109694787A (en) 2018-12-07 2018-12-07 A kind of precipitate handmade soap and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201811493578.XA CN109694787A (en) 2018-12-07 2018-12-07 A kind of precipitate handmade soap and preparation method thereof

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Publication Number Publication Date
CN109694787A true CN109694787A (en) 2019-04-30

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111139152A (en) * 2020-01-19 2020-05-12 山西醯谷源生物科技有限公司 Vinegar residue mature vinegar cold-made soap and preparation method thereof
CN113845983A (en) * 2021-09-30 2021-12-28 宁夏职业技术学院(宁夏广播电视大学) Soap prepared from wine lees and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111139152A (en) * 2020-01-19 2020-05-12 山西醯谷源生物科技有限公司 Vinegar residue mature vinegar cold-made soap and preparation method thereof
CN111139152B (en) * 2020-01-19 2021-02-26 山西醯谷源生物科技有限公司 Vinegar residue mature vinegar cold-made soap and preparation method thereof
CN113845983A (en) * 2021-09-30 2021-12-28 宁夏职业技术学院(宁夏广播电视大学) Soap prepared from wine lees and preparation method thereof

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Application publication date: 20190430