CN105342934A - Tea tree oil no-wash sanitizer and preparation method thereof - Google Patents

Tea tree oil no-wash sanitizer and preparation method thereof Download PDF

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Publication number
CN105342934A
CN105342934A CN201510917866.3A CN201510917866A CN105342934A CN 105342934 A CN105342934 A CN 105342934A CN 201510917866 A CN201510917866 A CN 201510917866A CN 105342934 A CN105342934 A CN 105342934A
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Prior art keywords
tea tree
tree oil
preparation
oil
radix glycyrrhizae
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Chinese (zh)
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饶雅琴
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Individual
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a tea tree oil no-wash sanitizer and a preparation method thereof, relating to the field of daily use chemicals. The tea tree oil no-wash sanitizer is prepared from the following components in percentage by weight: 0.1-2 percent of benzalkonium chloride, 0.5-3 percent of coco fatty acid diethanol amide, 0.5-3 percent of lauramidopropylamine oxide, 5-10 percent of glycerinum, 1-5 percent of olive oil, 3-10 percent of vaseline, 1-5 percent of vitamin E acetic ester, 1-5 percent of chitosan, 5-15 percent of liquorice extracting solution, 1-5 percent of tea tree oil and the balance of deionized water. The preparation method comprises: 1, preparation of the liquorice extracting solution, 2, preparation of an aqueous phase, 3, preparation of an oil phase, and 4, preparation of the tea tree oil no-wash sanitizer. The tea tree oil no-wash sanitizer is good in cleaning effect and moistening type, very little in irritation and suitable for daily use.

Description

Disposable handwashing liquid of a kind of tea tree oil and preparation method thereof
Technical field
The present invention relates to a kind of handwashing liquid.
Background technology
Along with the development of society, people are to the attention of Personal hygiene, and handwashing liquid, as the succedaneum of fancy soap, comes into huge numbers of families.Because handwashing liquid is generally bottled, each discharge by pressing uses on a small quantity, and handwashing liquid seldom has secondary pollution problem.But most of handwashing liquid quality comparatively thickness of market, uses afterflush difficulty, uses a large amount of water to be also difficult to rinse well.And the handwashing liquid generally needing water to rush can not use in the absence of water, make troubles can to like this some specific occasion.
Chinese patent application (application number: 201410461023.2) disclose and carry silver-colored mesoporous silicon washing-free antibacterial hand sanitizer and preparation method thereof a kind of containing, the functional components that comprises of the disposable bacteriostatic hand sanitizer of this invention carries silver-colored mesoporous silicon, the life-time service of its heavy metal silver can cause certain injury to skin, and is not suitable for ordinary people's routine use.
Chinese patent application (application number: 201310378336.7) disclose the disposable handwashing liquid of a kind of chitosan tea tree oil, chitosan solubilized under slightly acidic condition is utilized to become the gel character easily absorbed, add Sargassum cytokines, the seed of Fructus Crataegi extracting solution with antibacterial action and there is the natural plant composition such as Semen Granati extracting solution of the effect of moistening, forming through special process manufacture.The composition of the disposable handwashing liquid of tea tree oil of this invention is made up of natural product extraction substantially, poor to the oils and fats removal ability of hand.
Summary of the invention
For above-mentioned technical problem, the invention provides disposable handwashing liquid of a kind of tea tree oil and preparation method thereof.The disposable handwashing liquid of tea tree oil of the present invention is made up of the component of following percentage by weight: benzalkonium chloride 0.1 ~ 2%, lauric acid amide of ethanol 0.5 ~ 3%, dodecanamide propyl amine oxide 0.5 ~ 3%, glycerol 5 ~ 10%, olive oil 1 ~ 5%, vaseline 3 ~ 10%, dimension E acetate 1 ~ 5%, chitosan 1 ~ 5%, Radix Glycyrrhizae extract 5 ~ 15%, tea tree oil 1 ~ 5%, deionized water surplus.
Further, the disposable handwashing liquid of tea tree oil of the present invention is made up of the component of following percentage by weight: benzalkonium chloride 0.5 ~ 1.8%, lauric acid amide of ethanol 0.8 ~ 2%, dodecanamide propyl amine oxide 0.8 ~ 2%, glycerol 6 ~ 9%, olive oil 2 ~ 4%, vaseline 5 ~ 8%, dimension E acetate 2 ~ 4%, chitosan 2 ~ 4%, Radix Glycyrrhizae extract 8 ~ 13%, tea tree oil 2 ~ 4%, deionized water surplus.
Particularly, the disposable handwashing liquid of tea tree oil of the present invention is made up of the component of following percentage by weight: benzalkonium chloride 1%, lauric acid amide of ethanol 1%, dodecanamide propyl amine oxide 1%, glycerol 8%, olive oil 3%, vaseline 6%, dimension E acetate 3%, chitosan 3%, Radix Glycyrrhizae extract 10%, tea tree oil 3%, deionized water surplus.
The preparation method of the disposable handwashing liquid of tea tree oil of the present invention comprises the following steps:
(1). the preparation of aqueous phase: by formula ratio, after chitosan and benzalkonium chloride deionized water solution, adds Radix Glycyrrhizae extract, mix homogeneously, is heated to 60 ~ 70 DEG C;
(2). the preparation of oil phase: by formula ratio, is uniformly mixed lauric acid amide of ethanol, dodecanamide propyl amine oxide, glycerol, olive oil, vaseline 5 ~ 8%, dimension E acetate and tea tree oil, is heated to 50 ~ 60 DEG C;
(3). the preparation of the disposable handwashing liquid of tea tree oil: keep aqueous phase temperature, under stirring, the oil phase that step (2) is obtained is added in the obtained aqueous phase of step (1), make its emulsifying, slow cooling after emulsifying, add excess water, continue to be stirred to and be cooled to room temperature.
Wherein, the preparation method of described Radix Glycyrrhizae extract is as follows: Radix Glycyrrhizae is crushed to by 200 mesh sieves after cleaning, and adds the ratio of 3g water, is added to the water by Radix Glycyrrhizae powder, reflux 3 ~ 5 hours in 1g Radix Glycyrrhizae powder, and gained suspension cools rear elimination insoluble matter and get final product.
Tea tree oil of the present invention disposable handwashing liquid viscosity is less, adopts cationic surfactant to kill various bacteria.Product of the present invention is not containing ethanol, and therefore zest is weak, is suitable for crowd wide.And with the addition of the multiple composition with moisturizing, abnormal smells from the patient is pure and fresh, also can provide good protection while clean both hands to hand skin.
In order to understand better and implement, the following detailed description of the present invention.
Detailed description of the invention
preparation embodiment
The disposable handwashing liquid of tea tree oil of the present invention is prepared by following steps:
(1). the preparation of Radix Glycyrrhizae extract: Radix Glycyrrhizae is crushed to by 200 mesh sieves after cleaning, and adds the ratio of 3g water, is added to the water by Radix Glycyrrhizae powder, reflux 3 ~ 5 hours in 1g Radix Glycyrrhizae powder, gained suspension cools rear elimination insoluble matter and get final product.
(2). the preparation of aqueous phase: by table 1 formula ratio, after chitosan and benzalkonium chloride deionized water solution, adds Radix Glycyrrhizae extract, mix homogeneously, is heated to 60 ~ 70 DEG C;
(3). the preparation of oil phase: by table 1 formula ratio, is uniformly mixed lauric acid amide of ethanol, dodecanamide propyl amine oxide, glycerol, olive oil, vaseline 5 ~ 8%, dimension E acetate and tea tree oil, is heated to 50 ~ 60 DEG C;
(4). the preparation of the disposable handwashing liquid of tea tree oil: keep aqueous phase temperature, under stirring, the oil phase that step (2) is obtained is added in the obtained aqueous phase of step (1), make its emulsifying, slow cooling after emulsifying, add excess water, continue to be stirred to and be cooled to room temperature.
The each component formula amount of < table 1 is in percentage by weight (%) >
effect example
Effect of above-described embodiment 1-5 is described respectively by sensory evaluation below.
50 testers are equally divided into 5 groups, test group sample is given at random by " double blinding " test, require that tester to wash one's hands (i.e. handwashing liquid consumption by self daily custom of washing one's hands, Handwashing ways does not limit), cleaning effect, moist type and zest when the disposable handwashing liquid of the tea tree oil successively obtained by Evaluation operation example 1 ~ 5 is washed one's hands.
Tester according to oneself feel mark, standards of grading adopt 5 points of systems, the poorest with 1 point, and 5 points preferably calculate, finally with the sensory effects of mean values record each embodiment scoring, as shown in table 2 below.
< shows 2>
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Cleaning effect 4.6 4.8 4.9 4.5 4.5
Moistness 4.6 4.6 4.9 4.9 4.7
Zest 1.1 1.1 1.3 1.1 1.2
Can be drawn by upper table, the cleaning effect of the disposable handwashing liquid of the tea tree oil that the present embodiment obtains and moist type are all fine, and zest is very little, and tester is good with rear reflection.
The present invention is not limited to above-mentioned embodiment, if do not depart from the spirit and scope of the present invention to various change of the present invention or distortion, if these are changed and distortion belongs within claim of the present invention and equivalent technologies scope, then the present invention is also intended to comprise these changes and distortion.

Claims (5)

1. the disposable handwashing liquid of tea tree oil, is characterized in that being made up of the component of following percentage by weight: benzalkonium chloride 0.1 ~ 2%, lauric acid amide of ethanol 0.5 ~ 3%, dodecanamide propyl amine oxide 0.5 ~ 3%, glycerol 5 ~ 10%, olive oil 1 ~ 5%, vaseline 3 ~ 10%, dimension E acetate 1 ~ 5%, chitosan 1 ~ 5%, Radix Glycyrrhizae extract 5 ~ 15%, tea tree oil 1 ~ 5%, deionized water surplus.
2. the disposable handwashing liquid of tea tree oil according to claim 1, is characterized in that being made up of the component of following percentage by weight: benzalkonium chloride 0.5 ~ 1.8%, lauric acid amide of ethanol 0.8 ~ 2%, dodecanamide propyl amine oxide 0.8 ~ 2%, glycerol 6 ~ 9%, olive oil 2 ~ 4%, vaseline 5 ~ 8%, dimension E acetate 2 ~ 4%, chitosan 2 ~ 4%, Radix Glycyrrhizae extract 8 ~ 13%, tea tree oil 2 ~ 4%, deionized water surplus.
3. the disposable handwashing liquid of tea tree oil according to claim 2, is characterized in that being made up of the component of following percentage by weight: benzalkonium chloride 1%, lauric acid amide of ethanol 1%, dodecanamide propyl amine oxide 1%, glycerol 8%, olive oil 3%, vaseline 6%, dimension E acetate 3%, chitosan 3%, Radix Glycyrrhizae extract 10%, tea tree oil 3%, deionized water surplus.
4. prepare the method for the disposable handwashing liquid of tea tree oil described in claims 1 to 3 any one, it is characterized in that comprising the following steps:
(1). the preparation of aqueous phase: by formula ratio, after chitosan and benzalkonium chloride deionized water solution, adds Radix Glycyrrhizae extract, mix homogeneously, is heated to 60 ~ 70 DEG C;
(2). the preparation of oil phase: by formula ratio, is uniformly mixed lauric acid amide of ethanol, dodecanamide propyl amine oxide, glycerol, olive oil, vaseline 5 ~ 8%, dimension E acetate and tea tree oil, is heated to 50 ~ 60 DEG C;
(3). the preparation of the disposable handwashing liquid of tea tree oil: keep aqueous phase temperature, under stirring, the oil phase that step (2) is obtained is added in the obtained aqueous phase of step (1), make its emulsifying, slow cooling after emulsifying, add excess water, continue to be stirred to and be cooled to room temperature.
5. the disposable handwashing liquid of tea tree oil according to claim 4, it is characterized in that the preparation method of described Radix Glycyrrhizae extract is as follows: Radix Glycyrrhizae is crushed to by 200 mesh sieves after cleaning, the ratio of 3g water is added in 1g Radix Glycyrrhizae powder, Radix Glycyrrhizae powder is added to the water, reflux 3 ~ 5 hours, gained suspension cools rear elimination insoluble matter and get final product.
CN201510917866.3A 2015-12-11 2015-12-11 Tea tree oil no-wash sanitizer and preparation method thereof Pending CN105342934A (en)

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Application Number Priority Date Filing Date Title
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106265351A (en) * 2016-09-22 2017-01-04 长兴净安环保科技有限公司 One exempts from water bubble hand-cleaning liquid and preparation method thereof
CN107456401A (en) * 2017-08-14 2017-12-12 泉州亚林新材料科技有限公司 A kind of chitosan hand cleanser
CN109833216A (en) * 2017-11-24 2019-06-04 马文娅 A kind of disposable hand sanitizer formula
CN109846737A (en) * 2019-02-27 2019-06-07 广东医科大学 One kind is containing disposable hand cleanser of Tea Saponin and preparation method thereof
CN116437810A (en) * 2020-10-20 2023-07-14 联合利华知识产权控股有限公司 Method for microbiome equilibration

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1432640A (en) * 2002-01-15 2003-07-30 叶汉华 Water-free bacteriostatic hand-washing agent
CN1596877A (en) * 2003-09-16 2005-03-23 上海拜耳科生物科技有限公司 Antiseptic hand cleaning liquid with out water cleaning and its preparation method
CN104188811A (en) * 2014-07-30 2014-12-10 广州立白企业集团有限公司 Foam type wash-free antibacterial liquid soap and using method thereof
CN104666134A (en) * 2013-11-27 2015-06-03 大连林桥科技有限公司 Energy-saving liquid soap
CN104940063A (en) * 2015-06-15 2015-09-30 韩进 Medical liquid soap

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1432640A (en) * 2002-01-15 2003-07-30 叶汉华 Water-free bacteriostatic hand-washing agent
CN1596877A (en) * 2003-09-16 2005-03-23 上海拜耳科生物科技有限公司 Antiseptic hand cleaning liquid with out water cleaning and its preparation method
CN104666134A (en) * 2013-11-27 2015-06-03 大连林桥科技有限公司 Energy-saving liquid soap
CN104188811A (en) * 2014-07-30 2014-12-10 广州立白企业集团有限公司 Foam type wash-free antibacterial liquid soap and using method thereof
CN104940063A (en) * 2015-06-15 2015-09-30 韩进 Medical liquid soap

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中华人民共和国卫生部: "《化妆品卫生规范》", 31 January 2007 *
佚名: "Pure Herbaceous Hand wash Mousse", 《COSDNA》 *
佚名: "茶树精油 干洗手喷雾", 《COSDNA》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106265351A (en) * 2016-09-22 2017-01-04 长兴净安环保科技有限公司 One exempts from water bubble hand-cleaning liquid and preparation method thereof
CN107456401A (en) * 2017-08-14 2017-12-12 泉州亚林新材料科技有限公司 A kind of chitosan hand cleanser
CN109833216A (en) * 2017-11-24 2019-06-04 马文娅 A kind of disposable hand sanitizer formula
CN109846737A (en) * 2019-02-27 2019-06-07 广东医科大学 One kind is containing disposable hand cleanser of Tea Saponin and preparation method thereof
CN116437810A (en) * 2020-10-20 2023-07-14 联合利华知识产权控股有限公司 Method for microbiome equilibration

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Application publication date: 20160224

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