CN105342935A - No-wash oil sanitizer of lily of the valley and preparation method thereof - Google Patents
No-wash oil sanitizer of lily of the valley and preparation method thereof Download PDFInfo
- Publication number
- CN105342935A CN105342935A CN201510917884.1A CN201510917884A CN105342935A CN 105342935 A CN105342935 A CN 105342935A CN 201510917884 A CN201510917884 A CN 201510917884A CN 105342935 A CN105342935 A CN 105342935A
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- CN
- China
- Prior art keywords
- oil
- preparation
- radix glycyrrhizae
- herba convallariae
- percent
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
Abstract
The invention discloses a no-wash oil sanitizer of lily of the valley and a preparation method thereof, and relates to the field of daily chemicals. The no-wash oil sanitizer of lily of the valley is prepared from the following components by weight percent: 0.1 to 2 percent of benzalkonium chloride, 0.5 to 3 percent of coconut diethanolamide, 0.5 to 3 percent of lauramidopropylamine oxide, 5 to 10 percent of glycerinum, 1 to 5 percent of olive oil, 3 to 10 percent of vaseline, 1 to 5 percent of vitamin E acetic ester, 1 to 5 percent of chitosan, 5 to 15 percent of licorice extract, 1 to 5 percent of oil of lily of the valley and the balance of water. The preparation method comprises the following steps: 1, preparation of licorice extract, 2, preparation of an aqueous phase, 3, preparation of an oil phase, and 4, preparation of the no-wash oil sanitizer of lily of the valley. The no-wash oil sanitizer of lily of the valley is good in both cleaning effect and moistening effect, very small in irritation, and is suitable for daily use.
Description
Technical field
The present invention relates to a kind of handwashing liquid.
Background technology
Along with the development of society, people are to the attention of Personal hygiene, and handwashing liquid, as the succedaneum of fancy soap, comes into huge numbers of families.Because handwashing liquid is generally bottled, each discharge by pressing uses on a small quantity, and handwashing liquid seldom has secondary pollution problem.But most of handwashing liquid quality comparatively thickness of market, uses afterflush difficulty, uses a large amount of water to be also difficult to rinse well.And the handwashing liquid generally needing water to rush can not use in the absence of water, make troubles can to like this some specific occasion.
Chinese patent application (application number: 201410461023.2) disclose and carry silver-colored mesoporous silicon washing-free antibacterial hand sanitizer and preparation method thereof a kind of containing, the functional components that comprises of the disposable bacteriostatic hand sanitizer of this invention carries silver-colored mesoporous silicon, the life-time service of its heavy metal silver can cause certain injury to skin, and is not suitable for ordinary people's routine use.
Chinese patent application (application number: 201310378336.7) disclose the disposable handwashing liquid of a kind of chitosan Herba Convallariae oil, chitosan solubilized under slightly acidic condition is utilized to become the gel character easily absorbed, add Sargassum cytokines, the seed of Fructus Crataegi extracting solution with antibacterial action and there is the natural plant composition such as Semen Granati extracting solution of the effect of moistening, forming through special process manufacture.The composition of the disposable handwashing liquid of Herba Convallariae oil of this invention is made up of natural product extraction substantially, poor to the oils and fats removal ability of hand.
Summary of the invention
For above-mentioned technical problem, the invention provides disposable handwashing liquid of a kind of Herba Convallariae oil and preparation method thereof.The disposable handwashing liquid of Herba Convallariae oil of the present invention is made up of the component of following percentage by weight: benzalkonium chloride 0.1 ~ 2%, lauric acid amide of ethanol 0.5 ~ 3%, dodecanamide propyl amine oxide 0.5 ~ 3%, glycerol 5 ~ 10%, olive oil 1 ~ 5%, vaseline 3 ~ 10%, dimension E acetate 1 ~ 5%, chitosan 1 ~ 5%, Radix Glycyrrhizae extract 5 ~ 15%, Herba Convallariae oil 1 ~ 5%, deionized water surplus.
Further, the disposable handwashing liquid of Herba Convallariae oil of the present invention is made up of the component of following percentage by weight: benzalkonium chloride 0.5 ~ 1.8%, lauric acid amide of ethanol 0.8 ~ 2%, dodecanamide propyl amine oxide 0.8 ~ 2%, glycerol 6 ~ 9%, olive oil 2 ~ 4%, vaseline 5 ~ 8%, dimension E acetate 2 ~ 4%, chitosan 2 ~ 4%, Radix Glycyrrhizae extract 8 ~ 13%, Herba Convallariae oil 2 ~ 4%, deionized water surplus.
Particularly, the disposable handwashing liquid of Herba Convallariae oil of the present invention is made up of the component of following percentage by weight: benzalkonium chloride 1%, lauric acid amide of ethanol 1%, dodecanamide propyl amine oxide 1%, glycerol 8%, olive oil 3%, vaseline 6%, dimension E acetate 3%, chitosan 3%, Radix Glycyrrhizae extract 10%, Herba Convallariae oil 3%, deionized water surplus.
The preparation method of the disposable handwashing liquid of Herba Convallariae oil of the present invention comprises the following steps:
(1). the preparation of aqueous phase: by formula ratio, after chitosan and benzalkonium chloride deionized water solution, adds Radix Glycyrrhizae extract, mix homogeneously, is heated to 60 ~ 70 DEG C;
(2). the preparation of oil phase: by formula ratio, is uniformly mixed lauric acid amide of ethanol, dodecanamide propyl amine oxide, glycerol, olive oil, vaseline 5 ~ 8%, dimension E acetate and Herba Convallariae oil, is heated to 50 ~ 60 DEG C;
(3). the preparation of the disposable handwashing liquid of Herba Convallariae oil: keep aqueous phase temperature, under stirring, the oil phase that step (2) is obtained is added in the obtained aqueous phase of step (1), make its emulsifying, slow cooling after emulsifying, add excess water, continue to be stirred to and be cooled to room temperature.
Wherein, the preparation method of described Radix Glycyrrhizae extract is as follows: Radix Glycyrrhizae is crushed to by 200 mesh sieves after cleaning, and adds the ratio of 3g water, is added to the water by Radix Glycyrrhizae powder, reflux 3 ~ 5 hours in 1g Radix Glycyrrhizae powder, and gained suspension cools rear elimination insoluble matter and get final product.
The disposable handwashing liquid viscosity of Herba Convallariae oil of the present invention is less, adopts cationic surfactant to kill various bacteria.Product of the present invention is not containing ethanol, and therefore zest is weak, is suitable for crowd wide.And with the addition of the multiple composition with moisturizing, abnormal smells from the patient is pure and fresh, also can provide good protection while clean both hands to hand skin.
In order to understand better and implement, the following detailed description of the present invention.
Detailed description of the invention
preparation embodiment
The disposable handwashing liquid of Herba Convallariae oil of the present invention is prepared by following steps:
(1). the preparation of Radix Glycyrrhizae extract: Radix Glycyrrhizae is crushed to by 200 mesh sieves after cleaning, and adds the ratio of 3g water, is added to the water by Radix Glycyrrhizae powder, reflux 3 ~ 5 hours in 1g Radix Glycyrrhizae powder, gained suspension cools rear elimination insoluble matter and get final product.
(2). the preparation of aqueous phase: by table 1 formula ratio, after chitosan and benzalkonium chloride deionized water solution, adds Radix Glycyrrhizae extract, mix homogeneously, is heated to 60 ~ 70 DEG C;
(3). the preparation of oil phase: by table 1 formula ratio, is uniformly mixed lauric acid amide of ethanol, dodecanamide propyl amine oxide, glycerol, olive oil, vaseline 5 ~ 8%, dimension E acetate and Herba Convallariae oil, is heated to 50 ~ 60 DEG C;
(4). the preparation of the disposable handwashing liquid of Herba Convallariae oil: keep aqueous phase temperature, under stirring, the oil phase that step (2) is obtained is added in the obtained aqueous phase of step (1), make its emulsifying, slow cooling after emulsifying, add excess water, continue to be stirred to and be cooled to room temperature.
The each component formula amount of < table 1 is in percentage by weight (%) >
effect example
Effect of above-described embodiment 1-5 is described respectively by sensory evaluation below.
50 testers are equally divided into 5 groups, test group sample is given at random by " double blinding " test, require that tester to wash one's hands (i.e. handwashing liquid consumption by self daily custom of washing one's hands, Handwashing ways does not limit), cleaning effect, moist type and zest when the disposable handwashing liquid of Herba Convallariae oil successively obtained by Evaluation operation example 1 ~ 5 is washed one's hands.
Tester according to oneself feel mark, standards of grading adopt 5 points of systems, the poorest with 1 point, and 5 points preferably calculate, finally with the sensory effects of mean values record each embodiment scoring, as shown in table 2 below.
< shows 2>
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Cleaning effect | 4.7 | 4.7 | 4.7 | 4.6 | 4.8 |
| Moistness | 4.7 | 4.5 | 4.6 | 4.7 | 4.9 |
| Zest | 1.3 | 1.1 | 1.5 | 1.4 | 1.4 |
Can be drawn by upper table, cleaning effect and the moist type of the disposable handwashing liquid of Herba Convallariae oil that the present embodiment obtains are all fine, and zest is very little, and tester is good with rear reflection.
The present invention is not limited to above-mentioned embodiment, if do not depart from the spirit and scope of the present invention to various change of the present invention or distortion, if these are changed and distortion belongs within claim of the present invention and equivalent technologies scope, then the present invention is also intended to comprise these changes and distortion.
Claims (5)
1. the disposable handwashing liquid of Herba Convallariae oil, is characterized in that being made up of the component of following percentage by weight: benzalkonium chloride 0.1 ~ 2%, lauric acid amide of ethanol 0.5 ~ 3%, dodecanamide propyl amine oxide 0.5 ~ 3%, glycerol 5 ~ 10%, olive oil 1 ~ 5%, vaseline 3 ~ 10%, dimension E acetate 1 ~ 5%, chitosan 1 ~ 5%, Radix Glycyrrhizae extract 5 ~ 15%, Herba Convallariae oil 1 ~ 5%, deionized water surplus.
2. the disposable handwashing liquid of Herba Convallariae oil according to claim 1, is characterized in that being made up of the component of following percentage by weight: benzalkonium chloride 0.5 ~ 1.8%, lauric acid amide of ethanol 0.8 ~ 2%, dodecanamide propyl amine oxide 0.8 ~ 2%, glycerol 6 ~ 9%, olive oil 2 ~ 4%, vaseline 5 ~ 8%, dimension E acetate 2 ~ 4%, chitosan 2 ~ 4%, Radix Glycyrrhizae extract 8 ~ 13%, Herba Convallariae oil 2 ~ 4%, deionized water surplus.
3. the disposable handwashing liquid of Herba Convallariae oil according to claim 2, is characterized in that being made up of the component of following percentage by weight: benzalkonium chloride 1%, lauric acid amide of ethanol 1%, dodecanamide propyl amine oxide 1%, glycerol 8%, olive oil 3%, vaseline 6%, dimension E acetate 3%, chitosan 3%, Radix Glycyrrhizae extract 10%, Herba Convallariae oil 3%, deionized water surplus.
4. prepare the method for the disposable handwashing liquid of Herba Convallariae oil described in claims 1 to 3 any one, it is characterized in that comprising the following steps:
(1). the preparation of aqueous phase: by formula ratio, after chitosan and benzalkonium chloride deionized water solution, adds Radix Glycyrrhizae extract, mix homogeneously, is heated to 60 ~ 70 DEG C;
(2). the preparation of oil phase: by formula ratio, is uniformly mixed lauric acid amide of ethanol, dodecanamide propyl amine oxide, glycerol, olive oil, vaseline 5 ~ 8%, dimension E acetate and Herba Convallariae oil, is heated to 50 ~ 60 DEG C;
(3). the preparation of the disposable handwashing liquid of Herba Convallariae oil: keep aqueous phase temperature, under stirring, the oil phase that step (2) is obtained is added in the obtained aqueous phase of step (1), make its emulsifying, slow cooling after emulsifying, add excess water, continue to be stirred to and be cooled to room temperature.
5. the disposable handwashing liquid of Herba Convallariae oil according to claim 4, it is characterized in that the preparation method of described Radix Glycyrrhizae extract is as follows: Radix Glycyrrhizae is crushed to by 200 mesh sieves after cleaning, the ratio of 3g water is added in 1g Radix Glycyrrhizae powder, Radix Glycyrrhizae powder is added to the water, reflux 3 ~ 5 hours, gained suspension cools rear elimination insoluble matter and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510917884.1A CN105342935A (en) | 2015-12-11 | 2015-12-11 | No-wash oil sanitizer of lily of the valley and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510917884.1A CN105342935A (en) | 2015-12-11 | 2015-12-11 | No-wash oil sanitizer of lily of the valley and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105342935A true CN105342935A (en) | 2016-02-24 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510917884.1A Pending CN105342935A (en) | 2015-12-11 | 2015-12-11 | No-wash oil sanitizer of lily of the valley and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105342935A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109833216A (en) * | 2017-11-24 | 2019-06-04 | 马文娅 | A kind of disposable hand sanitizer formula |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104188811A (en) * | 2014-07-30 | 2014-12-10 | 广州立白企业集团有限公司 | Foam type wash-free antibacterial liquid soap and using method thereof |
| CN104414909A (en) * | 2013-08-28 | 2015-03-18 | 青岛医防消毒专业技术中心 | Chitosan washing-free hand sanitizer |
| CN104666134A (en) * | 2013-11-27 | 2015-06-03 | 大连林桥科技有限公司 | Energy-saving liquid soap |
-
2015
- 2015-12-11 CN CN201510917884.1A patent/CN105342935A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104414909A (en) * | 2013-08-28 | 2015-03-18 | 青岛医防消毒专业技术中心 | Chitosan washing-free hand sanitizer |
| CN104666134A (en) * | 2013-11-27 | 2015-06-03 | 大连林桥科技有限公司 | Energy-saving liquid soap |
| CN104188811A (en) * | 2014-07-30 | 2014-12-10 | 广州立白企业集团有限公司 | Foam type wash-free antibacterial liquid soap and using method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 中华人民共和国卫生部: "《化妆品卫生规范》", 31 January 2007 * |
| 王建新: "《化妆品植物原料大全》", 30 June 2012 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109833216A (en) * | 2017-11-24 | 2019-06-04 | 马文娅 | A kind of disposable hand sanitizer formula |
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| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20160224 |