CN109793696A - A kind of anti-dandruff plant composition and its preparation method and application - Google Patents
A kind of anti-dandruff plant composition and its preparation method and application Download PDFInfo
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- CN109793696A CN109793696A CN201910225334.1A CN201910225334A CN109793696A CN 109793696 A CN109793696 A CN 109793696A CN 201910225334 A CN201910225334 A CN 201910225334A CN 109793696 A CN109793696 A CN 109793696A
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Abstract
The invention discloses a kind of anti-dandruff plant compositions and its preparation method and application.Anti-dandruff plant composition includes the component of following weight ratio: frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed is 5~20:5~15:3~10:2~5:3~8:5~20:5~15:3~10:2~5.Anti-dandruff plant society is applied in shampoo, the anti-dandruff plant composition is 2~8% in the weight percentage of shampoo.Composition of the invention makes each component produce apparent synergistic effect, has stronger bacteriostasis by rationally screening and compounding herb extract, inhibit scalp pruritus, the effect for removing dandruff, can be applied in a variety of hair care products, have extraordinary application prospect.
Description
Technical field
The present invention relates to a kind of hair care product, be specifically related to a kind of anti-dandruff plant composition and preparation method thereof and
Using.
Background technique
Dandruff is a very universal scalp problems.In the world, according to incompletely statistics, disappearing more than 1/3
The person of expense is by its puzzlement.Cause dandruff a key factor be the chlosma on scalp hyper-proliferative, at present have one's hair wash
Common chemistry anti-dandruff agent is mostly broad spectrum antimicrobial agent in product, such as Octopirox (OCT), ZPT, climbazole and two pyridines
Thioketones magnesium sulfate salt (MDS) etc. intermittently using the growth that bacterium and fungi can be effectively suppressed, but is used for a long time and easily causes skin
The problems such as skin stimulation, sensitization and toxicity.
With the continuous development of society, current living environment pollution problem is paid more and more attention, people to " it is natural, organic,
The environmental protection, green " consumer goods are thirsted for growing day by day.In terms of daily necessities, requirement of the consumer to hair washing product is also continuously improved, and one
Aspect needs efficient product confrontation health pressure as caused by environmental pollution；On the other hand, it is desirable that product property temperature
With human and environment can be made to reach the equilibrium state of harmony and natural.Therefore, a kind of mild plant anti-dandruff component is developed, and is had
Antianaphylactic product is more by the favor of consumer.
Summary of the invention
It is provided a kind of with antiallergy plant desquamation compositions it is an object of the invention to overcome the above problem.
To achieve the above object, the technical solution adopted by the present invention is that a kind of anti-dandruff plant composition, which is characterized in that packet
Include following components: frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed.
In the solution of the present invention, frutus cnidii, root according to research reports, has dispelling wind and arresting itching, heat-clearing and damp-drying drug, anti-mistake
It is quick.
The effect of camellia seed has cleaning, sterilizing and itch-relieving, goes oil removal.
Ginger, it is warm-natured, containing main components such as gingerol, zingiberene, zingerone, gingerols, also contain glutamic acid, asparagine
A variety of amino acid such as acid, serine, glycine have stimulation scalp vein, strengthen scalp metabolism, and enhancing local blood follows
Ring activates hair follicle tissue, promotes the growth of hair, inhibits scalp pruritus, strengthens root of hair, there is cleaning scalp, removal dandruff and other effects.
Purslane, the substances such as SL3 fatty acid and vitamin A rich in, have it is clearing heat and detoxicating, Li Shui dries, dissipate blood
Detumescence, dust-collection sterilization, anti-inflammatory analgetic, the drug effects such as blood-stanching and blood-cooling.
Wrinkled giant hyssop: antimycotic and antivirus action.
Wild chrysanthemum, Compendium of Material Medica " property is sweet, slightly cold, has the effect of dissipating wind-heat, calming the liver and improving eyesight ".With antibacterial, disease-resistant
Toxic action, heat-clearing anti-inflammatory properties, elimination activity free radical, antioxidation prevent skin aging.
Rheum officinale, bitter and it is cold in nature, can cooling blood and hemostasis and astringing to arrest bleeding.It is clearing heat and detoxicating, promoting blood circulation.
Cortex Phellodendri has the effect of heat-clearing and damp-drying drug, purging intense heat, except steaming, detoxification sore treatment
Lopseed, solution poison rash, control eczema of scrotum, sore swollen toxin, and hair growth controls alopecia seborrheica etc.
The present invention shows that 9 kinds of component compoundings have achieved the effect that synergy by numerous studies, can be effectively
Inhibit chlosma and anti-dandruff effect, be provided simultaneously with antiallergy and deep layer deoil, oil-control effect.
As the preferred embodiment of the anti-dandruff plant composition of the present invention, the frutus cnidii, camellia seed, ginger, purslane,
Wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed weight ratio be frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild chrysanthemum:
Rheum officinale: Cortex Phellodendri: lopseed=5~20:5~15:3~10:2~5:3~8:5~20:5~15:3~10:2~5.
Plant extracts of the present invention uses the compounding of said ratio, can mutually promote and reach preferable inhibition horse traction
Color bacterium and anti-dandruff effect, be provided simultaneously with antiallergy and deep layer deoil, oil-control effect.
As the preferred embodiment of the anti-dandruff plant composition of the present invention, the frutus cnidii, camellia seed, ginger, purslane,
Wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed weight ratio be frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild chrysanthemum:
Rheum officinale: Cortex Phellodendri: lopseed=10:8~12:5~10:3~4:5~6:10:6~10:5:3.
Especially, antibacterial, anti-dandruff, deoil, oil-control effect when above-mentioned plant extract object is compounded according to the above ratio
More preferably.
As the preferred embodiment of the anti-dandruff plant composition of the present invention, the frutus cnidii, camellia seed, ginger, purslane,
Wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed weight ratio be frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild chrysanthemum:
Rheum officinale: Cortex Phellodendri: lopseed=10:8:10:4:6:10:8:5:3.
It is found by present inventor's lot of experiments, when the plant extracts is compounded using aforementioned proportion
When, bacterium, it is anti-dandruff, deoil, oil-control effect reaches best.
The second object of the present invention is the provision of the anti-dandruff plant composition and is preparing answering in hair care product
With.Any description above composition is preparing the application in hair care product, also belongs to protection scope of the present invention.
The third object of the present invention is the provision of a kind of hair care product containing the anti-dandruff plant composition.
The fourth object of the present invention is the provision of a kind of shampoo containing the anti-dandruff plant composition, described anti-dandruff
Plant composition weight percent in shampoo is 2~8%.With the increase of anti-dandruff plant society content in shampoo,
Its anti-dandruff effect also increases, when the additive amount of anti-dandruff plant composition is greater than 2%, anti-dandruff significant effect, when anti-dandruff plant group
When closing the additive amount of object and being greater than 8%, anti-dandruff effect increase it is unobvious, therefore, when the additive amount of anti-dandruff plant composition is 2~
When 8%, anti-dandruff significant effect.
As the preferred embodiment of shampoo of the invention, anti-dandruff plant composition weight percent in shampoo
Than being 4%.
As the preferred embodiment of shampoo of the invention, the shampoo further includes conditioner 0.5~10%, thickening
Agent 1~6%, aromatic 0.1~0.5%, surfactant 12~25%, pearling agent 0.5~3% are assigned ester agent 0.5~6%, are helped
The deionized water of solvent 1~5%, preservative 0.1~0.2%, chelating agent 0.05~0.1% and surplus.
Preferably, surfactant be laureth sodium sulphate, laureth ammonium sulfate, lauryl sodium sulfate,
Ammonium lauryl sulfate, laurel alcohol sulfuric ester ammonium, laruyl alcohol sodium sulfovinate, Coconut Fatty Acid Monoethanolamide, cocamidopropyl propyl amide sweet tea
At least one of dish alkali.
It is highly preferred that the surfactant uses following weight ratio ingredient: laureth ammonium sulfate, dodecyl sulphur
Sour ammonium, Coconut Fatty Acid Monoethanolamide, 10~14:3 of Cocoamidopropyl betaine weight ratio~6:1~3:2~5.
Preferably, conditioner is Polyquaternium-10, polyquaternium -7, polyquaternium -39, polyquaternium -73, guar gum
At least one of hydroxypropyl-trimethyl ammonium chloride, behenyl base trimethyl ammonium chloride, polydimethyl siloxane fluid.
It is highly preferred that conditioner is Polyquaternium-10, guar hydroxypropyltrimonium ammonium chloride, polydimethyl siloxane fluid matter
Amount is than being 0.05~0.2:0.1~0.2:0.8~3.
Preferably, thickener is card wave 2020, acrylic acid esters co-polymer, hydroxy cellulose sodium, hydroxyethyl cellulose, carboxylic
At least one of sodium carboxymethylcellulose pyce, coconut oleoyl amine DEA, NaCl.
It is highly preferred that thickener is coconut oleoyl amine DEA.
Preferably, assigning ester agent is lanolin, shea butter, olive oil, linseed oil, camellia oil, jojoba oil PEG-150 ester
Class, at least one of PEG-55 stearic acid esters etc..
It is highly preferred that assign ester agent be lanolin, jojoba oil PEG-150 esters, 0.3~3:0.1 of linseed oil weight ratio~
3:0.1~3.
Preferably, pearling agent is one of ethylene glycol double stearate, pearlite slurry.
It is highly preferred that ethylene glycol double stearate.
Preferably, cosolvent is ethoxydiglycol, in glycerol, propylene glycol, 1,3-BDO, 1618 alcohol, dipropylene glycol
At least one.
It is highly preferred that cosolvent is mass ratio 1~3:1~3 of glycerol, 1618 alcohol.
Preferably, chelating agent is one of EDTA- disodium, citric acid, sodium citrate.
Preferred chelating agent EDTA- disodium
Preferably, preservative be decoyl hydroximic acid, parahydroxyacet-ophenone, Kathon CG GG, glycerol octanoic acid rouge, outstanding Malaysia and China at least
It is a kind of.
Preferred preservative is parahydroxyacet-ophenone and decoyl hydroximic acid mass ratio is 0.5~1:0.2~1.
As the preferred embodiment of shampoo of the invention, the shampoo includes following components in percentage by weight:
Laureth ammonium sulfate 12%, ammonium lauryl sulfate 5%, Coconut Fatty Acid Monoethanolamide 1%, Cocoamidopropyl betaine
3%, 1.5% coconut oleoyl amine DEA, Polyquaternium-10 0.1%, guar hydroxypropyltrimonium ammonium chloride 0.1%, poly dimethyl
Silicone oil 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, linseed oil 0.3%, ethylene glycol double stearate
1.4%, glycerol 1.5%, 1618 alcohol 2.0%, anti-dandruff plant composition 4%, preservative 0.1%, 0.05% chelating agent, aromatic
0.4% and surplus deionized water.
When the shampoo is matched using said components, antibacterial, anti-dandruff, oil-control, effect of deoiling are best.
Beneficial effects of the present invention: composition of the invention keeps each component common by reasonably selecting traditional Chinese medicine ingredients compounding
It playing a role and achievees the effect that anti-dandruff sterilization, correct leatherware has preferable bactericidal effect, and plant extracts is non-stimulated to scalp,
It is able to suppress the excess oil of skin secretion, and hair quality is made to restore normal, permanence operation is more preferably.It can be applied to a variety of hairs
In care product, moreover, safety, Small side effects, have extraordinary application prospect.
Detailed description of the invention
Fig. 1 is the dandruff test effect figure of the embodiment of the present invention 1.
Specific embodiment
The present invention is made with specific embodiment with reference to the accompanying drawings of the specification and further being elaborated, the embodiment
It is served only for explaining the present invention, be not intended to limit the scope of the present invention.Test method as used in the following examples is such as without spy
Different explanation, is conventional method；Used material, reagent etc., unless otherwise specified, for the reagent commercially obtained
And material.
Each raw material involved by following embodiment is commercially available versatile material unless otherwise instructed.
Embodiment 1
As a kind of embodiment of anti-dandruff plant composition of the present invention, the anti-dandruff plant composition includes following components:
Frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed, the frutus cnidii, camellia seed, life
Ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed weight ratio are as follows: frutus cnidii: camellia seed: ginger: purslane:
Wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=10:8:10:4:6:10:8:5:3.
The anti-dandruff plant composition the preparation method comprises the following steps: first by medicinal material frutus cnidii, camellia seed, ginger, purslane, the leaves of pulse plants
Perfume, wild chrysanthemum, rheum officinale, Cortex Phellodendri, lopseed are crushed to coarse powder according to mass ratio, add 10 times of amount deionized waters, and small fire is heated to reflux 2
It is secondary, each 1h, filtration, merge 2 filtrates, be centrifuged, take supernatant, and on a rotary evaporator keep vacuum degree -0.1~-
0.08MPa, temperature 70 C are concentrated under reduced pressure into 52ml, that is, obtain the anti-dandruff compound of 1mg/ml, save backup in 4 DEG C of refrigerators.
The anti-dandruff plant composition is applied in shampoo, the shampoo includes the group of following weight percentage
Point: anti-dandruff plant composition 4%, laureth ammonium sulfate 12%, ammonium lauryl sulfate 5%, Coconut Fatty Acid Monoethanolamide
1%, Cocoamidopropyl betaine 3%, coconut oleoyl amine DEA 1.5%, Polyquaternium-10 0.1%, guar gum hydroxypropyl three
Ammonio methacrylate 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, linseed oil
0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%, preservative 0.1%, chelating agent 0.05%, virtue
The deionized water of pastil 0.4% and surplus.
The preparation method of the shampoo the following steps are included:
S1. first deionized water is poured into container, then by glycerol, Polyquaternium-10, guar hydroxypropyltrimonium chlorination
Ammonium is scattered in deionized water, is heated while stirring, by the temperature of mixture in container be heated to maintaining after 75 DEG C the temperature after
Continuous stirring obtains mixture A until Polyquaternium-10 is completely dissolved；
S2. laureth ammonium sulfate, ammonium lauryl sulfate, coconut oil are sequentially added into mixture A while stirring
Single ethanol amide, Cocoamidopropyl betaine, coconut oleoyl amine DEA are stirred evenly, and obtain mixture B,
S3. by the lanolin dissolved by heating, jojoba oil PEG-150 esters, ethylene glycol double stearate, 1618
Alcohol, linseed oil, polydimethyl siloxane fluid mixture, which are added in mixture B, obtains mixture C.In entire whipping process, in container
The temperature of mixture maintains always 75 DEG C；
S4. mixture C is naturally cooling to 40 DEG C, sequentially adds preservative and essence, stirred evenly, obtain hair washing liquid-based
Expect D；
S5. the anti-dandruff compound of plant and shampoo base D are mixed and stirred for uniformly.
Embodiment 2
The present embodiment difference from Example 1 is only that, the difference of the anti-dandruff plant composition, the cnidium monnieri
Son, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are as follows: frutus cnidii: camellia seed:
Ginger: purslane: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=5:15:10:5:8:20:15:10:5.
The preparation method of anti-dandruff plant composition of the invention is same as Example 1.
Embodiment 3
The present embodiment difference from Example 1 is only that, the difference of the anti-dandruff plant composition, the cnidium monnieri
Son, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are as follows: frutus cnidii: camellia seed:
Ginger: purslane: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed 20:5:3:2:3:5:5:3:2.
The preparation method of anti-dandruff plant composition of the invention is same as Example 1.
Embodiment 4
The present embodiment difference from Example 1 is only that, the difference of the anti-dandruff plant composition, the cnidium monnieri
Son, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are as follows: frutus cnidii: camellia seed:
Ginger: purslane: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed 10:12:6:4:6:10:10:5:3.
The preparation method of anti-dandruff plant composition of the invention is same as Example 1.
Embodiment 5
The present embodiment difference from Example 1 is only that, the difference of the anti-dandruff plant composition, the cnidium monnieri
Son, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are as follows: frutus cnidii: camellia seed:
Ginger: purslane: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed 10:10:5:3:5:10:6:5:3.
The preparation method of anti-dandruff plant composition of the invention is same as Example 1.
Embodiment 6
The present embodiment difference from Example 1 is only that the anti-dandruff plant composition is applied to the institute in shampoo
The weight percentage for accounting for addition is different, and the additive amount of the anti-dandruff plant composition of the present embodiment is 2%.
Embodiment 7
The present embodiment difference from Example 1 is only that the anti-dandruff plant composition is applied to the institute in shampoo
The weight percentage for accounting for addition is different, and the additive amount of the anti-dandruff plant composition of the present embodiment is 5%.
Embodiment 8
The present embodiment difference from Example 1 is only that the anti-dandruff plant composition is applied to the institute in shampoo
The weight percentage for accounting for addition is different, and the additive amount of the anti-dandruff plant composition of the present embodiment is 6%.
Embodiment 9
The present embodiment difference from Example 1 is only that the anti-dandruff plant composition is applied to the institute in shampoo
The weight percentage for accounting for addition is different, and the additive amount of the anti-dandruff plant composition of the present embodiment is 8%.
Embodiment 10
The present embodiment difference from Example 1 is only that, the difference of the component of the shampoo, the hair washing of the present embodiment
Water includes following components in percentage by weight: laureth ammonium sulfate 11%, ammonium lauryl sulfate 6%, coconut oil list second
Alkylolamides 2%, Cocoamidopropyl betaine 3%, coconut oleoyl amine DEA 2%, Polyquaternium-10 0.1%, guar gum hydroxypropyl
Base trimethyl ammonium chloride 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 1%, jojoba oil PEG-150 esters 0.6%, flax
Oily 0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%, anti-dandruff plant composition 6%, preservative
0.1%, chelating agent 0.05%, the deionized water of aromatic 0.1% and surplus.
The preparation method of the shampoo the following steps are included:
S1. first deionized water is poured into container, then by glycerol, Polyquaternium-10, guar hydroxypropyltrimonium chlorination
Ammonium is scattered in deionized water, is heated while stirring, by the temperature of mixture in container be heated to maintaining after 75 DEG C the temperature after
Continuous stirring obtains mixture A until Polyquaternium-10 is completely dissolved；
S2. laureth ammonium sulfate, ammonium lauryl sulfate, coconut oil are sequentially added into mixture A while stirring
Single ethanol amide, Cocoamidopropyl betaine, coconut oleoyl amine DEA are stirred evenly, and obtain mixture B,
S3. by the lanolin dissolved by heating, jojoba oil PEG-150 esters, ethylene glycol double stearate, 1618
Alcohol, linseed oil, polydimethyl siloxane fluid mixture, which are added in mixture B, obtains mixture C.In entire whipping process, in container
The temperature of mixture maintains always 75 DEG C；
S4. mixture C is naturally cooling to 40 DEG C, sequentially adds preservative and essence, stirred evenly, obtain hair washing liquid-based
Expect D；
S5. the anti-dandruff compound of plant and shampoo base D are mixed and stirred for uniformly.
Embodiment 11
The present embodiment difference from Example 1 is only that, the difference of the component of the shampoo, the hair washing of the present embodiment
Water includes following components in percentage by weight: laureth sodium sulphate 8%, lauryl sodium sulfate 2%, cocamidopropyl propyl amide
Glycine betaine 2%, card wave 2,020 0.5%, acrylic acid esters co-polymer 0.5%, polyquaternium -7 0.1%, behenyl base trimethyl
Ammonium chloride 0.1%, polydimethyl siloxane fluid 0.3%, lanolin 1.0%, jojoba oil PEG-150 esters 0.3%, camellia oil
1.0%, pearlite slurry 0.5%, ethoxydiglycol 0.5%, propylene glycol 0.5%, anti-dandruff plant composition 2%, preservative
0.1%, the deionized water of chelating agent 0.05%, aromatic 0.4% and surplus.
The preparation method of the shampoo the following steps are included:
S1. first deionized water is poured into container, then by ethoxydiglycol, polyquaternium -7, behenyl base trimethyl chlorine
Change ammonium to be scattered in deionized water, heats while stirring, the temperature of mixture in container is heated to maintain the temperature after 75 DEG C
Continue to stir, until polyquaternium -7 is completely dissolved, obtains mixture A；
S2. laureth sodium sulphate, lauryl sodium sulfate, cocounut oil acyl are sequentially added into mixture A while stirring
Amine propyl betaine, card wave 2020, acrylic acid esters co-polymer stir evenly, and obtain mixture B,
S3. by the lanolin dissolved by heating, jojoba oil PEG-150 esters, pearlite slurry, propylene glycol, camellia oil
Mixture is added in mixture B and obtains mixture C.In entire whipping process, the temperature of mixture is maintained always in container
75℃；
S4. mixture C is naturally cooling to 40 DEG C, sequentially adds preservative and essence, stirred evenly, obtain hair washing liquid-based
Expect D；
S5. the anti-dandruff compound of plant and shampoo base D are mixed and stirred for uniformly.
Embodiment 12
The present embodiment difference from Example 1 is only that, the difference of the component of the shampoo, the hair washing of the present embodiment
Water includes following components in percentage by weight: laurel alcohol sulfuric ester ammonium 13%, laruyl alcohol sodium sulfovinate 6%, coconut oil monoethanol
Amide 3%, Cocoamidopropyl betaine 3%, hydroxy cellulose sodium 3%, hydroxyethyl cellulose 3%, polyquaternium -39
4%, polyquaternium -73 2%, behenyl base trimethyl ammonium chloride 2%, polydimethyl siloxane fluid 2.0%, shea butter 2%, olive
Oily 2%, jojoba oil PEG-150 esters 0.3%, linseed oil 1.7%, ethylene glycol double stearate 3%, glycerol 2%, 1,3- fourth
Glycol 3%, anti-dandruff plant composition 4%, preservative 0.2%, 0.1% chelating agent, aromatic 0.5% and surplus deionization
Water.
The preparation method of the shampoo the following steps are included:
S1. first deionized water is poured into container, then by glycerol, polyquaternium -39, polyquaternium -73, behenyl base front three
Ammonium chloride is scattered in deionized water, is heated while stirring, and maintaining after the temperature of mixture in container is heated to 75 DEG C should
Temperature continues to stir, and until polyquaternium -39, polyquaternium -73 are completely dissolved, obtains mixture A；
S2. laurel alcohol sulfuric ester ammonium, laruyl alcohol sodium sulfovinate, coconut oil list are sequentially added into mixture A while stirring
Glycollic amide, Cocoamidopropyl betaine, hydroxy cellulose sodium, hydroxyethyl cellulose stir evenly, and obtain mixture B；
S3. the shea butter dissolved by heating, olive oil, jojoba oil PEG-150 esters, ethylene glycol is double stearic
Acid esters, 1,3-BDO, linseed oil, polydimethyl siloxane fluid mixture, which are added in mixture B, obtains mixture C.Entirely stirring
In the process, the temperature of mixture maintains always 75 DEG C in container；
S4. mixture C is naturally cooling to 40 DEG C, sequentially adds preservative and essence, stirred evenly, obtain hair washing liquid-based
Expect D；
S5. the anti-dandruff compound of plant and shampoo base D are mixed and stirred for uniformly.
Comparative example 1
This comparative example is distinguished with embodiment 1 and is only that, the difference of anti-dandruff plant composition, the anti-dandruff plant group of this comparative example
Close object include following components: purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed, the purslane, wrinkled giant hyssop, wild chrysanthemum,
Rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are as follows: purslane: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=4:6:10:8:5:
3。
The anti-dandruff plant composition of this comparative example is applied in shampoo, the shampoo includes following weight percentage
Component: anti-dandruff plant composition 4%, laureth ammonium sulfate 12%, ammonium lauryl sulfate 5%, coconut oil monoethanol
Amide 1%, Cocoamidopropyl betaine 3%, coconut oleoyl amine DEA 1.5%, Polyquaternium-10 0.1%, guar gum hydroxypropyl
Base trimethyl ammonium chloride 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, Asia
Sesame oil 0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%, preservative 0.1%, chelating agent
0.05%, the deionized water of aromatic 0.4% and surplus.
The anti-dandruff plant composition of this comparative example and the preparation method of shampoo are same as Example 1.
Comparative example 2
This comparative example difference from Example 1 is only that, the difference of anti-dandruff plant composition, the anti-dandruff plant of this comparative example
Compositions include following components: frutus cnidii, camellia seed, ginger, rheum officinale, Cortex Phellodendri and lopseed, the frutus cnidii, camellia seed,
Ginger, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are as follows: frutus cnidii: camellia seed: ginger: rheum officinale: Cortex Phellodendri: lopseed=10:8:
10:8:5:3.
The anti-dandruff plant composition of this comparative example is applied in shampoo, the shampoo includes following weight percentage
Component: anti-dandruff plant composition 4%, laureth ammonium sulfate 12%, ammonium lauryl sulfate 5%, coconut oil monoethanol
Amide 1%, Cocoamidopropyl betaine 3%, coconut oleoyl amine DEA 1.5%, Polyquaternium-10 0.1%, guar gum hydroxypropyl
Base trimethyl ammonium chloride 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, Asia
Sesame oil 0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%, preservative 0.1%, chelating agent
0.05%, the deionized water of aromatic 0.4% and surplus.
The anti-dandruff plant composition of this comparative example and the preparation method of shampoo are same as Example 1.
Comparative example 3
The anti-dandruff plant composition of this comparative example includes following components: frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop,
Wild chrysanthemum, the frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum weight ratio are as follows: frutus cnidii: camellia seed: raw
Ginger: purslane: wrinkled giant hyssop: wild chrysanthemum=10:8:10:4:6:10.
The anti-dandruff plant composition of this comparative example is applied in shampoo, the shampoo includes following weight percentage
Component: anti-dandruff plant composition 4%, laureth ammonium sulfate 12%, ammonium lauryl sulfate 5%, coconut oil monoethanol
Amide 1%, Cocoamidopropyl betaine 3%, coconut oleoyl amine DEA 1.5%, Polyquaternium-10 0.1%, guar gum hydroxypropyl
Base trimethyl ammonium chloride 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, Asia
Sesame oil 0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%, preservative 0.1%, chelating agent
0.05%, the deionized water of aromatic 0.4% and surplus.
The anti-dandruff plant composition of this comparative example and the preparation method of shampoo are same as Example 1.
Comparative example 4
The anti-dandruff plant composition of this comparative example includes following components: frutus cnidii, ginkgo leaf, cacumen biotae, hundred steps, wrinkled giant hyssop,
Wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed, the frutus cnidii, ginkgo leaf, cacumen biotae, hundred steps, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri
With the weight ratio of lopseed are as follows: frutus cnidii: ginkgo leaf: cacumen biotae: hundred steps: wrinkled giant hyssop: wild chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=
10:8:10:4:6:10:8:5:3.
The anti-dandruff plant composition of this comparative example is applied in shampoo, the shampoo includes following weight percentage
Component: anti-dandruff plant composition 4%, laureth ammonium sulfate 12%, ammonium lauryl sulfate 5%, coconut oil monoethanol
Amide 1%, Cocoamidopropyl betaine 3%, coconut oleoyl amine DEA 1.5%, Polyquaternium-10 0.1%, guar gum hydroxypropyl
Base trimethyl ammonium chloride 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, Asia
Sesame oil 0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%, preservative 0.1%, chelating agent
0.05%, the deionized water of aromatic 0.4% and surplus.
The anti-dandruff plant composition of this comparative example and the preparation method of shampoo are same as Example 1.
Comparative example 5
The anti-dandruff plant composition of this comparative example includes following components: frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop,
Wild chrysanthemum, Radix Astragali, the fruit of summer cypress and the achene of Siberian cocklebur, the frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, Radix Astragali,
The weight ratio of skin and the achene of Siberian cocklebur are as follows: frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild chrysanthemum: Radix Astragali: the fruit of summer cypress: Siberian cocklebur
Son=10:8:10:4:6:10:8:5:3.
The anti-dandruff plant composition of this comparative example and the preparation method of shampoo are same as Example 1.
Comparative example 6
The shampoo of this comparative example includes following components in percentage by weight: laureth ammonium sulfate 12%, dodecane
Base ammonium sulfate 5%, Coconut Fatty Acid Monoethanolamide 1%, Cocoamidopropyl betaine 3%, 1.5% coconut oleoyl amine DEA, polyquaternary amine
Salt -10 0.1%, guar hydroxypropyltrimonium ammonium chloride 0.1%, polydimethyl siloxane fluid 2.5%, lanolin 0.2%, flash
Bar oil PEG-150 esters 0.6%, linseed oil 0.3%, ethylene glycol double stearate 1.4%, glycerol 1.5%, 1618 alcohol 2.0%,
Anti-dandruff agent ZPT 1%, preservative 0.1%, the deionized water of chelating agent 0.05%, aromatic 0.4% and surplus.
The preparation method of the shampoo of this comparative example is same as Example 1.
Comparative example 7
The shampoo of this comparative example includes following components in percentage by weight: laurel the difference is that without anti-dandruff agent
Alcohol polyethers ammonium sulfate 12%, ammonium lauryl sulfate 5%, Coconut Fatty Acid Monoethanolamide 1%, Cocoamidopropyl betaine 3%,
Coconut oleoyl amine DEA 1.5%, Polyquaternium-10 0.1%, guar hydroxypropyltrimonium ammonium chloride 0.1%, poly dimethyl silicon
Oily 2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, linseed oil 0.3%, ethylene glycol double stearate
1.4%, glycerol 1.5%, 1618 alcohol 2.0%, preservative 0.1%, chelating agent 0.05%, aromatic 0.4% and surplus go from
Sub- water.
The shampoo preparation method of this comparative example such as embodiment 1.
Comparative example 8
The present embodiment difference from Example 1 is only that the anti-dandruff plant composition is applied to the institute in shampoo
The weight percentage for accounting for addition is different, and the additive amount of the anti-dandruff plant composition of the present embodiment is 1.5%.
Comparative example 9
The present embodiment difference from Example 1 is only that the anti-dandruff plant composition is applied to the institute in shampoo
The weight percentage for accounting for addition is different, and the additive amount of the anti-dandruff plant composition of the present embodiment is 9%.
Embodiment 12
Measure of merit is carried out to the shampoo that embodiment 1~12 and comparative example 1~9 are prepared.
(1) anti-dandruff effect
Above-described embodiment 1~12 and the shampoo of comparative example 1~9, according to dandruff is how many and the selection of itching degree is slight,
Moderate, severe patient totally 1260 people, it is primary using " half a head test method(s) " hair washing in every 4 days, check dandruff is how many and scratches after hair washing 4 days
Itch degree, observes 5 hair washing situations altogether.It is effective: without visible furfur, no itch；It is effective: the accidental tiny furfur of root of hair, no itch；
Improve: the visible a small amount of tiny furfur of root of hair is felt to itch；Invalid: a large amount of tiny furfurs are felt to itch.As illustrated in chart 1, it and fills in
It is as shown in table 2 that table on probation carrys out overall merit its using effect, fills in table on probation after on probation and scores.It is every in grade form to use
It is best result that effect total score, which is 5 points: 5 points, is indicated very satisfied；4 points are preferably, to be relatively satisfied with；3 points are that can receive；3
Divide the following are the range that cannot receive, every using effect average situation is as shown in table 1:
Table 1
As can be known from Table 1, the embodiment of the present invention 1~12 and 6 shampoo of comparative example have slight, moderate, severe patient
Good anti-dandruff and itching-relieving effect, in the anti-dandruff plant composition in comparative example 1~3 compared with Example 1, lacked frutus cnidii,
Fractions in camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed, and as can be known from the results,
Compared with Example 1, significant effect declines anti-dandruff effect；Anti-dandruff plant composition in comparative example 4~5 compared with Example 1,
It is compounded using ginkgo leaf, cacumen biotae, hundred steps, Radix Astragali, the fruit of summer cypress and Siberian cocklebur subconstiuent instead of fractions of the present invention,
And as can be known from the results, effect is not so good as the present invention, it is known that, frutus cnidii of the invention, camellia seed, ginger, purslane, wrinkled giant hyssop,
Wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed are compounded, and have anti-dandruff synergistic function.
Comparative example 7 is in no addition anti-dandruff component.In 75 test crowds, anti-dandruff group of natural plants is being added to
2% antipruritic effect suitable with 1%ZPT group effect is very poor.Illustrate this with anti-dandruff group of plant contained by plant can be anti-dandruff at related, separately
Outside, in comparative example 7 in severe patient group, effect do not contain anti-dandruff group of plant it is good, this may be due to test before some patientss
The reason to develop drug resistance after the shampoo containing ZPT is used for a long time.What is particularly worth mentioning is that user is generally reflected
ZPT group shampoo feels that degreasing power is too strong after washing, and hair and scalp sensation of dryness are prominent, and have apparent stimulation to eyes when flushing
Effect, and there is no these feelings for the shampoo of plant debris group, it was demonstrated that anti-dandruff group of plant, milder more safer than ZPT group.
The result of comparative example 8~9 it is found that with anti-dandruff plant society content in shampoo increase, anti-dandruff effect
Also increase, when the additive amount of anti-dandruff plant composition is greater than 2%, anti-dandruff significant effect, when the addition of anti-dandruff plant composition
When amount is greater than 8%, anti-dandruff effect increase is unobvious, therefore, when the additive amount of anti-dandruff plant composition is 2~8%, anti-dandruff effect
Fruit is significant.
2 embodiment 1~12 of table and the shampoo items using effect average situation of comparative example 6~7
| Group | Oil-control | Foaming abundancy degree | Irritation | Cleaning | It is submissive |
| Embodiment 1 | 4.95 | 4.98 | 5.00 | 4.97 | 4.97 |
| Embodiment 2 | 4.85 | 4.83 | 4.98 | 4.87 | 4.90 |
| Embodiment 3 | 4.90 | 4.85 | 4.93 | 4.83 | 4.87 |
| Embodiment 4 | 4.95 | 4.92 | 4.99 | 4.95 | 4.92 |
| Embodiment 5 | 4.94 | 4.93 | 4.99 | 4.95 | 4.93 |
| Embodiment 6 | 4.80 | 4.82 | 4.95 | 4.87 | 4.80 |
| Embodiment 7 | 4.93 | 4.97 | 5.00 | 4.95 | 4.93 |
| Embodiment 8 | 4.95 | 4.97 | 5.00 | 4.95 | 4.97 |
| Embodiment 9 | 4.93 | 4.97 | 4.99 | 4.98 | 4.91 |
| Embodiment 10 | 4.90 | 4.86 | 4.98 | 4.95 | 4.92 |
| Embodiment 11 | 4.89 | 4.87 | 5.00 | 4.96 | 4.91 |
| Embodiment 12 | 4.91 | 4.78 | 5.00 | 4.96 | 4.92 |
| Comparative example 6 | 4.65 | 4.97 | 4.69 | 4.97 | 4.95 |
| Comparative example 7 | 4.66 | 4.80 | 4.90 | 4.90 | 4.89 |
From table 2 it can be seen that with comparative example 6~7, the shampoo of embodiment 1~12 show as it is non-stimulated, preferably
Cleannes, flexibility show that shampoo of the present invention has preferable conditioning effect to hair, while showing preferable oil-control effect
Fruit illustrates that the plant dandruff control shampoo containing of the present invention containing plant anti-dandruff and itching-relieving agent has preferable oil-control effect and is substantially better than not
Containing the anti-dandruff shampoo of plant, and embodiment 1 is best.
(2) Physico-chemical tests are carried out to the shampoo of embodiment 1~12 and comparative example 1~9, gained Testing index is as follows:
(1) pH value detects
To embodiment 1~12 and the hair washing water sampling of comparative example 1~9, measured with pH meter, measure pH value be 6.0~
6.5。
(2) viscosity number detects
To embodiment 1~12 and the hair washing water sampling of comparative example 1~9, is measured with viscosimeter, measure viscosity number 10000
~16000.
(3) Detection of Stability
It to embodiment 1~12 and the hair washing water sampling of comparative example 1~9, is encapsulated in transparence cosmetic bottle, respectively
Be placed in quartz lamp illumination, -15 DEG C, 5 DEG C, 25 DEG C, under 48 DEG C of experiment conditions, to appearance, fragrance, pH value, viscosity and other
Mesh carries out 3 months by a definite date continuance tests, sees whether bleed, layering, separation, precipitating, discoloration, peculiar smell, demulsification etc. occur no
Good phenomenon, testing result show that the above bad result does not appear in test process, illustrate that it has good stability.
(4) centrifugation detection
Described in embodiment 1~12 and comparative example 1~9 sample, be encapsulated in centrifuge tube under 3000r/min from
30min sees whether that dispersion component, testing result do not show not dispersion component do not occur for appearance, illustrate that its Combination is good
It is good.
(5) stimulation anaphylaxis detects
To embodiment 1~12 and the hair washing water sampling of comparative example 1~9, it is 18-58 that it is applied to 60 age brackets in right amount
On volunteer's neck in year, 30min is observed, sees whether it phenomena such as redness, dermexanthesis, blistering occurs, observation indicate that,
All volunteers do not occur above-mentioned ill symptoms in 30min, illustrate that this product will not lead to the problem of stimulation and anaphylaxis to skin.
(3) bacteriostatic experiment
Activated Malassezia furfur is configured to bacteria suspension (4 × 105CFU/mL), 0.3mL is taken to be applied to
10min is placed on Leeming&Notman culture medium flat plate, flat plate cover is opened in aseptic superclean bench, is dried up with sterile wind
Plate (about 20min).4 Oxford cups are placed in each plate, 1 negative control (being free of test sample) Oxford cup, other three
100 μ L samples to be tested of a instillation.Oxford cup is gently pressed with aseptic nipper, so that it is close to planar surface, covers plate, set 30 DEG C of constant temperature
It is inverted culture 7 days in incubator, measures the diameter of inhibition zone, calculates average value, compares research.Antibacterial circle diameter is less than
8mm be it is invalid, otherwise to be effective, 3 times repetition test have bacteriostasis result person, be judged to qualification.Negative control group is without antibacterial
Ring generates, and otherwise test data is invalid.Bacteriostatic experiment is carried out to Chinese medicine in table 3, the results are shown in Table 3:
Table 3
As can be known from Table 3, frutus cnidii, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri, lopseed suppression
Bacterium effect is preferable, and the present invention has chosen this 9 kinds of Chinese medicine compoundings, and carries out antibacterial reality to embodiment 1~12 and comparative example 1~5
It tests, experimental result is as shown in table 4:
Table 4
| Group | Antibacterial circle diameter (mm) |
| Embodiment 1 | 24.6±0.3 |
| Embodiment 2 | 20.3±0.5 |
| Embodiment 3 | 21.0±0.2 |
| Embodiment 4 | 23.1±0.1 |
| Embodiment 5 | 23.5±0.4 |
| Embodiment 6 | 21.8±0.6 |
| Embodiment 7 | 22.5±0.4 |
| Embodiment 8 | 23.1±0.3 |
| Embodiment 9 | 23.9±0.6 |
| Embodiment 10 | 23.0±0.4 |
| Embodiment 11 | 21.6±0.2 |
| Embodiment 12 | 24.3±0.1 |
| Comparative example 1 | 15.8±0.5 |
| Comparative example 2 | 14.9±0.7 |
| Comparative example 3 | 15.2±0.6 |
| Comparative example 4 | 13.9±0.4 |
| Comparative example 5 | 14.7±0.3 |
As can be seen from Table 4, the good antimicrobial effect of the embodiment of the present invention 1~12, wherein when frutus cnidii, camellia seed, ginger, horse
Bitterroot, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri, lopseed according to mass ratio be 10:8:10:4:6:10:8:5:3 when, obtain most
Big antibacterial circle diameter is 24.6mm.In anti-dandruff plant composition in comparative example 1~3 compared with Example 1, cnidium monnieri has been lacked
Fractions in son, camellia seed, ginger, purslane, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed, and as can be known from the results,
Its fungistatic effect is not so good as embodiment 1；Anti-dandruff plant composition in comparative example 4~5 compared with Example 1, use ginkgo leaf,
Cacumen biotae, hundred steps, Radix Astragali, the fruit of summer cypress and Siberian cocklebur subconstiuent are compounded instead of fractions of the present invention, and as can be known from the results,
Its fungistatic effect is not so good as the present invention, it is known that, when using frutus cnidii of the invention, camellia seed, ginger, purslane, wrinkled giant hyssop, mother chrysanthemum
Flower, rheum officinale, Cortex Phellodendri and lopseed are compounded, and have antibacterial synergistic function.
(4) anti-dandruff contrast test
The age is chosen between 18 years old to 30 years old and by 30 volunteers that dandruff perplexs, every group of 10 people, selection implementation
1 shampoo of example and 6~7 shampoo of comparative example compare anti-dandruff effect, are used continuously one month using shampoo, and use three weekly
Secondary, then to using preceding and rear dandruff being used to weigh, statistical average variance is simultaneously analyzed.Wherein sample 1: embodiment
1；Sample 2: comparative example 6；Sample 3: comparative example 7.Experimental result is as shown in Figure 1:
It can be seen from figure 1 that the control of dandruff has extraordinary effect after applying plant desquamation compositions.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent substitution, improvement and etc. done be should be included within the scope of the present invention.
Claims (10)
1. a kind of anti-dandruff plant composition, which is characterized in that including following components: frutus cnidii, camellia seed, ginger, purslane, the leaves of pulse plants
Perfume, wild chrysanthemum, rheum officinale, Cortex Phellodendri and lopseed.
2. anti-dandruff plant composition according to claim 1, which is characterized in that the frutus cnidii, camellia seed, ginger, horse
Bitterroot, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild
Chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=5~20:5~15:3~10:2~5:3~8:5~20:5~15:3~10:2~5.
3. anti-dandruff plant composition according to claim 2, which is characterized in that the frutus cnidii, camellia seed, ginger, horse
Bitterroot, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild
Chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=10:8~12:5~10:3~4:5~6:10:6~10:5:3.
4. anti-dandruff plant composition according to claim 3, which is characterized in that the frutus cnidii, camellia seed, ginger, horse
Bitterroot, wrinkled giant hyssop, wild chrysanthemum, rheum officinale, Cortex Phellodendri and the weight ratio of lopseed are frutus cnidii: camellia seed: ginger: purslane: wrinkled giant hyssop: wild
Chrysanthemum: rheum officinale: Cortex Phellodendri: lopseed=10:8:10:4:6:10:8:5:3.
5. preparing the application in hair care product to 4 any anti-dandruff plant compositions according to claim 1.
6. a kind of hair care product containing plant composition anti-dandruff as described in any one of Claims 1 to 4.
7. a kind of shampoo containing any anti-dandruff plant composition of Claims 1-4, which is characterized in that described anti-dandruff
Plant composition weight percent in shampoo is 2~8%.
8. shampoo according to claim 7, which is characterized in that anti-dandruff plant composition weight percent in shampoo
Than being 4%.
9. according to the shampoo of claim 7 or 8, which is characterized in that the shampoo further include conditioner 0.5~10%,
Thickener 1~6%, aromatic 0.1~0.5%, surfactant 12~25%, pearling agent 0.5~3%, tax ester agent 0.5~
6%, the deionized water of cosolvent 1~5%, preservative 0.1~0.2%, chelating agent 0.05~0.1% and surplus.
10. shampoo according to claim 9, which is characterized in that including following components in percentage by weight: laureth
Ammonium sulfate 12%, ammonium lauryl sulfate 5%, Coconut Fatty Acid Monoethanolamide 1%, Cocoamidopropyl betaine 3%, 1.5%
Coconut oleoyl amine DEA, Polyquaternium-10 0.1%, guar hydroxypropyltrimonium ammonium chloride 0.1%, polydimethyl siloxane fluid
2.5%, lanolin 0.2%, jojoba oil PEG-150 esters 0.6%, linseed oil 0.3%, ethylene glycol double stearate 1.4%,
Glycerol 1.5%, 1618 alcohol 2.0%, anti-dandruff plant composition 4%, preservative 0.1%, 0.05% chelating agent, aromatic 0.4%
With the deionized water of surplus.
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