CN101669892B - Arborvitae mask and preparation method thereof - Google Patents

Arborvitae mask and preparation method thereof Download PDF

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Publication number
CN101669892B
CN101669892B CN2009101927790A CN200910192779A CN101669892B CN 101669892 B CN101669892 B CN 101669892B CN 2009101927790 A CN2009101927790 A CN 2009101927790A CN 200910192779 A CN200910192779 A CN 200910192779A CN 101669892 B CN101669892 B CN 101669892B
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cacumen platycladi
arborvitae
timber
mask
oil
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CN101669892A (en
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苏薇薇
雷华平
王永刚
李沛波
彭维
杨翠平
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Guangdong Hongtu Biotechnology Co ltd
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Sun Yat Sen University
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Abstract

The invention discloses an arborvitae extract mask and preparation method thereof. The traditional Chinese medicine mask in the invention adopts arborvitae extract as main active ingredient, the mask is formed by the step that arborvitae extract, water, glycerol and emulsifier are mixed to be uniform and then are immersed into mask paper made of non-woven fabrics; wherein the arborvitae extract includes arborvitae oil and arborvitae water extract, the arborvitae oil is obtained by adopting super supercritical carbon dioxide extraction or organic solvent extraction, and the arborvitae water extract is obtained by the step that the arborvitae after oil extraction is added with water to be decocted and extracted and then is filtered and concentrated. The mask of the invention has the effects of cleaning, whitening skin, removing beverage and moisturizing as well as promoting face blood circulation and nourishing face skin.

Description

A kind of arborvitae mask and preparation method thereof
Technical field
The invention belongs to the cosmetics technical field, be specifically related to a kind of arborvitae mask and technology of preparing thereof.
Background technology
Facial film is one of cosmetics of bringing into use very early, and its effect is to be coated on the skin of face, through behind the certain hour, after this film taken off or wash off, can reach the purpose of clean skin, skin protection and beauty treatment.Along with growth in the living standard, people also constantly increase the demand of various facial films.The facial film of various functions can allow skin well be nursed, as clean, preserve moisture, whiten, speckle dispelling and nutrition or the like.Everyone can find corresponding facial film at the skin situation of oneself.The facial film that one opening and closing are suitable can help improve facial skin.
Along with the raising that science and technology development and people require operational maintenance, the plant extract that the manufacturer begins to have certain effect prepares the skin care item that satisfy people's requirement.Arborvitae extract has multiple aesthetic health care function.The difference of extraction process, the effective ingredient in the arborvitae extract are also different, thereby the effect that it had is also different.The contained oils composition of Cacumen Platycladi timber has blood circulation promoting, promotes cell metabolism and effects such as cell regeneration, calmness and blood pressure lowering that contain flavone compound etc. in addition, water extract then has effects such as speckle dispelling, blood circulation promoting and antioxidation.Arborvitae mask that forms through scientific matching with compositions such as Cacumen Platycladi timber oil and water extract and deionized waters and preparation method thereof at home and abroad is not reported, and still belongs to blank.
Summary of the invention
It is main effective ingredient that the technical problem to be solved in the present invention provides a kind of employing Cacumen Platycladi extract, the facial film that the convenience that is prepared from is easy-to-use.
The technical scheme that the present invention addresses the above problem is:
A kind of Cacumen Platycladi extract that adopts is the Chinese medicine facial film of main effective ingredient, and this facial film immerses the fabric face paper of nonwoven after by mix homogeneously such as Cacumen Platycladi extract, water, glycerol, emulsifying agents and forms; Wherein, described Cacumen Platycladi is carried thing and is divided into Cacumen Platycladi timber oil and Cacumen Platycladi water extract, Cacumen Platycladi timber is oily for adopting supercritical carbon dioxide extraction or adopting organic solvent extraction to obtain, and Cacumen Platycladi timber water extract obtains for decocting with water extraction and filtering and concentrating through the Cacumen Platycladi timber behind the extraction oil.The concrete extracting mode of Cacumen Platycladi timber oil is: can adopt supercritical carbon dioxide extraction, get Cacumen Platycladi wooden shavings, pulverizing, use supercritical carbon dioxide extraction, extracting pressure 8~20MPa, 30~60 ℃ of extraction temperature are resolved pressure 4~8MPa, 35~75 ℃ of resolution temperatures, collect the extract anhydrous sodium sulfate dehydration, get Cacumen Platycladi timber oil; Also can adopt organic solvent extraction, get Cacumen Platycladi wooden shavings, pulverizing, add 2~30 times of volume organic solvents, this organic solvent can be petroleum ether, gasoline or ethyl acetate, extract 1~5 time, and each 1 day to 7 days, reclaim solvent, promptly obtain Cacumen Platycladi timber oil.Wherein the optimization technology of supercritical carbon dioxide extraction is used supercritical carbon dioxide extraction, extracting pressure 15MPa for getting Cacumen Platycladi wooden shavings, pulverizing, 35 ℃ of extraction temperature are resolved pressure 8MPa, 40 ℃ of resolution temperatures, collect the extract anhydrous sodium sulfate dehydration, get Cacumen Platycladi timber oil; The optimization technology of organic solvent extraction is, gets Cacumen Platycladi wooden shavings, pulverizing, adds 10 times of amount petroleum ether (60~90 ℃), extract 3 times, and each 2 days, the recovery solvent promptly obtained Cacumen Platycladi timber oil.
Cacumen Platycladi water extraction detailed process: the wood shavings of learning from else's experience, pulverizing and supercritical carbon dioxide extraction or organic solvent extraction rear side Cupressus funebris Endl. material, add entry with the ratio of material liquid volume than 1: 2~1: 30, decoct and extracted 10 minutes~2 hours, filter, filtering residue repeats to decoct 1 time, merging filtrate concentrates, and being concentrated into density is 1.05~1.10g/ml, gets the Cacumen Platycladi water extract.Through optimum experimental, its preferred extraction process is the wood shavings of learning from else's experience, pulverizing and supercritical carbon dioxide extraction or organic solvent extraction rear side Cupressus funebris Endl. material, add entry with the ratio of material liquid volume than 1: 10, decoct and extracted 0.5 hour, filter, filtering residue repeats to decoct 1 time, and merging filtrate concentrates, being concentrated into density is 1.10g/ml, gets the Cacumen Platycladi water extract.
In above-mentioned arborvitae mask, the weight proportion of active component and auxiliary agent thereof is as follows: Cacumen Platycladi timber oil 0.1~0.5%; Cacumen Platycladi water extract 2~20%; Glycerol 2~6%; Propylene glycol 2~6%; Lauric acid polyoxyethylene (7) ester 0.5~2%; Sodium alginate 0.5~3.5%; Germall B 0.5~2%; Deionized water 60~92.4%.Its optimization formula is: Cacumen Platycladi timber oil 0.3%; Cacumen Platycladi water extract 10%; Glycerol 3%; Propylene glycol 3%; Lauric acid polyoxyethylene (7) ester 1%; Sodium alginate 1%; Germall B 1%; Deionized water 80.7%.Concrete preparation process: get glycerol, add propylene glycol, Cacumen Platycladi timber oil and lauric acid polyoxyethylene (7) ester, stirring and evenly mixing; Get sodium alginate and be dissolved in the deionized water, add the Cacumen Platycladi water extract, stirring and evenly mixing adds mixture such as above-mentioned glycerol then while stirring; After stirring, add germall B again, stir; Soak in the mixed solution that the non-woven fabrics Face film towel is obtained at last and put imbibition, take out, packing, promptly.
Compared with prior art, the present invention has following beneficial effect: the active component of facial film of the present invention is Cacumen Platycladi timber oil and Cacumen Platycladi timber water extract.Facial film of the present invention has cleaning, whitens, speckle dispelling, the effect of preserving moisture and promoting facial blood circulation, nutrition face skin.Reach lasting moisturizing skin, it is tender smooth that skin is moistened; Also contain flavone compound in the water extract, have antioxidation and absorb action of ultraviolet radiation, can be played the skin whitening effect by skin absorbs; Cacumen Platycladi timber oil has multiple volatile oil component, can percutaneous osmosis be absorbed by human body, and blood circulation promoting and new diligent metabolism can be promoted the growth of skin cell, nutrition and gloss skin, and the effect of wrinkle resistant, cold resistant and ultraviolet radiation preventing is arranged.
The specific embodiment
Embodiment 1 gets 1kg Cacumen Platycladi timber, and supercritical carbon dioxide extraction is used in wood shavings, pulverizing, extracting pressure 15MPa, and 35 ℃ of extraction temperature are resolved pressure 8MPa, and 40 ℃ of resolution temperatures are collected the extract anhydrous sodium sulfate dehydration, get Cacumen Platycladi timber oil.
Embodiment 2 gets 1kg Cacumen Platycladi timber, and wood shavings, pulverizing add 10 times of volume petroleum ether, and 70 ℃, extract 3 times, each 2 days, reclaim solvent, promptly obtain Cacumen Platycladi timber oil.
Embodiment 3 gets the Cacumen Platycladi timber 1kg after embodiment 1 or embodiment 2 carry oil, adds entry with 1: 10 ratio of solid-liquid ratio, decocts and extracts 0.5 hour, filters, and filtering residue repeats to decoct 1 time, and merging filtrate concentrates, and being concentrated into density is 1.10g/ml, the Cacumen Platycladi water extract.
Embodiment 4 gets embodiment 1 obtained Cacumen Platycladi timber oil, by weight Cacumen Platycladi timber oil 0.3%, Cacumen Platycladi water extract 10% (embodiment 3), glycerol 3%, propylene glycol 3%, lauric acid polyoxyethylene (7) ester 1%, sodium alginate 1%, germall B 1%, deionized water 80.7% proportional sampling.Get glycerol earlier, add propylene glycol, Cacumen Platycladi timber oil and lauric acid polyoxyethylene (7) ester, stirring and evenly mixing; Get sodium alginate and be dissolved in the deionized water, add the Cacumen Platycladi water extract, stirring and evenly mixing adds mixture such as above-mentioned glycerol then while stirring; After stirring, add germall B again, stir; Soak in the mixed solution that the non-woven fabrics Face film towel is obtained at last and put imbibition, take out, packing, promptly.
Embodiment 5 gets embodiment 2 obtained Cacumen Platycladi timber oil, by Cacumen Platycladi timber oil 0.3%, Cacumen Platycladi water extract 10% (embodiment 3), glycerol 3%, propylene glycol 3%, lauric acid polyoxyethylene (7) ester 1%, sodium alginate 1%, germall B 1%, deionized water 80.7% proportional sampling.Get glycerol earlier, add propylene glycol, Cacumen Platycladi timber oil and lauric acid polyoxyethylene (7) ester, stirring and evenly mixing; Get sodium alginate and be dissolved in the deionized water, add the Cacumen Platycladi water extract, stirring and evenly mixing adds mixture such as above-mentioned glycerol then while stirring; After stirring, add germall B again, stir; Soak in the mixed solution that the non-woven fabrics Face film towel is obtained at last and put imbibition, take out, packing, promptly.
Embodiment 6 human body proof tests
1. test material embodiment 4, embodiment 5 described facial films.
2. test crowd's age is between 18~50 one full year of life, has obviously person of skin dark stain or acne, dark complexion tarnish, is divided into two groups and experimentizes.
3. test method is got facial film, after clear water is washed one's face facial film is spread on the face, takes down the clean face of clear water behind 10min~15 minute; Used once in per three days, and all do not adopt other cosmetics between the operating period, be one month service time.
Result of the test the results are shown in Table 1 with table 2, participating in the test people uses rear face skin little red, promptly recover original-pack in 10~30 minutes after stopping using, there are not obvious anaphylaxis or other irritative response, illustrate after this face skin uses the effect that promotes facial blood circulation is arranged, use the rear face turgor continuously, moist glossy, spot is improved.
Table 1 adopts embodiment 4 facial film human body result on trial
Figure G2009101927790D00061
Table 2 adopts embodiment 5 facial film human body result on trial
Figure G2009101927790D00062

Claims (9)

1. arborvitae mask is characterized in that being made up of the component of following percetage by weight:
Cacumen Platycladi timber oil 0.1~0.5% Cacumen Platycladi timber water extract 2~20%
Surplus is an auxiliary agent;
Described Cacumen Platycladi timber is oily for adopting supercritical carbon dioxide extraction or adopting the organic solvent extraction Cacumen Platycladi to obtain, and described Cacumen Platycladi timber water extract obtains for decocting with water extraction and filtering and concentrating through the Cacumen Platycladi timber behind the extraction oil.
2. arborvitae mask as claimed in claim 1 is characterized in that being made by the component of following percetage by weight: Cacumen Platycladi timber oil 0.1~0.5%; Cacumen Platycladi timber water extract 2~20%; Glycerol 2~6%; Propylene glycol 2~6%; Lauric acid polyoxyethylene (7) ester 0.5~2%; Sodium alginate 0.5~3.5%; Germall B 0.5~2%; Deionized water 60~92.4%.
3. arborvitae mask as claimed in claim 1 is characterized in that being made by the component of following percetage by weight: Cacumen Platycladi timber oil 0.3%; Cacumen Platycladi timber water extract 10%; Glycerol 3%; Propylene glycol 3%; Lauric acid polyoxyethylene (7) ester 1%; Sodium alginate 1%; Germall B 1%; Deionized water 80.7%.
4. arborvitae mask as claimed in claim 1, it is characterized in that described Cacumen Platycladi timber oil supercritical carbon dioxide extraction process is: get Cacumen Platycladi timber, wood shavings, pulverizing, use supercritical carbon dioxide extraction, extracting pressure 8~20MPa, 30~60 ℃ of extraction temperature, resolve pressure 4~8MPa, 35~75 ℃ of resolution temperatures are collected the extract anhydrous sodium sulfate dehydration, get Cacumen Platycladi timber oil.
5. arborvitae mask as claimed in claim 1 is characterized in that described Cacumen Platycladi timber oil organic solvent extraction process is: get Cacumen Platycladi wooden shavings, pulverizing, add the organic solvent of 2~30 times of volumes, extract 1~5 time, reclaim solvent, promptly obtain Cacumen Platycladi timber oil.
6. arborvitae mask as claimed in claim 5 is characterized in that described organic solvent is petroleum ether, gasoline or ethyl acetate.
7. arborvitae mask as claimed in claim 1, it is characterized in that described Cacumen Platycladi water extraction process is: Cacumen Platycladi timber is behind wood shavings, pulverizing and supercritical carbon dioxide extraction or organic solvent extraction, add entry with 1: 2~1: 30 volume ratio of solid-liquid ratio, decoct and extracted 10 minutes~2 hours, filter, filtering residue repeats to decoct 1 time, and merging filtrate concentrates, being concentrated into density is 1.05~1.10g/ml, gets the Cacumen Platycladi water extract.
8. arborvitae mask as claimed in claim 7, it is characterized in that described Cacumen Platycladi water extraction process is: Cacumen Platycladi timber is behind wood shavings, pulverizing and supercritical carbon dioxide extraction or organic solvent extraction, added entry than 1: 10 with material liquid volume, decoct and extracted 0.5 hour, filter, filtering residue repeats to decoct 1 time, and merging filtrate concentrates, being concentrated into density is 1.10g/ml, gets the Cacumen Platycladi water extract.
9. the preparation method of the described arborvitae mask of claim 2 is characterized in that this method comprises the steps: to get glycerol, adds propylene glycol, Cacumen Platycladi timber oil and lauric acid polyoxyethylene (7) ester, stirring and evenly mixing; Get sodium alginate and be dissolved in the deionized water, add the Cacumen Platycladi water extract, stirring and evenly mixing adds above-mentioned glycerol mixture then while stirring; After stirring, add germall B again, stir; Soak in the mixed solution that the non-woven fabrics Face film towel is obtained at last and put imbibition, take out, packing, promptly.
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CN102676292A (en) * 2012-06-02 2012-09-19 哈尔滨工业大学 Separation process of toad maggot essential oil
CN108158869B (en) * 2018-03-07 2021-04-30 四川桧元素生物科技有限公司 Antibacterial wet tissue liquid, wet tissue and preparation method of wet tissue
CN108186426B (en) * 2018-03-07 2021-03-26 四川桧元素生物科技有限公司 Antibacterial mask liquid, mask and preparation method of mask liquid
CN108186427B (en) * 2018-03-07 2021-06-11 四川桧元素生物科技有限公司 Antibacterial toner and preparation method thereof
CN109646370A (en) * 2018-12-10 2019-04-19 中山职业技术学院 A kind of preparation method of pure plant wood shavings water

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1478461A (en) * 2003-07-08 2004-03-03 昆明圣火制药有限责任公司 Twelve classic Chinese medicine pack and its preparation process
JP2005179226A (en) * 2003-12-18 2005-07-07 Shiseido Co Ltd Method for extracting skin-whitening ingredient from hakushinin
CN101254156A (en) * 2007-03-01 2008-09-03 段亚东 Cosmetic composition and uses thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1478461A (en) * 2003-07-08 2004-03-03 昆明圣火制药有限责任公司 Twelve classic Chinese medicine pack and its preparation process
JP2005179226A (en) * 2003-12-18 2005-07-07 Shiseido Co Ltd Method for extracting skin-whitening ingredient from hakushinin
CN101254156A (en) * 2007-03-01 2008-09-03 段亚东 Cosmetic composition and uses thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
詹永等.中药化妆品的研发思路与申报.《重庆中草药研究》.2007,(第2期),50-54,64. *
赵红兰.中药倒模面膜治疗痤疮、黄褐斑、扁平疣216 例疗效观察.《临床医药实践杂志》.2007,第16卷(第1期),54-55. *

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