CN105769683A - Anti-oxidation moisturizing sleeping mask containing peony seed oil and preparation method thereof - Google Patents
Anti-oxidation moisturizing sleeping mask containing peony seed oil and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses an anti-oxidation moisturizing sleeping mask containing peony seed oil and a preparation method thereof.The sleeping mask is prepared from, by mass, 0.5%-20% of peony seed oil, 0.1%-5% of oil-soluble vitamin E, 0.1%-5% of an emulsifier, 1%-10% of rose hydrosol, 0.5%-20% of chamomile extract, 1%-10% of glycerin, 0.5%-3% of lower-molecular hyaluronic acid, 5%-15% of aloe gel, 0.05%-5% of an antibacterial agent and the balance deionized water.After peony seed oil, rose hydrosol, chamomile extract, aloe gel, lower-molecular hyaluronic acid and other substances are mixed, the sleeping mask suitable for modern women is formed; the sleeping mask has the advantage of being free of washing, and thus use is quite convenient.With natural substances serving as main raw materials, the mask has the advantages of being mild without irritation and easy to absorb and is high in moisturizing performance and good in anti-oxidation effect; after the mask is used, the skin is smooth and fine, moist and compact, crystal clear and full of vitality.
Description
Technical field
The invention belongs to daily cosmetics technical field, relate to the cosmetic composition of a kind of antioxidation moisturizing, particularly relate to
A kind of antioxidation moisturizing sleep mask containing peony seed oil and preparation method thereof.
Background technology
Modern female, in addition to nervous operating pressure, family's pressure, also to stand severe air ambient, and skin is easily
Hydropenia, aging, also easily cause acne and the generation of face skin allergy.Facial film is to utilize to cover of short duration in face
Time, be temporarily isolating the external world air and pollution, improve skin temperature, skin pore expansion, promote sweat gland secretion with
Metabolism, makes the oxygen content of skin rise, and beneficially skin gets rid of the metabolic product of epidermis cell and the oil of accumulation
Lipid material.Moisture in facial film penetrates into the horny layer of epidermis, and skin becomes soft, and skin light naturally is flexible.Sleep
After dormancy facial film refers to finish basis skin protection at night, sleep mask is applied a kind of facial film in directly sleep on the face.
Presently commercially available facial film is a feast for the eyes, is divided into whitening, moisturizing, cleaning, Sage Extract, anti-ageing according to different efficacies
Always, releive, compact facial film etc., but not only lead, hydrargyrum, benzene, phenol content overproof in most products, and can add
Substantial amounts of thickening agent, such as materials such as card ripple, triethanolamine, sodium acrylate/sodium acryloyldimethyl taurate copolymers,
And EDTA chelating agen and containing the preservative of Form aldehyde release body, although can temporarily make skin present glossy soft state, but
It is thinning to be that life-time service can make horny layer come off, and causes red swelling of the skin, forms mottle, is unfavorable for skin health.And it is natural
Plant facial film is because of its more and more welcomed by the people green, natural, safe, harmless.
CN103330671A discloses a kind of sleep mask, and this facial film is a kind of containing pansy extract, Fructus psidii guajavae immaturus extraction
The wink saturating granulation promoting water composition of thing and hydrolyzed pearl, said composition can allow skin in abundant moisturizing at night, open for skin
Percdation passage, supplement aminoacid, strengthening skin updating ability, breathe smooth and easy.But, this facial mask liquid is functional relatively
For single, it is difficult to help skin to relax and press, protection skin effectively resists extraneous pressure.
CN104706566A discloses a kind of Semen Fructus Chaenomelis wrinkle resistant sleep mask of oil, and described facial film is by Semen Fructus Chaenomelis oil, hyaluronic acid
Sodium, collagen protein, Radix Ginseng extract, glycyrrhizic acid dipotassium, glycerol, propylene glycol, Mel, vitamin, carbomer, three
Ethanolamine, ethylparaben and germall BP composition.By combining effect of facial film, the health care of Fructus Chaenomelis is melted
Enter wherein, but containing card ripple in its formula, life-time service the phenomenon of dermal toxicity easily occur, is unfavorable for skin health,
And the both effectiveness data of this facial film are the weakest.
Peony seed oil selects the high-quality seed of Flos Moutan of ecosystem to be raw material, uses pure physics cold pressing process to refine and forms, maximum
The natural active matter composition remained in peony seed oil of limit.By retrieving domestic and international prior art, the most not yet send out
Peony seed oil is now utilized to prepare the document report of sleep mask, the more needleless efficacy detection to this facial film.
Summary of the invention
In view of the deficiencies in the prior art, it is an object of the invention to provide a kind of be available for that modern female uses containing seed of Flos Moutan
Sleep mask of oil and preparation method thereof, blank to fill up peony seed oil use in prepared by facial film, solution air pollution,
The various skin problems that the reasons such as fatigue cause.
In order to realize the purpose of the present invention, inventor, by lot of experiments research persistent exploration, is finally obtained and contains as follows
There is an antioxidation moisturizing sleep mask technical scheme of peony seed oil:
A kind of antioxidation moisturizing sleep mask containing peony seed oil, this sleep mask is prepared from by following component: Paeonia suffruticosa
Seed oil, fat soluble vitamin E (Vitamin E, VE), emulsifying agent, MEIGUI CHUNLU, camomile extract, glycerol,
Low molecule hyaluronic acid, Aloe glue, antibacterial and deionized water composition.
Preferably, the antioxidation moisturizing sleep mask containing peony seed oil as above, the percent mass of the most each component
Content is: peony seed oil 0.5%-20%, fat soluble vitamin E 0.1%-5%, emulsifying agent 0.1%-5%, organic guarantor add
Leah MEIGUI CHUNLU 1%-10%, camomile extract 0.5%-20%, glycerol 1%-10%, low molecule hyaluronic acid 0.5%-3%,
Aloe glue 5%-15%, antibacterial 0.05%-5%, surplus is deionized water.
It is further preferred that contain the antioxidation moisturizing sleep mask of peony seed oil, the matter of the most each component as above
Amount percentage composition is: peony seed oil 0.6%-6%, fat soluble vitamin E 0.5%-0.6%, emulsifying agent 0.1%, You Jibao
Add Leah MEIGUI CHUNLU 2%, camomile extract 1%, glycerol 4%, low molecule hyaluronic acid 0.8%, Aloe glue 6%,
Antibacterial 0.2%, surplus is deionized water.
The most preferably, the antioxidation moisturizing sleep mask containing peony seed oil as above, emulsifying agent therein
In cetearyl alcohol, lauryl alcohol phosphate ester, C9-15 alcohol phosphate ester, stearyl alcohol phosphate ester and C20-22 alcohol phosphate ester
At least one.
The most preferably, the antioxidation moisturizing sleep mask containing peony seed oil as above, Flos Matricariae chamomillae therein
Extract is prepared as follows forming: takes Flos Matricariae chamomillae and adds in extraction kettle, is passed through carbon dioxide with 30-50L/h flow velocity,
By 1-2L/h speed add volumetric concentration be the ethanol of 75%-80%, temperature remain 40-60 DEG C, pressure be 10-15
2-3h is extracted under conditions of MPa；Obtain Flos Matricariae chamomillae ORGANIC SOLVENT MIXTURES；Put it in decompression low-temperature concentration equipment again,
It is depressurized to-0.05-0.05MPa, under the conditions of 45-55 DEG C, reclaims organic solvent, obtain camomile extract.
The most preferably, the antioxidation moisturizing sleep mask containing peony seed oil as above, antibacterial therein
For Compositional antiseptic agent: caprylyl glycol and pentanediol are allocated than 1:4 as compounding.Caprylyl glycol is a kind of plant antimicrobial, belongs to
In the end group glycol of middle short carbon chain, compounding with pentanediol use, can effectively suppress growing of antibacterial and mycete in facial film.
It addition, present invention also offers the preparation method of a kind of above-mentioned antioxidation moisturizing sleep mask containing peony seed oil,
The method comprises the steps:
1) add the peony seed oil of recipe quantity, fat soluble vitamin E and emulsifying agent in a reservoir, stir, be denoted as molten
Liquid I, standby；
2) in another container, deionized water, MEIGUI CHUNLU, camomile extract, glycerol, Aloe glue and low point are added
Sub-hyaluronic acid, stirs, and is denoted as solution II, standby；
3) solution II of the 10%-15% taking full dose adds in solution I, stirs 4-5min, after causing flocculence material occurs,
Add 20%-25% solution II, continue stirring 4-5min, cream molding, add remaining solution II, continue stirring all
Even, standby；
4) in step 3) gained cream adds antibacterial, i.e. obtain sleep mask after stirring.
Find according to antioxygenic property experimental study, contain the sample 2 of 0.6% peony seed oil and 0.6%VE simultaneously
Non-oxidizability be significantly higher than and add 0.6% peony seed oil without the sample 3 of VE, and be significantly higher than only interpolation
0.6%VE is without the sample 4 of peony seed oil, and peony seed oil and being used in combination of VE are had in skin care item by this explanation
The collaborative effect removing skin histology excessive free radicals.Therefore, present invention also offers and newly should associated with two kinds of specific components
With, it may be assumed that peony seed oil and fat soluble vitamin E be answering in the skin care item of excessive free radicals in skin histology is removed in preparation
With；Or the application that peony seed oil and fat soluble vitamin E are in preparation non-oxidizability skin care item.It is further preferred that
Described skin care item are peony seed oil sleep mask, and wherein peony seed oil with the weight ratio of fat soluble vitamin E is
0.5-10:1, preferably 0.8-2:1.
The antioxidation moisturizing sleep mask that the present invention relates to has the advantages that peony seed oil, MEIGUI CHUNLU, ocean
The materials such as Flos Chrysanthemi extract, Aloe glue, low molecule hyaluronic acid are prepared as the sleep mask of a kind of suitable for modern women, permissible
It is effectively improved the oxidation resistance of skin, and injects sufficient moisture for skin, prevent the moisture in keratodermatitis from evaporating,
The plant essence making load is prone to absorb, and keeps face to moisten, it is to avoid face skin accelerated ageing, reduces facial wrinkles,
There is the effect of preferable antioxidation, slow down aging.It addition, another advantage of sleep mask that the present invention provides is disposable,
Very easy to use, to no skin irritation, life-time service does not haves the phenomenon of dermal toxicity, is a kind of healthy, many
The sleep mask of function, is conducive to large-scale production and the sale of this facial mask liquid.
Accompanying drawing explanation
The moisturizing rate curve chart of the antioxidation moisturizing sleep mask of Fig. 1: embodiment 2 preparation；
The sleep mask DPPH clearance rate effect contrast figure of Fig. 2: different disposal；Wherein: 1 is 6% peony seed oil+0.6%VE
Process group；2 is 0.6% peony seed oil+0.6%VE process group；3 is 0.6% peony seed oil process group；4 is 0.6%VE process
Group；Letter represents the difference analysis result on the significance level of 5%, shows without notable containing same letter between process
Sex differernce, shows to there is significant difference without same letter.
Detailed description of the invention
The present invention is only further illustrated by the following examples, limits the present invention never in any form.The embodiment of the present invention
The organic MEIGUI CHUNLU of Bulgaria that MEIGUI CHUNLU used by is commercially available, Flos Rosae Rugosae quintessence oil content is 0.05%；In embodiment
The part by weight of the raw material being previously mentioned can make the appropriate adjustments.
Embodiment 1: the preparation of camomile extract
Taking Flos Matricariae chamomillae to add in extraction kettle, be passed through carbon dioxide with 30L/h flow velocity, adding volumetric concentration by 1L/h is 75%
Ethanol, temperature remain 40 DEG C, pressure be 10MPa under conditions of extract 2h；Extract is put into pillar separate
Still separates, obtains Flos Matricariae chamomillae ORGANIC SOLVENT MIXTURES；Put it into again in decompression low-temperature concentration equipment, be depressurized to 0.01
MPa, reclaims organic solvent under the conditions of 50 DEG C, obtains camomile extract.
Embodiment 2: the preparation of antioxidation moisturizing sleep mask
A kind of antioxidation moisturizing sleep mask containing peony seed oil, its component and the weight percentage of each component thereof are such as
Under:
Preparation method is as follows:
1) carry out vessel sterilization with the ethanol of 75%, or carry out disinfection with ultraviolet irradiation 30min；
2) in the beaker of 100mL, peony seed oil 6g, fat soluble vitamin E 0.5g, lauryl alcohol phosphate ester 1g are added,
Stir, be denoted as solution I, standby；
3) in another beaker, deionized water 78.5mL, organic Bulgarian Rose hydrosol 2g, camomile extract are added
1g, glycerol 4g, Aloe glue 6g, low molecule hyaluronic acid 0.8g, stir, be denoted as solution II, standby；
4) take 10mL solution II and add in solution I, stir 4-5min, after causing flocculence material occurs, add 20mL
Solution II, continues stirring 5min, cream basic forming, adds remaining solution II, continue to stir, standby；
5) in cream, add antibacterial 0.2mL, tank after stirring, can be entered.
Embodiment 3: the preparation of antioxidation moisturizing sleep mask
A kind of antioxidation moisturizing sleep mask containing peony seed oil, its component and the weight percentage of each component thereof are such as
Under:
After the part by weight of raw material makes the appropriate adjustments, prepare facial film according to embodiment 1 preparation method.
Embodiment 4: the preparation of antioxidation moisturizing sleep mask
A kind of antioxidation moisturizing sleep mask containing peony seed oil, its component and the weight percentage of each component thereof are such as
Under:
After the part by weight of raw material makes the appropriate adjustments, prepare facial film according to embodiment 1 preparation method.
Embodiment 5: product moisture retention determination test
Select the antioxidation moisturizing sleep mask of embodiment 2 preparation, and test its moisture retention.According to Deng Yiqing " 4 kinds of oceans
Shellfish polysaccharide extracts and moisture retention is studied " method in document, slightly modified, specific as follows: to use silica gel drier,
Ambient temperature is 20 DEG C.Taking sleep mask 1mL containing 6% peony seed oil to be placed in EP pipe, its quality of accurate weighing is remembered
Make H0, be placed in exsiccator, place 1,2,3,4,5,6,7, again weigh after 23h, be denoted as Hn, moisturizing rate
Computing formula is as follows: moisturizing rate (%)=Hn/H0In × 100% formula: H0For sample containing water quality, HnFor placing n h
Rear sample contains water quality.
Experimental result is added up as shown in Figure 1.It will be seen from figure 1 that the moisture retention of this kind of sleep mask is after 7h, still can
Enough reaching 99.7%, after 23h, moisturizing rate is also up to 98.5%, and moisture retention far above Kong Hexin etc., " protect by the moisture absorption of laminine
Moist and dynamics research " conventional wetting agent glycerol (moisturizing rate: 96%) and L-are bad in the skin care item mentioned in document
Propylhomoserin hydrochlorate (moisturizing rate: 87.6%).
Embodiment 6: product non-oxidizability determination test
Antioxidation moisturizing sleep mask prepared by prescription and technique according to embodiment 2, and tests its non-oxidizability.Consider
Facial film is made up of oil phase and aqueous phase two parts, thus add in test very small amount (0.6%) peony seed oil and without
VE is as processing 3 (using deionized water to replace VE and Paeonia suffruticosa seed oil, lower same)；Meanwhile, in order to detect 2 kinds of things
The contribution to non-oxidizability of the appropriate proportioning of matter, design adds 0.6% peony seed oil and 0.6%VE as processing 2, and 6%
Peony seed oil and 0.6%VE are as processing 1.With reference to " Antioxidative properties of xanthan on the such as Shimada
Autoxidation of soybean oil in cyclodextrin " method mentioned in document, slightly modified, specific as follows: to take
2mL sample solution adds in EP pipe, adds people 2mL 1mmol L-1DPPH ethanol solution, lucifuge is in dark at room temperature
Place's reaction 30min, observes the change of its color, determines have the ascorbic dense of identical antioxidation according to this color
Degree.Take 2mL vitamin c solution to add in EP pipe, add people 2mL 1mmol L-1DPPH ethanol solution；Take 2mL70%
Ethanol solution add in EP pipe, add people 2mL 1mmol L-1DPPH ethanol solution, lucifuge is at dark at room temperature
Reaction 30min, the ethanol solution using 70%, as blank, measures absorbance (A at 525nm525), it is denoted as respectively
ASampleAnd AComparison.Each concentration is repeated 3 times tests to ensure the accuracy of experimental result, finally averages as matching number
According to.DPPH clearance rate computing formula is as follows: DPPH clearance rate (%)=(1-ASample/AComparison)×100.Color is the most shallow, to DPPH
The clearance rate of free radical is the highest, and non-oxidizability is the strongest.
Experimental result is as shown in Figure 2.Result of the test according to Fig. 2 is it can be seen that add 0.6% peony seed oil and 0.6%VE
Non-oxidizability (81.6%) significance of (processing 2) is higher than only adding 0.6% peony seed oil without VE's (processing 3)
Non-oxidizability (53.4%), and it is significantly higher than the antioxidation only adding 0.6%VE without peony seed oil (processing 4)
Property (13.1%)；This shows that peony seed oil and VE enough carry out effective synergism, improves the facial film removing to free radical
Rate, strengthens non-oxidizability.Under the conditions of not changing VE content, when the addition of peony seed oil is increased to 6%, (process 1),
Its non-oxidizability improves further, and its antioxygen rate can also be up to 95.6%, and this will be for pure plant mask and plant antioxygen
The research and development of agent provide new clue and thinking.
Embodiment 7: product sensory is tested
Select the sleep mask containing 6% peony seed oil of embodiment 2 preparation, test its trial effect.This facial film is given
20 ages are on probation the Ms of 20 to 50 years old, it is stipulated that use 2 times weekly, fill in trial effect feedback form after 4w on probation.
Trial effect is added up such as following table:
Claims (10)
1. the antioxidation moisturizing sleep mask containing peony seed oil, it is characterised in that this sleep mask is prepared by following component
Form: peony seed oil, fat soluble vitamin E, emulsifying agent, MEIGUI CHUNLU, camomile extract, glycerol, low molecule glass are urinated
Acid, Aloe glue, antibacterial and deionized water composition.
Antioxidation moisturizing sleep mask containing peony seed oil the most according to claim 1, it is characterised in that this sleep
In facial film, the weight/mass percentage composition of each component is: peony seed oil 0.5%-20%, fat soluble vitamin E 0.1%-5%, emulsifying agent
0.1%-5%, organic Bulgarian Rose hydrosol 1%-10%, camomile extract 0.5%-20%, glycerol 1%-10%, low point
Sub-hyaluronic acid 0.5%-3%, Aloe glue 5%-15%, antibacterial 0.05%-5%, surplus is deionized water.
Antioxidation moisturizing sleep mask containing peony seed oil the most according to claim 2, it is characterised in that this sleep
In facial film, the weight/mass percentage composition of each component is: peony seed oil 0.6%-6%, fat soluble vitamin E 0.5%-0.6%, emulsifying agent
1%, MEIGUI CHUNLU 2%, camomile extract 1%, glycerol 4%, low molecule hyaluronic acid 0.8%, Aloe glue 6%, antibacterial
0.2%, surplus is deionized water.
4. according to the antioxidation moisturizing sleep mask containing peony seed oil described in claim 1 or 2 or 3, it is characterised in that
Described emulsifying agent is selected from cetearyl alcohol, lauryl alcohol phosphate ester, C9-15 alcohol phosphate ester, stearyl alcohol phosphate ester and C20-22 alcohol
At least one in phosphate ester.
5. according to the antioxidation moisturizing sleep mask containing peony seed oil described in claim 1 or 2 or 3, it is characterised in that
Described camomile extract is prepared as follows forming: takes Flos Matricariae chamomillae and adds in extraction kettle, is passed through two with 30-50L/h flow velocity
Carbonoxide, adding volumetric concentration by the speed of 1-2L/h is the ethanol of 75%-80%, remains 40-60 DEG C, pressure in temperature
For extracting 2-3h under conditions of 10-15MPa；Obtain Flos Matricariae chamomillae ORGANIC SOLVENT MIXTURES；Put it into decompression low-temperature concentration equipment again
In, it is depressurized to-0.05-0.05MPa, under the conditions of 45-55 DEG C, reclaims organic solvent, obtain camomile extract.
6. according to the antioxidation moisturizing sleep mask containing peony seed oil described in claim 1 or 2 or 3, it is characterised in that
Antibacterial therein is Compositional antiseptic agent: caprylyl glycol and pentanediol are allocated than 1:4 as compounding.Caprylyl glycol is a kind of Genes For Plant Tolerance
Microbial inoculum, belongs to the end group glycol of middle short carbon chain, compounding with pentanediol uses, and can effectively suppress growing of antibacterial and mycete in facial film.
7. according to a preparation method for the antioxidation moisturizing sleep mask containing peony seed oil described in claim 1 or 2 or 3,
It is characterized in that, the method comprises the steps:
1) add the peony seed oil of recipe quantity, fat soluble vitamin E and emulsifying agent in a reservoir, stir, be denoted as solution I,
Standby；
2) in another container, add deionized water, MEIGUI CHUNLU, camomile extract, glycerol, Aloe glue and low molecule glass urine
Acid, stirs, and is denoted as solution II, standby；
3) solution II of the 10%-15% taking full dose adds in solution I, stirs 4-5min, after causing flocculence material occur, then adds
Enter 20%-25% solution II, continue stirring 4-5min, cream molding, add remaining solution II, continue to stir, standby；
4) in step 3) gained cream adds antibacterial, i.e. obtain sleep mask after stirring.
8. peony seed oil and the fat soluble vitamin E application in the skin care item of excessive free radicals in skin histology is removed in preparation, its
Middle peony seed oil is 0.5-10:1, preferably 0.8-2:1 with the weight ratio of fat soluble vitamin E.
9. peony seed oil and the fat soluble vitamin E application in preparation non-oxidizability skin care item, wherein peony seed oil and oil-soluble
The weight ratio of vitamin E is 0.5-10:1, preferably 0.8-2:1.
10. to go the application described in 8 or 9 according to right, it is characterised in that described skin care item are sleep mask.
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| CN107411998A (en) * | 2017-07-03 | 2017-12-01 | 浙江海洋大学 | A kind of anti-oxidant face mask of the active peptide containing hairtail |
| CN107875058A (en) * | 2017-11-30 | 2018-04-06 | 安徽心缘康生物科技有限公司 | Shining face film of a kind of tree peony and preparation method thereof |
| CN108030733A (en) * | 2017-12-28 | 2018-05-15 | 河南健特生物科技集团有限公司 | Facial mask containing brown sugar, peony essential oil and chamomile Ultramicro-powder and preparation method thereof |
| CN108143648A (en) * | 2018-03-07 | 2018-06-12 | 安徽心缘康生物科技有限公司 | A kind of preparation method of the facial mask containing peony essential oil |
| CN109498492A (en) * | 2018-12-29 | 2019-03-22 | 天津金汇药业集团有限公司 | A kind of comprehensive cream of moist type war preparedness |
| CN109908035A (en) * | 2019-04-25 | 2019-06-21 | 山西纳安生物科技有限公司 | A kind of freckle-removing mask based on peony seed oil |
| CN110538105A (en) * | 2019-07-26 | 2019-12-06 | 馥德（上海）科技有限公司 | hydrolat wet compress mask and preparation method thereof |
| CN110652478A (en) * | 2019-10-24 | 2020-01-07 | 樊瑞 | Peony seed oil mask and preparation method thereof |
| CN110742836A (en) * | 2019-12-12 | 2020-02-04 | 广州丹荟生物科技有限公司 | Peony stock solution skin-refreshing mask and preparation method thereof |
| CN113143826A (en) * | 2021-05-17 | 2021-07-23 | 山东派恩生物科技有限公司 | Antioxidant moisturizing sleeping mask containing peony flower stock solution and preparation method thereof |
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| CN108030733A (en) * | 2017-12-28 | 2018-05-15 | 河南健特生物科技集团有限公司 | Facial mask containing brown sugar, peony essential oil and chamomile Ultramicro-powder and preparation method thereof |
| CN108143648A (en) * | 2018-03-07 | 2018-06-12 | 安徽心缘康生物科技有限公司 | A kind of preparation method of the facial mask containing peony essential oil |
| CN109498492A (en) * | 2018-12-29 | 2019-03-22 | 天津金汇药业集团有限公司 | A kind of comprehensive cream of moist type war preparedness |
| CN109908035A (en) * | 2019-04-25 | 2019-06-21 | 山西纳安生物科技有限公司 | A kind of freckle-removing mask based on peony seed oil |
| CN110538105A (en) * | 2019-07-26 | 2019-12-06 | 馥德（上海）科技有限公司 | hydrolat wet compress mask and preparation method thereof |
| CN110652478A (en) * | 2019-10-24 | 2020-01-07 | 樊瑞 | Peony seed oil mask and preparation method thereof |
| CN110742836A (en) * | 2019-12-12 | 2020-02-04 | 广州丹荟生物科技有限公司 | Peony stock solution skin-refreshing mask and preparation method thereof |
| WO2022084638A1 (en) * | 2020-10-22 | 2022-04-28 | Pierre Fabre Dermo-Cosmetique | Oil of paeonia x suffruticosa andrews for protecting the skin and hair |
| FR3115459A1 (en) * | 2020-10-22 | 2022-04-29 | Pierre Fabre Dermo-Cosmetique | Paeonia x suffruticosa Andrews oil for skin and hair protection |
| CN113143826A (en) * | 2021-05-17 | 2021-07-23 | 山东派恩生物科技有限公司 | Antioxidant moisturizing sleeping mask containing peony flower stock solution and preparation method thereof |
| CN113679641A (en) * | 2021-09-28 | 2021-11-23 | 山东派恩生物科技有限公司 | Mask added with peony extract and preparation method thereof |
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