CN110652478A - Peony seed oil mask and preparation method thereof - Google Patents
Peony seed oil mask and preparation method thereof Download PDFInfo
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- CN110652478A CN110652478A CN201911016680.5A CN201911016680A CN110652478A CN 110652478 A CN110652478 A CN 110652478A CN 201911016680 A CN201911016680 A CN 201911016680A CN 110652478 A CN110652478 A CN 110652478A
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- seed oil
- peony seed
- fucosterol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- Life Sciences & Earth Sciences (AREA)
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- Birds (AREA)
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- Mycology (AREA)
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- Engineering & Computer Science (AREA)
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a peony seed oil mask which comprises the following components in percentage by mass: the feed additive comprises, by weight, 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of calendula extract, wherein the sum of the percentages of the components is 100%. The preparation method comprises the steps of stirring the peony seed oil and the fucosterol at the temperature of 30-50 ℃ until the peony seed oil and the fucosterol are dissolved, placing the mixture into an emulsifying pot after stirring is completed, and completely emulsifying to obtain a material A; and sequentially adding the material A, the vitamin E and the calendula extract into hyaluronic acid, stirring for 30-60 min, and cooling to normal temperature after completely stirring to form the peony seed oil smearing type mask. According to the invention, the peony seed oil and the fucosterol are emulsified in a heating state to achieve a good deoiling effect, and the effects of whitening, resisting bacteria and diminishing inflammation can be achieved by combining the vitamin E and the calendula extract.
Description
Technical Field
The invention belongs to the field of skin care products, and particularly relates to a peony seed oil mask and a preparation method of the mask.
Background
With the development of science and technology, people pay more attention to their skin conditions, and whitening is a pursuit of much girls, but due to a series of reasons such as air pollution in daily life, exposure to sunlight, dry climate and the like, the skin condition becomes worse, and with the increase of age, the metabolism speed of self cells is slowed down, and the simple substance skin looks lusterless and drier, and with the pursuit of the beauty lovers for whitening, people are more and more high.
The peony essence is called 'the king of flowers', the peony is precious from top to bottom in the whole body, the peony seeds can extract oil for medical use, and great contribution is made to the field of cosmetics in recent years, however, the cosmetics of the mask appearing on the market at present use the peony seed oil as an auxiliary material, because firstly, the water and oil are mixed and are difficult to mix uniformly, secondly, oil substances are directly applied to the face and can feel oily, and a skin care product mask mainly containing the peony seed oil is lacking on the market at present.
Disclosure of Invention
The invention aims to provide a peony seed oil mask which has the characteristics of moisture retention and low possibility of greasiness.
The invention also provides a preparation method of the peony seed oil mask.
The first technical scheme adopted by the invention is that the peony seed oil mask comprises the following components in percentage by mass: the feed additive comprises, by weight, 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of calendula extract, wherein the sum of the percentages of the components is 100%.
The first technical solution adopted by the present invention is further characterized in that,
the mass ratio of the fucosterol to the peony seed oil is 1: 1-1.25.
The second technical scheme adopted by the invention is as follows: a preparation method of a peony seed oil mask is implemented according to the following specific steps:
step 1, taking cleaned and dried marigold petals, adding 60-80% of absolute ethyl alcohol for reflux extraction, filtering, combining filtrate, concentrating and drying to obtain a marigold extract;
step 2, respectively weighing 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of the calendula extract prepared in the step 1 according to the mass percentage, wherein the sum of the percentages of the components is 100%;
step 3, stirring the peony seed oil and the fucosterol weighed in the step 2 at 30-50 ℃ until the peony seed oil and the fucosterol are dissolved, placing the mixture into an emulsifying pot after stirring is completed, and completely emulsifying to obtain a material A;
step 4, sequentially adding the material A, the vitamin E and the calendula extract obtained in the step 3 into hyaluronic acid, and stirring for 30-60 min;
and 5, cooling the material obtained in the step 4 to normal temperature to form the smearing type mask of the peony seed oil.
The second technical solution adopted by the present invention is further characterized in that,
the mass ratio of the marigold petals to the absolute ethyl alcohol in the step 1 is 1: 6-8, the reflux extraction temperature is 80-100 ℃, and the extraction times are 2-3.
And 3, stirring for 30-60 min in the step 3, wherein the emulsifying time is 20-30 min.
And in the step 4, the stirring temperature is 20-25 ℃.
The invention has the following beneficial effects: according to the peony seed oil facial mask, the peony seed oil has the functions of oxidation resistance, inflammation diminishing and bacteria resistance, but a certain discomfort can be caused when the oily matrix is directly applied to a skin care product.
Detailed Description
The present invention will be described in detail with reference to the following embodiments.
The invention relates to a peony seed oil mask which comprises the following components in percentage by mass: the feed additive comprises, by weight, 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of calendula extract, wherein the sum of the percentages of the components is 100%.
The mass ratio of the fucosterol to the peony seed oil is 1: 1-1.25.
The invention relates to a preparation method of a peony seed oil mask, which is implemented by the following steps:
step 1, taking cleaned and dried marigold petals, adding 6-8 times of 60% -80% absolute ethyl alcohol, performing reflux extraction for 2-3 times at 80-100 ℃, filtering, combining filtrate, concentrating and drying to obtain the marigold extract.
Step 2, respectively weighing 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of the calendula extract prepared in the step 1 according to the mass percentage, wherein the sum of the percentages of the components is 100%.
And 3, placing the peony seed oil and the fucosterol weighed in the step 2 in a beaker, heating to 30-50 ℃, stirring for 30-60 min until the peony seed oil and the fucosterol are dissolved, placing the mixture in an emulsifying pot after stirring is completed, and emulsifying for 20-30 min to obtain a material A.
And 4, sequentially adding the material A, the vitamin E and the calendula extract obtained in the step 3 into hyaluronic acid, and stirring for 30-60 min at 20-25 ℃.
And 5, cooling the material obtained in the step 4 to normal temperature to form the smearing type mask of the peony seed oil. In step 4, the heating temperature is strictly controlled, and if the temperature is too low, the mixing is likely to be uneven, and if the temperature is higher, the active ingredient is likely to be lost.
Example 1
The invention relates to a preparation method of a peony seed oil mask, which is implemented by the following steps:
step 1, taking cleaned and dried marigold petals, adding 6 times of 60% absolute ethyl alcohol, carrying out reflux extraction for 2 times at 80 ℃, filtering, combining filtrates, concentrating and drying to obtain the marigold extract.
Step 2, respectively weighing 2% of vitamin E, 20% of peony seed oil, 15% of fucosterol and 50% of hyaluronic acid according to the mass percentage, and 13% of the calendula extract prepared in the step 1, wherein the sum of the percentages of the components is 100%.
And 3, placing the peony seed oil and the fucosterol weighed in the step 2 in a beaker, heating to 30 ℃, stirring for 30min until the peony seed oil and the fucosterol are dissolved, placing the mixture in an emulsifying pot after stirring, and emulsifying for 30min to obtain a material A.
And 4, sequentially adding the material A obtained in the step 3, vitamin E and the calendula extract into hyaluronic acid, and stirring for 60min at 25 ℃.
And 5, cooling the material obtained in the step 4 to normal temperature to form the smearing type mask of the peony seed oil.
Example 2
Step 1, taking cleaned and dried marigold petals, adding 7 times of 70% absolute ethyl alcohol, carrying out reflux extraction for 2 times at 90 ℃, filtering, combining filtrates, concentrating and drying to obtain the marigold extract.
Step 2, respectively weighing 5% of vitamin E, 25% of peony seed oil, 20% of fucosterol, 30% of hyaluronic acid and 20% of the calendula extract prepared in step 1 according to the mass percentage, wherein the sum of the percentages of the components is 100%.
And 3, placing the peony seed oil and the fucosterol weighed in the step 2 in a beaker, heating to 40 ℃, stirring for 45min until the peony seed oil and the fucosterol are dissolved, placing the mixture in an emulsifying pot after stirring, and emulsifying for 20min to obtain a material A.
And 4, sequentially adding the material A obtained in the step 3, vitamin E and the calendula extract into hyaluronic acid, and stirring for 60min at 23 ℃.
And 5, cooling the material obtained in the step 4 to normal temperature to form the smearing type mask of the peony seed oil.
Example 3
Step 1, taking cleaned and dried marigold petals, adding 8 times of 80% absolute ethyl alcohol, carrying out reflux extraction for 3 times at 100 ℃, filtering, combining filtrates, concentrating and drying to obtain the marigold extract.
Step 2, respectively weighing 3% of vitamin E, 30% of peony seed oil, 25% of fucosterol and 32% of hyaluronic acid according to the mass percentage, and 10% of the calendula extract prepared in the step 1, wherein the sum of the percentages of the components is 100%.
And 3, placing the peony seed oil and the fucosterol weighed in the step 2 in a beaker, heating to 30-50 ℃, stirring for 30-60 min until the peony seed oil and the fucosterol are dissolved, placing the mixture in an emulsifying pot after stirring is completed, and emulsifying for 20-30 min to obtain a material A.
And 4, sequentially adding the material A, the vitamin E and the calendula extract obtained in the step 3 into hyaluronic acid, and stirring for 30-60 min at 20-25 ℃.
And 5, cooling the material obtained in the step 4 to normal temperature to form the smearing type mask of the peony seed oil. Comparative example 1
Unlike example 1, no peony seed oil was added, and the rest was the same.
And (3) effect testing:
80 women with sensitive muscles and acnes of 20-50 years old are randomly divided into four groups, the mask products prepared in examples 1-3 and comparative example 1 are continuously used, the mask products are uniformly smeared on the face after the face is washed every night, the testing time is 1 month, and the testing results are shown in the following table 1.
TABLE 1 test results
From the results in table 1, it can be seen that: the examples 1-3 and the comparison document 1 of the invention can improve the acne to a certain extent, but the improvement effect in the comparison example 1 is obviously smaller than that in the examples 1-3, and the subjects in the examples 1-3 do not have skin sensitivity during use, which indicates that sensitive muscles can be used, while people in the comparison example 1 who have 1/5 have uncomfortable feeling, and the facial mask in the example 3 has the best effect of diminishing inflammation and removing acne, and has good effects of increasing the skin fineness, improving the skin whiteness and shrinking pores.
In view of the comparison, the mask containing the peony seed oil prepared by the invention can play roles of diminishing inflammation, sterilizing, repairing cells and effectively removing acnes, vitamin E is a well-known antioxidant, can protect skin from being damaged by ultraviolet rays and pollution, reduces scars and pigment deposition, also contains certain vitamins in the peony seed oil, and the calendula extract is a Chinese herbal medicine, cannot cause stimulation to the skin, can play a good synergistic effect with the peony seed oil, effectively protects skin lipid cells from being damaged by free radicals, and keeps the skin natural, tender and glossy.
Claims (6)
1. The peony seed oil mask is characterized by comprising the following components in percentage by mass: the feed additive comprises, by weight, 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of calendula extract, wherein the sum of the percentages of the components is 100%.
2. The peony seed oil mask as claimed in claim 1, wherein the mass ratio of the fucosterol to the peony seed oil is 1: 1-1.25.
3. The preparation method of the peony seed oil mask as claimed in claim 1, which is implemented according to the following specific steps:
step 1, taking cleaned and dried marigold petals, adding 60-80% of absolute ethyl alcohol for reflux extraction, filtering, combining filtrate, concentrating and drying to obtain a marigold extract;
step 2, respectively weighing 2-5% of vitamin E, 20-30% of peony seed oil, 15-25% of fucosterol, 30-50% of hyaluronic acid and 10-20% of the calendula extract prepared in the step 1 according to the mass percentage, wherein the sum of the percentages of the components is 100%;
step 3, stirring the peony seed oil and the fucosterol weighed in the step 2 at 30-50 ℃ until the peony seed oil and the fucosterol are dissolved, placing the mixture into an emulsifying pot after stirring is completed, and completely emulsifying to obtain a material A;
step 4, sequentially adding the material A, the vitamin E and the calendula extract obtained in the step 3 into hyaluronic acid, and stirring for 30-60 min;
and 5, cooling the material obtained in the step 4 to normal temperature to form the smearing type mask of the peony seed oil.
4. The preparation method of the peony seed oil mask as claimed in claim 3, wherein the mass ratio of the marigold petals to the absolute ethyl alcohol in the step 1 is 1: 6-8, the reflux extraction temperature is 80-100 ℃, and the extraction times are 2-3.
5. The preparation method of the peony seed oil mask as claimed in claim 3, wherein the stirring in step 3 is carried out for 30-60 min, and the emulsifying time is 20-30 min.
6. The preparation method of the peony seed oil mask as claimed in claim 3, wherein the stirring temperature in the step 4 is 20-25 ℃.
Priority Applications (1)
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CN201911016680.5A CN110652478A (en) | 2019-10-24 | 2019-10-24 | Peony seed oil mask and preparation method thereof |
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CN201911016680.5A CN110652478A (en) | 2019-10-24 | 2019-10-24 | Peony seed oil mask and preparation method thereof |
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Citations (7)
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CN105769683A (en) * | 2016-04-13 | 2016-07-20 | 武汉市农业科学技术研究院林业果树科学研究所 | Anti-oxidation moisturizing sleeping mask containing peony seed oil and preparation method thereof |
CN106413678A (en) * | 2014-01-23 | 2017-02-15 | 延世大学校产学协力团 | Composition containing fucosterol for skin whitening or moisturizing |
CN106580839A (en) * | 2016-04-25 | 2017-04-26 | 山东省农业科学院农产品研究所 | Peony seed protein smearing type mask and preparation method thereof |
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CN107929195A (en) * | 2017-11-28 | 2018-04-20 | 安徽心缘康生物科技有限公司 | A kind of nourishes rough skin tree peony facial mask and preparation method thereof |
CN108143674A (en) * | 2018-03-07 | 2018-06-12 | 安徽心缘康生物科技有限公司 | A kind of lotion containing peony seed oil and preparation method thereof |
CN108998225A (en) * | 2018-10-16 | 2018-12-14 | 广州暨南生物医药研究开发基地有限公司 | A kind of preparation method and application of peony seed oil |
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2019
- 2019-10-24 CN CN201911016680.5A patent/CN110652478A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106413678A (en) * | 2014-01-23 | 2017-02-15 | 延世大学校产学协力团 | Composition containing fucosterol for skin whitening or moisturizing |
CN105769683A (en) * | 2016-04-13 | 2016-07-20 | 武汉市农业科学技术研究院林业果树科学研究所 | Anti-oxidation moisturizing sleeping mask containing peony seed oil and preparation method thereof |
CN106580839A (en) * | 2016-04-25 | 2017-04-26 | 山东省农业科学院农产品研究所 | Peony seed protein smearing type mask and preparation method thereof |
CN106727126A (en) * | 2016-12-20 | 2017-05-31 | 铜陵凤丹种植科技开发有限责任公司 | A kind of peony seed oil facial mask and preparation method thereof |
CN107929195A (en) * | 2017-11-28 | 2018-04-20 | 安徽心缘康生物科技有限公司 | A kind of nourishes rough skin tree peony facial mask and preparation method thereof |
CN108143674A (en) * | 2018-03-07 | 2018-06-12 | 安徽心缘康生物科技有限公司 | A kind of lotion containing peony seed oil and preparation method thereof |
CN108998225A (en) * | 2018-10-16 | 2018-12-14 | 广州暨南生物医药研究开发基地有限公司 | A kind of preparation method and application of peony seed oil |
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Application publication date: 20200107 |