CN103958552B - 高纯度对苯乙烯磺酸钠的制造方法以及聚苯乙烯磺酸钠的制造方法 - Google Patents

高纯度对苯乙烯磺酸钠的制造方法以及聚苯乙烯磺酸钠的制造方法 Download PDF

Info

Publication number
CN103958552B
CN103958552B CN201280055963.0A CN201280055963A CN103958552B CN 103958552 B CN103958552 B CN 103958552B CN 201280055963 A CN201280055963 A CN 201280055963A CN 103958552 B CN103958552 B CN 103958552B
Authority
CN
China
Prior art keywords
salt
acid
sodium
pss
styrene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201280055963.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN103958552A (zh
Inventor
尾添真治
山野井健
山野井健一
松永秀秋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tosoh Organic Chemical Co Ltd
Original Assignee
Tosoh Organic Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tosoh Organic Chemical Co Ltd filed Critical Tosoh Organic Chemical Co Ltd
Publication of CN103958552A publication Critical patent/CN103958552A/zh
Application granted granted Critical
Publication of CN103958552B publication Critical patent/CN103958552B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/45—Anti-settling agents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/168—After-treatment
    • C01B32/174—Derivatisation; Solubilisation; Dispersion in solvents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/194—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F12/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F12/02—Monomers containing only one unsaturated aliphatic radical
    • C08F12/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F12/14—Monomers containing only one unsaturated aliphatic radical containing one ring substituted by hetero atoms or groups containing heteroatoms
    • C08F12/30—Sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/22—Emulsion polymerisation
    • C08F2/24—Emulsion polymerisation with the aid of emulsifying agents
    • C08F2/28—Emulsion polymerisation with the aid of emulsifying agents cationic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/24—Electrically-conducting paints

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Wood Science & Technology (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Polymerization Catalysts (AREA)
  • Graft Or Block Polymers (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
CN201280055963.0A 2011-11-16 2012-08-31 高纯度对苯乙烯磺酸钠的制造方法以及聚苯乙烯磺酸钠的制造方法 Active CN103958552B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2011251116 2011-11-16
JP2011-251116 2011-11-16
PCT/JP2012/072119 WO2013073259A1 (ja) 2011-11-16 2012-08-31 高純度パラスチレンスルホン酸(塩）、それを用いたポリスチレンスルホン酸(塩)、およびポリスチレンスルホン酸(塩)を用いた、分散剤、導電性ポリマードーパント、ナノカーボン材料水性分散体、導電性ポリマー水性分散体、ならびにポリスチレンスルホン酸(塩)の製造方法

Publications (2)

Publication Number Publication Date
CN103958552A CN103958552A (zh) 2014-07-30
CN103958552B true CN103958552B (zh) 2016-11-16

Family

ID=48429334

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280055963.0A Active CN103958552B (zh) 2011-11-16 2012-08-31 高纯度对苯乙烯磺酸钠的制造方法以及聚苯乙烯磺酸钠的制造方法

Country Status (4)

Country Link
JP (1) JP5954798B2 (ja)
CN (1) CN103958552B (ja)
TW (1) TWI573781B (ja)
WO (1) WO2013073259A1 (ja)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5930307B2 (ja) * 2012-10-15 2016-06-08 東ソー有機化学株式会社 流動性と溶解性に優れるパラスチレンスルホン酸ナトリウム、及びその製造方法
US9505713B2 (en) 2012-10-15 2016-11-29 Tosoh Organic Chemical Co., Ltd High-purity sodium p-styrenesulfonate with excellent hue, method for producing the same, poly(sodium p-styrenesulfonate) with excellent hue using the same, and dispersant and synthetic starch for clothing finishing using the poly(sodium p-styrenesulfonate)
JP2015105315A (ja) * 2013-11-29 2015-06-08 東ソー有機化学株式会社 有機溶剤への溶解性と耐熱性に優れたスチレンスルホン酸リチウム共重合体、ならびに当該スチレンスルホン酸リチウム共重合体を用いた帯電防止剤
JP6209157B2 (ja) * 2013-12-25 2017-10-04 信越化学工業株式会社 高分子化合物
CN106414320A (zh) 2014-01-31 2017-02-15 日本瑞翁株式会社 碳纳米管分散液、导电膜及导电性膜
JP6710685B2 (ja) 2014-08-15 2020-06-17 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 導電性透明層の製造のための銀ナノワイヤーおよびスチレン／（メタ）アクリル酸コポリマーを含む組成物
JP6335138B2 (ja) * 2014-08-28 2018-05-30 信越化学工業株式会社 導電性ポリマー複合体及び基板
CN104231755B (zh) * 2014-09-24 2016-02-10 深圳市科恩环保有限公司 一种石墨烯改性色浆材料及其制备方法
JP6383337B2 (ja) * 2015-01-30 2018-08-29 信越化学工業株式会社 導電性高分子組成物、被覆品、パターン形成方法、及び基板
DE102015102553A1 (de) 2015-02-23 2016-08-25 Technische Hochschule Nürnberg Georg Simon Ohm Dispergier-Additiv
JP6844952B2 (ja) * 2015-04-15 2021-03-17 東ソー・ファインケム株式会社 水溶性共重合体及びその製造方法
JP6818288B2 (ja) * 2015-06-16 2021-01-20 国立大学法人東北大学 白金族担持触媒及びその製造方法
JP6580424B2 (ja) * 2015-09-01 2019-09-25 テイカ株式会社 導電性高分子組成物、その分散液、その製造方法およびその用途
JP6401134B2 (ja) * 2015-09-10 2018-10-03 信越化学工業株式会社 導電性ポリマー複合体及び基板
JP6580436B2 (ja) * 2015-09-16 2019-09-25 テイカ株式会社 導電性高分子組成物およびその用途
JP6686500B2 (ja) * 2016-02-12 2020-04-22 東ソー株式会社 導電性高分子水溶液、及び導電性高分子膜
CN107774316B (zh) * 2016-08-29 2020-05-01 中国石油化工股份有限公司 液相氧化合成芳香多元羧酸催化剂
CN107790179B (zh) * 2016-08-29 2020-04-17 中国石油化工股份有限公司 液相氧化生产芳香多元羧酸的催化剂
WO2019088665A2 (ko) * 2017-10-30 2019-05-09 주식회사 엘지화학 전도성 폴리아릴렌 설파이드 수지 조성물
CN112889123A (zh) 2018-08-10 2021-06-01 阿维科斯公司 包含本征导电聚合物的固体电解电容器
US11183342B2 (en) 2018-08-10 2021-11-23 Avx Corporation Solid electrolytic capacitor containing polyaniline
US11114250B2 (en) 2018-08-10 2021-09-07 Avx Corporation Solid electrolytic capacitor formed from conductive polymer particles
CN111097555B (zh) * 2018-10-25 2023-04-07 中国石油化工股份有限公司 强碱性石墨烯复合离子交换树脂材料及其制备方法
CN118213199A (zh) 2018-12-11 2024-06-18 京瓷Avx元器件公司 含有本征导电聚合物的固体电解电容器
JP7310279B2 (ja) * 2019-05-09 2023-07-19 東ソー株式会社 ポリチオフェン－ポリスチレンスルホン酸共重合体からなる複合体、及びそれを含有する水分散液
CN112011137B (zh) * 2019-05-13 2021-10-08 中国科学院化学研究所 一种石墨烯/水溶性聚合物复合材料及其制备方法
CN112436139A (zh) * 2019-08-24 2021-03-02 深圳格林德能源集团有限公司 一种三维复合导电剂制备方法
DE112020004416T5 (de) 2019-09-18 2022-06-15 KYOCERA AVX Components Corporation Festelektrolytkondensator zur Verwendung bei hohen Spannungen
CN110828839B (zh) * 2019-10-30 2021-03-26 深圳氢时代新能源科技有限公司 一种燃料电池复合材料的制备、材料、双极板和燃料电池
JP7126169B2 (ja) * 2019-11-12 2022-08-26 大日精化工業株式会社 顔料分散液
DE112020006028T5 (de) 2019-12-10 2022-10-06 KYOCERA AVX Components Corporation Festelektrolytkondensator, der eine Vorbeschichtung und ein intrinsisch leitfähiges Polymer enthält
DE112020006024T5 (de) 2019-12-10 2022-10-06 KYOCERA AVX Components Corporation Tantalkondensator mit erhöhter Stabilität
KR102229867B1 (ko) * 2020-01-21 2021-03-19 연세대학교 산학협력단 용매 치환이 가능한 높은 일함수 및 투명도를 가지는 전도성 고분자 용액 및 이의 제조방법
JP2021140999A (ja) * 2020-03-06 2021-09-16 学校法人早稲田大学 導電材、およびこれを利用した導電膜ならびに太陽電池
JP6785390B1 (ja) * 2020-03-23 2020-11-18 東ソー・ファインケム株式会社 導電性ポリマー水性分散液、導電性ポリマー塗膜及びその製造方法
JP7447658B2 (ja) 2020-04-21 2024-03-12 三菱ケミカル株式会社 積層ポリエステルフィルム
US11631548B2 (en) 2020-06-08 2023-04-18 KYOCERA AVX Components Corporation Solid electrolytic capacitor containing a moisture barrier
CN113480920A (zh) * 2021-07-23 2021-10-08 浙江永立钢业有限公司 一种高温耐蚀无缝钢管及其制备方法
JP7365444B2 (ja) 2022-03-09 2023-10-19 東ソー・ファインケム株式会社 高純度４－（２－ブロモエチル）ベンゼンスルホン酸及びそれから誘導される高純度スチレンスルホン酸類とそのポリマー、並びにそれらの製造方法
WO2024005174A1 (ja) * 2022-07-01 2024-01-04 Ｐｈｃホールディングス株式会社 導電性炭素フィラーを含む試薬層、当該試薬層を有するセンサ、および当該試薬層の形成方法
WO2024046965A1 (en) 2022-09-01 2024-03-07 Agfa-Gevaert Nv Method of preparing a polymer capacitor, a conductive polymer composition, and it's use as a conductive layer in an electronic device

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1057595A (zh) * 1990-06-29 1992-01-08 狮子株式会社 分散剂
CN1488671A (zh) * 2002-07-26 2004-04-14 H.C.ʩ���˹ɷ����޹�˾ 含聚（3，4-二烷氧基噻吩）和聚阴离子复合物的水分散体及其制备方法
CN1671401A (zh) * 2002-07-22 2005-09-21 基酶有限公司 聚(钾和钠的苯乙烯苯磺酸盐),其制备及其用途
CN101663714A (zh) * 2007-02-20 2010-03-03 东丽株式会社 碳纳米管集合体和导电性膜

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03168239A (ja) * 1989-11-28 1991-07-22 Mita Ind Co Ltd 粒子表面に極性基を有する樹脂粒子およびその製造方法
JPH10139816A (ja) * 1996-11-15 1998-05-26 Tosoh Corp ｐ−スチレンスルホン酸及びその塩の水溶性低分子量重合物の製造方法
JP3601222B2 (ja) * 1996-11-21 2004-12-15 東ソー株式会社 スチレンスルホン酸ナトリウム半水和物、それよりなる組成物及びその製造方法
DE602004010506D1 (de) * 2003-04-24 2008-01-17 Carbon Nanotechnologies Inc Leitfähiger kohlenstoff-nanoröhrenpolymerverbundstoff
JP2005263608A (ja) * 2004-03-22 2005-09-29 Kao Corp カーボンナノチューブ用水性分散剤
JP2006233012A (ja) * 2005-02-24 2006-09-07 Nippon Chem Ind Co Ltd リビングラジカル重合開始剤、その製造方法、及びそれを用いたリビングラジカル重合方法
KR101327242B1 (ko) * 2005-11-17 2013-11-12 헤레우스 프레셔스 메탈스 게엠베하 운트 코. 카게 폴리(3,4-디알콕시티오펜)과 폴리음이온의 복합체의수분산체의 제조방법
FR2902102B1 (fr) * 2006-06-07 2011-11-18 Univ Paris 13 Procede de greffage de polymeres bioactifs sur des materiaux prothetiques
JP5359132B2 (ja) * 2008-09-05 2013-12-04 コニカミノルタ株式会社 透明電極及び該透明電極を有する有機エレクトロルミネッセンス素子
JP5482194B2 (ja) * 2009-03-31 2014-04-23 東レ株式会社 カーボンナノチューブ水性分散液、導電性複合体およびその製造方法
JP5760326B2 (ja) * 2010-03-31 2015-08-05 東ソー株式会社 分子量分布の狭いポリスチレンスルホン酸類又はその塩の製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1057595A (zh) * 1990-06-29 1992-01-08 狮子株式会社 分散剂
CN1671401A (zh) * 2002-07-22 2005-09-21 基酶有限公司 聚(钾和钠的苯乙烯苯磺酸盐),其制备及其用途
CN1488671A (zh) * 2002-07-26 2004-04-14 H.C.ʩ���˹ɷ����޹�˾ 含聚（3，4-二烷氧基噻吩）和聚阴离子复合物的水分散体及其制备方法
CN101663714A (zh) * 2007-02-20 2010-03-03 东丽株式会社 碳纳米管集合体和导电性膜

Also Published As

Publication number Publication date
WO2013073259A1 (ja) 2013-05-23
CN103958552A (zh) 2014-07-30
JPWO2013073259A1 (ja) 2015-04-02
TW201335125A (zh) 2013-09-01
JP5954798B2 (ja) 2016-07-20
TWI573781B (zh) 2017-03-11

Similar Documents

Publication Publication Date Title
CN103958552B (zh) 高纯度对苯乙烯磺酸钠的制造方法以及聚苯乙烯磺酸钠的制造方法
McCarthy et al. Structure–property relationships for tailoring phenoxazines as reducing photoredox catalysts
Szczepaniak et al. Making ATRP more practical: oxygen tolerance
Pan et al. Externally controlled atom transfer radical polymerization
Corbin et al. Photoinduced organocatalyzed atom transfer radical polymerization (O-ATRP): precision polymer synthesis using organic photoredox catalysis
JP5850474B2 (ja) ポリスチレンスルホン酸共重合体、それを用いた分散剤、およびナノカーボン材料水性分散体、ならびにポリスチレンスルホン酸共重合体の製造方法
Jiang et al. Photoorganocatalyzed reversible-deactivation alternating copolymerization of chlorotrifluoroethylene and vinyl ethers under ambient conditions: facile access to main-chain fluorinated copolymers
Berger et al. Halogen bonding in polymer science: from crystal engineering to functional supramolecular polymers and materials
Ye et al. Versatile grafting approaches to functionalizing individually dispersed graphene nanosheets using RAFT polymerization and click chemistry
Sukegawa et al. Expanding the dimensionality of polymers populated with organic robust radicals toward flow cell application: synthesis of TEMPO-crowded bottlebrush polymers using anionic polymerization and ROMP
Samanta et al. Multifunctional hydrophilic poly (vinylidene fluoride) graft copolymer with supertoughness and supergluing properties
Qiao et al. Ultrafast visible-light-induced ATRP in aqueous media with carbon quantum dots as the catalyst and its application for 3D printing
He et al. Synthesis of Poly (ionic liquid) s by Atom Transfer Radical Polymerization with ppm of Cu Catalyst
Yang et al. Metal-free photoinduced electron transfer–atom transfer radical polymerization integrated with bioinspired polydopamine chemistry as a green strategy for surface engineering of magnetic nanoparticles
Peter et al. Synthesis and characterization of bifunctional polymers carrying tris (bipyridyl) ruthenium (II) and triphenylamine units
KR101813650B1 (ko) 도전성 고분자 조성물 및 그 제조 방법
JP2015105315A (ja) 有機溶剤への溶解性と耐熱性に優れたスチレンスルホン酸リチウム共重合体、ならびに当該スチレンスルホン酸リチウム共重合体を用いた帯電防止剤
KR20110107386A (ko) 복합 전기 전도성 폴리머 조성물, 이의 제조 방법, 이를 함유하는 용액, 및 이의 용도
CN105899547B (zh) 包含聚(3,4-亚乙基二氧噻吩)和具有有限酸性的阴离子稳定剂的稳定成分
TW201041963A (en) Complex conductive polymer composition, manufacturing method thereof, solution containing said composition, and applications for said composition
Corbin et al. Radical addition to N, N-diaryl dihydrophenazine photoredox catalysts and implications in photoinduced organocatalyzed atom transfer radical polymerization
TW201536820A (zh) 高分子化合物
Kapil et al. Fully oxygen-tolerant visible-light-induced ATRP of acrylates in water: toward synthesis of protein-polymer hybrids
Schroot et al. Nitroxide-mediated polymerization of styrenic triarylamines and chain-end functionalization with a ruthenium complex: toward tailored photoredox-active architectures
Fonseca Parra et al. Mechanistic Insights into Oxygen Tolerance of Graphitic Carbon Nitride-Mediated Heterogeneous Photoinduced Electron Transfer-Reversible Addition Fragmentation Chain Transfer Polymerization

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant