CN102835333A - Amino acid fertilizer water slurry special for aquaculture and preparation method - Google Patents

Amino acid fertilizer water slurry special for aquaculture and preparation method Download PDF

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CN102835333A
CN102835333A CN2012102991616A CN201210299161A CN102835333A CN 102835333 A CN102835333 A CN 102835333A CN 2012102991616 A CN2012102991616 A CN 2012102991616A CN 201210299161 A CN201210299161 A CN 201210299161A CN 102835333 A CN102835333 A CN 102835333A
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amino acid
raw materials
water slurry
quality percentage
aminoacids solution
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张怀火
张娟
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WUHAN HONGSHAN LVDUN AMINO ACID FACTORY
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WUHAN HONGSHAN LVDUN AMINO ACID FACTORY
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
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    • Y02A40/81Aquaculture, e.g. of fish

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Abstract

The invention discloses amino acid fertilizer water slurry special for aquaculture and a preparation method of the amino acid fertilizer water slurry. The amino acid fertilizer water slurry consists of amino acid solution, microelements, fermentation organic matters, inorganic fertilizer, mineral matters, a water quality modifier and beneficial bacteria according to a certain proportion. The preparation method comprises the following steps of: A, producing the amino acid solution, i.e., a, hydrolyzing, b, neutralizing, c, filtering and d, concentrating; B, producing the fermentation organic matters, i.e., a, stirring, uniformly stirring organic matter raw materials with the amino acid solution, b, inoculating, uniformly stirring the organic matter raw materials with the beneficial bacteria, and c, fermenting; and C, producing the amino acid fertilizer water slurry, i.e., a, chelating, heating the amino acid solution, and adding the microelements under stirring for chelating, b, mixing, adding the fermentation organic matters, the inorganic fertilizer, the mineral matters, the water quality modifier and the beneficial bacteria in sequence and uniformly stirring and mixing, c, checking according to related quality standard, and d, packaging. According to the amino acid fertilizer water slurry, the immunity of fishes is improved, diseases are reduced, the breeding yield of spotted sliver carp is increased, the fish breeding cost is reduced, and the fish quality is improved.

Description

Special-purpose amino acid rich water slurry of aquaculture and preparation method
Technical field
The invention belongs to the biological fish-fertilizer technical field, more specifically relate to the special-purpose amino acid rich water slurry of a kind of aquaculture, also relate to the method for a kind of amino acid fertilizer water slurry of " waste water " preparation that utilizes in L-cystine, L-leucine, the L-tyrosine production process simultaneously.This rich water slurry is a kind of biological fish-fertilizer of high-efficiency environment friendly, is applicable to each fish of freshwater aquiculture, shrimps, crab class, shellfish etc.
Technical background
Fertilizer commonly used in the culture fishery mainly contains three major types, i.e. fertilizer, inorganic fertilizer, biological fish-fertilizer.Traditional fertilizer has its advantage, but fertilizer efficiency is slow, and the process of being utilized by plankton is longer; And in decomposing mineralization process, consume a large amount of oxygen in the water body, this growth to fish is disadvantageous, and in most of the cases; Utilization ratio is low, causes water pollution easily, in addition; Fertilizer should be made base manure, and is mainly used in the Winter-Spring water temperature than low season.Though inorganic fertilizer comes rapidly fertile, function is also comparatively single, uses a series of problems such as quality of bringing environment, water quality and aquatic products in a large number.Biological fish-fertilizer has remedied the deficiency of fertilizer, inorganic fertilizer, and composite beneficial bacterium, trace element etc., is the main flow fertilizer of present aquaculture.
There is " waste water " of great deal of high concentration to produce with hair-hydrolyzation extraction L-cystine, L-leucine, L-tyrosine, mainly contains 18 seed amino acids and ammonium chloride, if directly discharging has not only been wasted valuable resource, and polluted water environment.How to turn waste into wealth, turn harm into good, China scientific worker has passed through long-term exploration and research, and report is that " amino acid journal 1992.4 also has report successively to soil and fertilizer research institute of the Chinese Academy of Sciences afterwards about " research of Fertilizer Efficiency of Amino Acids effect " the earliest.Research shows: amino acid can directly be absorbed by leaves of plants, stem, root, can promote plant tillering, and fertilizer efficiency is fast, and kilnitamin is stronger than the effect of single amino acids, and the fertility ratio waits the inorganic nitrogeneous fertilizer high about 50% of nitrogen amount.How " waste water " of L-cystine, L-leucine, L-tyrosine being effectively used in the culture fishery and going, in order to improve the fertile effect of fishing, reduce the cost of breeding fish, is the problem that a lot of scientific workers study for a long period of time and explore, and is not resolved so far.
Amino acid " waste water " as fertilizer sources is used for aquaculture, and the applicant has carried out reaching research and the exploration in 12 years, and has obtained breakthrough.Through applicant's retrieval, also do not see special-purpose amino acid rich water slurry of a kind of aquaculture and preparation method at present and be disclosed or use.
Summary of the invention
The objective of the invention is to be to provide a kind of aquaculture special-purpose amino acid rich water slurry; Special growth characteristics to fish and food organisms thereof; Adopt modern biotechnology to produce amino acid; Carry out chelating with trace element again, composite then fermented organic, inorganic fertilizer, mineral matter, improver of water quality, beneficial bacterium organically combine inorganic quick-acting, organic long-acting, bio-synergistic; The meticulous special-purpose amino acid rich water slurry of the aquaculture of development, 18 kinds of free amino acids that are rich in that plankton very easily digests and assimilates and necessary 10 seed amino acids of fish growth.After making fishing fertilizer apply water body, can satisfy the nutritional need of fish growth and breed fish, can improve water quality again, improve fish immunity power, reduce disease and take place, increase the variegated carp cultured output, reduce the cost of breeding fish, improve the fish quality with the water body of fostering and apply fertilizer.
Another object of the present invention is the preparation method who has been to provide the special-purpose amino acid rich water slurry of a kind of aquaculture; Easy to implement the method; Easy and simple to handle; With " waste water " in the L-cystine production process through concentrate, fermentation, chelating and preparation amino acid fertilizer water slurry organically combine, and both solved amino acid whose " waste water " problem, and the amino acid resource of a large amount of cheapness is provided for culture fishery again.If remove painstakingly to add amino acid in the fertile preparation of fishing, that is a kind of luxury goods.
The technical scheme of amino acid fertilizer water slurry provided by the present invention is:
The present invention is used for aquaculture with amino acid " waste water " as fertilizer sources, and the efficient utilization of resource and recycle and environmental protection are closely combined, and in order to improve the fertile effect of fishing, reduces the cost of breeding fish.18 kinds of free amino acids that amino acid fertilizer water slurry of the present invention is rich in that plankton very easily digests and assimilates and necessary 10 seed amino acids of fish growth; Lysine, glutamic acid, leucine glycine particularly wherein; Phytoplankton there is peculiar photosynthesis; Can increase the water body dissolved oxygen, improve water body environment, effectively avoid of the harm of dissolved oxygen deficiency fish.After fishing fertilizer applies water body, can satisfy the nutritional need of fish growth and breed fish, can improve water quality again, improve fish immunity power, reduce the fish diseases generation, increase the output of breeding fish, reduce the cost of breeding fish, improve the fish quality with the water body of fostering and apply fertilizer.
The special-purpose amino acid rich water slurry of a kind of aquaculture, it is processed by the raw material of following mass fraction:
Figure BDA00002040154800021
Described aminoacids solution is behaved and is sent out, pig hair, chicken feather, drake feather, goose feather, wool, ox hair wherein any one through hydrochloric acid hydrolysis; Obtain a kind of aminoacids solution, in aminoacids solution, containing each amino acid masses percentage through detection is asparatate 1.3~2.5, threonine 1.0~1.6, serine 1.8~4.0, glutamic acid 2.0~3.5, proline 2.0~3.0, glycine 2.0~3.5, alanine 1.6~2.0, cystine 0.1~0.2, valine 1.5~2.0, methionine 0.1~0.2, isoleucine 0.5~1.5, leucine 0.6~0.8, tyrosine 0.2~0.3, phenyl alanine 1.2~1.5, lysine 0.3~0.4, histidine 0.1~0.2, tryptophan 0.1~0.2, arginine 1.5~2.0.
Described trace element comprises ferrous sulfate, magnesium sulfate, manganese sulphate, ammonium molybdate, zinc sulphate, cobalt sulphate, Boratex, sodium silicate, sodium selenate a kind of or two to eight kinds of combination in any wherein;
Described fermented organic derives from fermentation grouts, vinasse, straw powder, system chaff a kind of or two to four kinds of combination in any wherein;
Described inorganic fertilizer comprises urea, ammonium chloride, ammonium sulfate, carbonic hydroammonium, ammonium nitrate, ammonium humate, MAP, diammonium phosphate, fused calcium magnesium phosphate, superphosphate, double superphosphate a kind of or two to 11 kinds of combination in any wherein;
Described mineral matter comprises kaolin, diatomite, bentonite, atlapulgite, zeolite powder a kind of or two to five kinds of combination in any wherein;
Described improver of water quality comprises potassium fulvate, sodium humate, calper calcium peroxide, sodium perborate a kind of or two to three kinds of combination in any wherein;
Described beneficial bacterium comprises lactic acid bacteria, Bifidobacterium, bacillus, saccharomycete, nitrifying bacteria, photosynthetic bacteria a kind of or two to six kinds of combination in any wherein;
The preparation method of the special-purpose amino acid rich water slurry of a kind of aquaculture the steps include:
A. the preparation of aminoacids solution:
A. hydrolysis
Hair (people sends out, pig hair, chicken feather, drake feather, goose feather, wool, ox hair wherein any one): hydrochloric acid (28~31%)=1:2, temperature is controlled at 108~115 ℃, and the reaction time is at 6~8h;
B. neutralization
Be neutralized to pH4.8~5.1 with under 40~70 ℃ in 99.9% liquefied ammonia;
C. filter (comprising rough and refining)
Filter cake extracts L-cystine, L-leucine, L-tyrosine, and it is subsequent use that filtrating changes enrichment process over to;
D. concentrate
To filtrate-0.06~-be concentrated into 28~30Be ' under the 0.08Mpa, aminoacids solution.
B. the preparation of fermented organic:
A. spice
Organic matter: aminoacids solution=1:1 mixes thoroughly;
B. inoculation
The fermented organic raw material is equipped with 0.5~1% beneficial bacterium and mixes thoroughly and beat heap;
C. fermentation
50~60 ℃ of bottom fermentations 6~8 days, obtain fermented organic.
C. the preparation of amino acid fertilizer water slurry:
A. chelating
Aminoacids solution is heated to 70~90 ℃, stirs trace element chelated 2~3 hours of adding down;
B. be mixed
Add fermented organic, inorganic fertilizer, mineral matter, improver of water quality, beneficial bacterium successively, stirring and evenly mixing;
C. check
Test according to the correlated quality standard;
D. pack
Different finished products packing specification is on request carried out metering packing;
E. accumulating
To be up to the standards, the storage of the finished product of Proper Packing, transportation.
The present invention compares with the various fishing fertilizer of other uses, has following outstanding advantage:
1. 18 kinds of free amino acids that are rich in that plankton very easily digests and assimilates and necessary 10 seed amino acids of fish growth;
2. lysine, glutamic acid, leucine glycine particularly has peculiar photosynthesis to phytoplankton, can increase the water body dissolved oxygen amount, reduces fish and raises the nose above water to breathe the general pool;
3. various nutritive element proportioning science, fish were both direct-edible, and the water body food organisms of can fostering and apply fertilizer again are edible indirectly by fish, and feed, fertilizer coefficient are low, can save concentrated feed 33~45%;
4. post-directed training fish high-quality food organisms breed zooplankton in a large number, have strengthened the input ratio of flower silver carp, are increased to 7:3 by traditional 1:3;
5. beneficial bacterium and improver of water quality; Can effectively improve water quality and purifying water body environment, effectively decompose the residual bait of fish, ight soil, organic matter, reduce the content of ammonia nitrogen, nitrite; Suppress the breeding growth of harmful bacterium; Improve fish body immunity, effectively prevented the incidence of disease of fish hemorrhage, enteritis, fin rot, reduced death;
6. consumption is few, and instant effect is easy to use, and fragrant odour has the distinctive sauce fragrance of dense amino acid, polluted-water not, and at the bottom of the pond of not hardening, environmental protection, efficient cheap;
7. input-output ratio is high, and per kilogram amino acid fertilizer water slurry can be produced 2.2 kilograms of fresh fish;
8. turn the foul and rotten into the rare and ethereal, efficient utilization and the recycle of amino acid " waste water " with resource organically combined, realized excellent transfer by " luxury goods " to " popular ".
Description of drawings
Fig. 1 is a kind of aminoacids solution process chart
Fig. 2 is a kind of fermented organic process chart
Fig. 3 is a kind of amino acid fertilizer water slurry process chart
Embodiment
The special-purpose amino acid rich water slurry of a kind of aquaculture, its proportioning is following:
Table 1 amino acid fertilizer water slurry formulation examples unit: mass percent
Described aminoacids solution, in aminoacids solution, containing each amino acid masses percentage through detection is asparatate 1.3~2.5, threonine 1.0~1.6, serine 1.8~4.0, glutamic acid 2.0~3.5, proline 2.0~3.0, glycine 2.0~3.5, alanine 1.6~2.0, cystine 0.1~0.2, valine 1.5~2.0, methionine 0.1~0.2, isoleucine 0.5~1.5, leucine 0.6~0.8, tyrosine 0.2~0.3, phenyl alanine 1.2~1.5, lysine 0.3~0.4, histidine 0.1~0.2, tryptophan 0.1~0.2, arginine 1.5~2.0.
Described trace element comprises ferrous sulfate 15%, magnesium sulfate 15%, manganese sulphate 5%, ammonium molybdate 5%, zinc sulphate 15%, cobalt sulphate 5%, Boratex 15%, sodium silicate 20%, sodium selenate 5% a kind of or two to eight kinds of combination in any wherein;
Described fermented organic derives from fermentation grouts 25%, vinasse 25%, straw powder 20%, system chaff 30% a kind of or two to four kinds of combination in any wherein;
Described inorganic fertilizer comprises urea 10%, ammonium chloride 20%, ammonium sulfate 10%, carbonic hydroammonium 10%, ammonium nitrate 5%, ammonium humate 5%, MAP 20%, diammonium phosphate 5%, fused calcium magnesium phosphate 5%, superphosphate 5%, double superphosphate 5% a kind of or two to 11 kinds of combination in any wherein;
Described mineral matter comprises kaolin 10%, diatomite 20%, bentonite 20%, atlapulgite 10%, zeolite powder 40% a kind of or two to five kinds of combination in any wherein;
Described improver of water quality comprises potassium fulvate 60%, sodium humate 20%, calper calcium peroxide 10%, sodium perborate 10% a kind of or two to three kinds of combination in any wherein.
Described beneficial bacterium comprises lactic acid bacteria 10%, Bifidobacterium 10%, bacillus 30%, saccharomycete 15%, nitrifying bacteria 15%, photosynthetic bacteria 20% a kind of or two to six kinds of combination in any wherein;
The preparation method of the special-purpose amino acid rich water slurry of a kind of aquaculture the steps include:
A. the production of aminoacids solution (seeing accompanying drawing 1 for details)
A. hydrolysis 1.
Hair (people sends out, pig hair, chicken feather, drake feather, goose feather, wool, ox hair wherein any one): hydrochloric acid (28~31%)=1:2, temperature are controlled at 108 or 110 or 111 or 113 or 114 or 115 ℃, the reaction time 6 or 7 or 8h;
B. neutralization 2.
Be neutralized to pH4.8 or 4.9 or 5 or 5.1 with under 99.9% liquefied ammonia 40 or 43 or 46 or 48 or 51 or 55 or 58 or 61 or 64 or 66 or 68 or 70 ℃;
C. filter (comprise rough 3. with refining 4.)
Filter cake extracts L-cystine, L-leucine, L-tyrosine, and it is subsequent use that filtrating changes enrichment process over to;
D. concentrate 5.
To filtrate-0.06 or-0.07 or-be concentrated into 28 or 29 or 30Be ' under the 0.08Mpa, aminoacids solution 6..
B. the production of fermented organic (seeing accompanying drawing 2 for details)
A. spice 7.
Organic matter: aminoacids solution=1:1 mixes thoroughly;
B. inoculation
The fermented organic raw material is equipped with 0.5 or 0.6 or 0.7 or 0.8 or 0.9 or 1% beneficial bacterium and mixes thoroughly and beat heap;
C. fermentation 8.
50 or 55 or 60 ℃ of bottom fermentations 6 or 7 or 8 days, obtain fermented organic;
C. the production of amino acid fertilizer water slurry (seeing accompanying drawing 3 for details)
A. chelating 9.
Aminoacids solution stirs trace element chelated 2 or 2.5 or 3 hours of adding down at 70 or 75 or 80 or 85 or 90 ℃;
B. be mixed 10.
Add fermented organic, inorganic fertilizer, mineral matter, improver of water quality, beneficial bacterium successively, stirring and evenly mixing;
C. check
Figure BDA00002040154800061
Test according to the correlated quality standard;
D. pack
Figure BDA00002040154800062
Different finished products packing specification is on request carried out metering packing;
E. accumulating
To be up to the standards, the storage of the finished product of Proper Packing, transportation.
1. to the requirement of breeding water body
The quality of breeding water body is great to the growth relationship of fish, and so-called " breed fish is exactly to support water " is exactly this reason.Therefore, require during the whole breed of breeding fish, to require dissolved oxygen>=5mg/L, ammonia nitrogen≤0.02mg/L, nitrite≤0.1mg/L.
2. culture and use and effect
Evenly be spilled in the breeding water body after the dissolving of the special-purpose amino acid rich water slurry of aquaculture of the present invention water, effect is following:
Culture application example:
The lake surface that Xinzhou, Wuhan in 2012 is 26000 mu, the depth of water 2.5~3.5m is main to put variegated carp in a suitable place to breed; Throw in 870,000 jin of 780,000 tail of variegated carp fingerling altogether, 30,000 jin of 40,000 tail of silver carp fingerling, April 15 and twice sampling on April 30; Variegated carp 914 tails, 1.10 jin of average every cabrage amounts, transparency 130cm.Used our factory's amino acid fertilizer water slurry since May 2, water body progressively reaches fertile tender the feeling well of living.Detected water sample and selective examination fish appearance on July 5:
Water sample: 35 ℃ of temperature, 30 ℃ of water temperatures, transparency 40cm; 2250/L of zooplankton total amount, biomass 17.91mg/L, wherein to account for total amount percentage respectively be rotifers 64 for each zooplankton quantity and biomass; 4.01, cladocera 8,30.15, copepoda 10,62.80, nauplius 8; 3.01, protozoa 10,0.18.Conclusion is: belong to medium rich water, the quantity of zooplankton is moderate.
Fish appearance: variegated carp 180 tails, 2.27 jin of average every cabrage amounts.Conclusion is: weightening finish reaches expection, and coefficient of condition can.Fish has infected Chinese Sao, desinsection.

Claims (10)

1. the special-purpose amino acid rich water of aquaculture is starched, and it is processed by the raw material of following mass fraction:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 40~60 trace elements 0.5~1
Fermented organic 12~20 inorganic fertilizer 16~20
Mineral matter 6~10 improver of water quality 5~10
Beneficial bacterium 0.5~1;
Described aminoacids solution is behaved and is sent out, pig hair, chicken feather, drake feather, goose feather, wool, ox hair wherein any one through hydrochloric acid hydrolysis; Obtain a kind of aminoacids solution, in aminoacids solution, containing each amino acid masses percentage through detection is asparatate 1.3~2.5, threonine 1.0~1.6, serine 1.8~4.0, glutamic acid 2.0~3.5, proline 2.0~3.0, glycine 2.0~3.5, alanine 1.6~2.0, cystine 0.1~0.2, valine 1.5~2.0, methionine 0.1~0.2, isoleucine 0.5~1.5, leucine 0.6~0.8, tyrosine 0.2~0.3, phenyl alanine 1.2~1.5, lysine 0.3~0.4, histidine 0.1~0.2, tryptophan 0.1~0.2, arginine 1.5~2.0;
Described trace element comprises ferrous sulfate, magnesium sulfate, manganese sulphate, ammonium molybdate, zinc sulphate, cobalt sulphate, Boratex, sodium silicate, sodium selenate a kind of or two to eight kinds of combination in any wherein;
Described fermented organic derives from fermentation grouts, vinasse, straw powder, system chaff a kind of or two to four kinds of combination in any wherein;
Described inorganic fertilizer comprises urea, ammonium chloride, ammonium sulfate, carbonic hydroammonium, ammonium nitrate, ammonium humate, MAP, diammonium phosphate, fused calcium magnesium phosphate, superphosphate, heavy persulfuric acid calcium a kind of or two to 11 kinds of combination in any wherein;
Described mineral matter comprises kaolin, diatomite, bentonite, atlapulgite, zeolite powder a kind of or two to five kinds of combination in any wherein;
Described improver of water quality comprises potassium fulvate, sodium humate, calper calcium peroxide, sodium perborate a kind of or two to three kinds of combination in any wherein;
Described beneficial bacterium comprises lactic acid bacteria, Bifidobacterium, bacillus, saccharomycete, nitrifying bacteria, photosynthetic bacteria a kind of or two to six kinds of combination in any wherein.
2. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 52 trace elements 0.5
Fermented organic 20 inorganic fertilizer 15
Mineral matter 5 improver of water quality 7
Beneficial bacterium 0.5.
3. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 49.8 trace elements 0.6
Fermented organic 19 inorganic fertilizer 16
Mineral matter 6 improver of water quality 8
Beneficial bacterium 0.6.
4. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 47.6 trace elements 0.7
Fermented organic 18 inorganic fertilizer 17
Mineral matter 7 improver of water quality 9
Beneficial bacterium 0.7.
5. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 45.4 trace elements 0.8
Fermented organic 18 inorganic fertilizer 17
Mineral matter 8 improver of water quality 10
Beneficial bacterium 0.8.
6. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 45.4 trace elements 0.8
Fermented organic 17 inorganic fertilizer 18
Mineral matter 8 improver of water quality 10
Beneficial bacterium 0.8.
7. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 47.6 trace elements 0.7
Fermented organic 17 inorganic fertilizer 18
Mineral matter 7 improver of water quality 9
Beneficial bacterium 0.7.
8. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 49.8 trace elements 0.6
Fermented organic 16 inorganic fertilizer 19
Mineral matter 6 improver of water quality 8
Beneficial bacterium 0.6.
9. the special-purpose amino acid rich water slurry of a kind of aquaculture according to claim 1 is characterized in that:
Raw materials quality percentage raw materials quality percentage
Aminoacids solution 52 trace elements 0.5
Fermented organic 15 inorganic fertilizer 20
Mineral matter 5 improver of water quality 7
Beneficial bacterium 0.5.
10. the preparation method of the special-purpose amino acid rich water slurry of the described a kind of aquaculture of claim 1 the steps include:
A. the preparation of aminoacids solution:
A. hydrolysis
Hair: hydrochloric acid=1:2,108~115 ℃ of reaction 6~8h;
B. neutralization
Be neutralized to PH4.8~5.1 with under 40~70 ℃ in 99.9% liquefied ammonia;
C. filter
Filter cake extracts L-cystine, L-leucine, L-tyrosine, and it is subsequent use that filtrating changes enrichment process over to;
D. concentrate
To filtrate-0.06~-be concentrated into 28~30Be ' under the 0.08MPa, aminoacids solution;
B. the preparation of fermented organic:
A. spice
Organic matter: aminoacids solution=1:1 mixes thoroughly;
B. inoculation
The fermented organic raw material is equipped with 0.5~1% beneficial bacterium and mixes thoroughly and beat heap;
C. fermentation
50~60 ℃ of bottom fermentations 6~8 days;
C. the preparation of amino acid fertilizer water slurry:
A. chelating
Aminoacids solution is heated to 70~90 ℃, stirs trace element chelated 2~3 hours of adding down;
B. be mixed
Add fermented organic, inorganic fertilizer, mineral matter, improver of water quality, beneficial bacterium successively, stirring and evenly mixing;
C. check.
CN2012102991616A 2012-08-21 2012-08-21 Amino acid fertilizer water slurry special for aquaculture and preparation method Pending CN102835333A (en)

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CN107488590A (en) * 2017-09-27 2017-12-19 张家港鸿蚓生物科技有限公司 A kind of rich water protects careless liquid culture medium and preparation method thereof
WO2017214959A1 (en) * 2016-06-17 2017-12-21 张铭强 Organic carbon water activator for purifying water and replenishing energy so as to improve quality and yield of aquatic products, and preparation method and application thereof
CN107879806A (en) * 2017-11-29 2018-04-06 深圳地天国际生物工程科技有限公司 Rich water powder long for flower silver carp speed and preparation method thereof
CN108083354A (en) * 2017-12-26 2018-05-29 深圳地天国际生物工程科技有限公司 A kind of water-bed purification tablet and its preparation process for aquaculture
CN108164324A (en) * 2017-12-22 2018-06-15 武汉华扬动物药业有限责任公司 A kind of aquatic products training algae cream
CN108328750A (en) * 2018-04-25 2018-07-27 河南牧业经济学院 A kind of improver of water quality used for aquiculture and preparation method thereof
CN108633657A (en) * 2018-04-25 2018-10-12 福建省农业科学院农业质量标准与检测技术研究所 A kind of method that red worm cultivation is made altogether with Rice Cropping
CN110089622A (en) * 2019-06-19 2019-08-06 庞红兴 Aquatic feeds of plant protein source and preparation method thereof
CN111248123A (en) * 2020-03-20 2020-06-09 天津农学院 Fertilizer water paste for seawater shellfish pond culture and use method thereof

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CN103936174A (en) * 2014-05-15 2014-07-23 蒋常德 Biological agent for preventing and treating mosses in water body and preparation method of biological agent
CN103936174B (en) * 2014-05-15 2015-06-24 中铁建生态环境设计研究有限公司 Biological agent for preventing and treating mosses in water body and preparation method of biological agent
CN104256136A (en) * 2014-09-17 2015-01-07 常德市元拓有机肥有限公司 Biological fish manure for bighead carps or silver carps, and preparation method thereof
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CN104446747A (en) * 2014-11-03 2015-03-25 廖景慈 Formula of indirect carp feed
CN104351478A (en) * 2014-11-25 2015-02-18 武汉轻工大学 Composite functional amino acid feed additive and application
CN105010816A (en) * 2015-06-25 2015-11-04 江西农业大学 Breeding eel feed and preparation method thereof
CN105010816B (en) * 2015-06-25 2019-05-17 江西农业大学 A kind of parent's eel feed and preparation method thereof
CN105052837A (en) * 2015-07-29 2015-11-18 通威股份有限公司 Breeding method of larval stage feed of coregonus peled fry
CN105130679A (en) * 2015-09-22 2015-12-09 江苏农林职业技术学院 Efficient large-water-surface fishing bacteria-algae balancing bio-fertilizer
CN105272448A (en) * 2015-09-30 2016-01-27 洛阳林泉农业开发有限公司 Wool-containing amino acid foliar fertilizer and preparation method thereof
WO2017214959A1 (en) * 2016-06-17 2017-12-21 张铭强 Organic carbon water activator for purifying water and replenishing energy so as to improve quality and yield of aquatic products, and preparation method and application thereof
CN106946359A (en) * 2017-02-28 2017-07-14 嵊州市派特普科技开发有限公司 A kind of improver of water quality and preparation method thereof
CN107488590A (en) * 2017-09-27 2017-12-19 张家港鸿蚓生物科技有限公司 A kind of rich water protects careless liquid culture medium and preparation method thereof
CN107879806A (en) * 2017-11-29 2018-04-06 深圳地天国际生物工程科技有限公司 Rich water powder long for flower silver carp speed and preparation method thereof
CN108164324A (en) * 2017-12-22 2018-06-15 武汉华扬动物药业有限责任公司 A kind of aquatic products training algae cream
CN108083354A (en) * 2017-12-26 2018-05-29 深圳地天国际生物工程科技有限公司 A kind of water-bed purification tablet and its preparation process for aquaculture
CN108328750A (en) * 2018-04-25 2018-07-27 河南牧业经济学院 A kind of improver of water quality used for aquiculture and preparation method thereof
CN108633657A (en) * 2018-04-25 2018-10-12 福建省农业科学院农业质量标准与检测技术研究所 A kind of method that red worm cultivation is made altogether with Rice Cropping
CN110089622A (en) * 2019-06-19 2019-08-06 庞红兴 Aquatic feeds of plant protein source and preparation method thereof
CN111248123A (en) * 2020-03-20 2020-06-09 天津农学院 Fertilizer water paste for seawater shellfish pond culture and use method thereof
CN111248123B (en) * 2020-03-20 2021-09-14 天津农学院 Fertilizer water paste for seawater shellfish pond culture and use method thereof

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