CN101472664A - 干燥包含氟丙烯的气流的方法 - Google Patents
干燥包含氟丙烯的气流的方法 Download PDFInfo
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- CN101472664A CN101472664A CNA2007800223173A CN200780022317A CN101472664A CN 101472664 A CN101472664 A CN 101472664A CN A2007800223173 A CNA2007800223173 A CN A2007800223173A CN 200780022317 A CN200780022317 A CN 200780022317A CN 101472664 A CN101472664 A CN 101472664A
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- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 46
- 238000001035 drying Methods 0.000 title claims abstract description 21
- VJGCZWVJDRIHNC-UHFFFAOYSA-N 1-fluoroprop-1-ene Chemical compound CC=CF VJGCZWVJDRIHNC-UHFFFAOYSA-N 0.000 title abstract 4
- 239000002808 molecular sieve Substances 0.000 claims abstract description 51
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 51
- 239000012530 fluid Substances 0.000 claims abstract description 45
- 238000012546 transfer Methods 0.000 claims abstract description 11
- 239000013529 heat transfer fluid Substances 0.000 claims abstract description 7
- LVGUZGTVOIAKKC-UHFFFAOYSA-N 1,1,1,2-tetrafluoroethane Chemical compound FCC(F)(F)F LVGUZGTVOIAKKC-UHFFFAOYSA-N 0.000 claims description 23
- QBTUCBKAWGUMMK-UHFFFAOYSA-N C=CC.[F] Chemical group C=CC.[F] QBTUCBKAWGUMMK-UHFFFAOYSA-N 0.000 claims description 19
- FXRLMCRCYDHQFW-UHFFFAOYSA-N 2,3,3,3-tetrafluoropropene Chemical group FC(=C)C(F)(F)F FXRLMCRCYDHQFW-UHFFFAOYSA-N 0.000 claims description 18
- 239000003507 refrigerant Substances 0.000 claims description 16
- 239000000314 lubricant Substances 0.000 claims description 15
- 239000003463 adsorbent Substances 0.000 claims description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 13
- 238000004378 air conditioning Methods 0.000 claims description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 238000005057 refrigeration Methods 0.000 claims description 8
- 150000002148 esters Chemical class 0.000 claims description 7
- 239000004215 Carbon black (E152) Substances 0.000 claims description 5
- 239000000975 dye Substances 0.000 claims description 5
- 229930195733 hydrocarbon Natural products 0.000 claims description 5
- 150000002430 hydrocarbons Chemical class 0.000 claims description 5
- 239000002480 mineral oil Substances 0.000 claims description 5
- 235000010446 mineral oil Nutrition 0.000 claims description 5
- 239000003381 stabilizer Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 150000001993 dienes Chemical class 0.000 claims description 2
- 150000002118 epoxides Chemical group 0.000 claims description 2
- 239000007850 fluorescent dye Substances 0.000 claims description 2
- 150000002989 phenols Chemical class 0.000 claims description 2
- 239000002274 desiccant Substances 0.000 abstract description 10
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 25
- 229910021536 Zeolite Inorganic materials 0.000 description 24
- 239000010457 zeolite Substances 0.000 description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 23
- 239000000203 mixture Substances 0.000 description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000007788 liquid Substances 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 239000011148 porous material Substances 0.000 description 8
- 238000010521 absorption reaction Methods 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 229920001289 polyvinyl ether Polymers 0.000 description 6
- 229910052802 copper Inorganic materials 0.000 description 5
- 239000010949 copper Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 4
- 150000003926 acrylamides Chemical class 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 238000003109 Karl Fischer titration Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- PXBRQCKWGAHEHS-UHFFFAOYSA-N dichlorodifluoromethane Chemical compound FC(F)(Cl)Cl PXBRQCKWGAHEHS-UHFFFAOYSA-N 0.000 description 3
- 235000019404 dichlorodifluoromethane Nutrition 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- RFCAUADVODFSLZ-UHFFFAOYSA-N 1-Chloro-1,1,2,2,2-pentafluoroethane Chemical compound FC(F)(F)C(F)(F)Cl RFCAUADVODFSLZ-UHFFFAOYSA-N 0.000 description 2
- 235000019406 chloropentafluoroethane Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 239000004340 Chloropentafluoroethane Substances 0.000 description 1
- 239000004338 Dichlorodifluoromethane Substances 0.000 description 1
- 208000035126 Facies Diseases 0.000 description 1
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000012809 cooling fluid Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 238000002194 freeze distillation Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 230000026030 halogenation Effects 0.000 description 1
- 238000005658 halogenation reaction Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- -1 neopentyl polyol ester Chemical class 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 239000002594 sorbent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/261—Drying gases or vapours by adsorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/389—Separation; Purification; Stabilisation; Use of additives by adsorption on solids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
- F25B43/00—Arrangements for separating or purifying gases or liquids; Arrangements for vaporising the residuum of liquid refrigerant, e.g. by heat
- F25B43/003—Filters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/106—Silica or silicates
- B01D2253/108—Zeolites
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Power Engineering (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Drying Of Gases (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Drying Of Solid Materials (AREA)
- Lubricants (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
MS3A | MS4A | MS5A | MS13X | |
TFIM | 0.003 | 0.012 | 0.009 | 0.02 |
R-1234yf | 0.003 | 0.01 | 0.021 | 0.019 |
R-134a | 0.004 | 0.007 | 0.009 | 0.02 |
MS3A | MS4A | MS5A | MS13X |
TFIM | 0.097 | 0.088 | 0.091 | 0.08 |
R-1234yf | 0.097 | 0.09 | 0.079 | 0.081 |
R-134a | 0.096 | 0.093 | 0.091 | 0.08 |
Claims (25)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB0611742.8 | 2006-06-14 | ||
GBGB0611742.8A GB0611742D0 (en) | 2006-06-14 | 2006-06-14 | Desiccants for fluids |
PCT/GB2007/002223 WO2007144632A1 (en) | 2006-06-14 | 2007-06-14 | Process for drying a gas stream comprising a fluoropropene |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101472664A true CN101472664A (zh) | 2009-07-01 |
CN101472664B CN101472664B (zh) | 2011-11-16 |
Family
ID=36775605
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2007800223173A Ceased CN101472664B (zh) | 2006-06-14 | 2007-06-14 | 干燥包含氟丙烯的气流的方法 |
Country Status (13)
Country | Link |
---|---|
US (3) | US10130909B2 (zh) |
EP (1) | EP2035117B1 (zh) |
JP (1) | JP4899013B2 (zh) |
KR (1) | KR101177924B1 (zh) |
CN (1) | CN101472664B (zh) |
AT (1) | ATE508785T1 (zh) |
ES (1) | ES2395399T3 (zh) |
GB (2) | GB0611742D0 (zh) |
HK (1) | HK1132700A1 (zh) |
MX (1) | MX2008015858A (zh) |
PT (1) | PT2035117E (zh) |
WO (1) | WO2007144632A1 (zh) |
ZA (1) | ZA200810759B (zh) |
Cited By (9)
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CN102939352A (zh) * | 2010-05-06 | 2013-02-20 | 霍尼韦尔国际公司 | 五氟丙烯和水的类共沸组合物 |
CN103108852A (zh) * | 2010-09-07 | 2013-05-15 | 大金工业株式会社 | 从含氟化合物中的水分除去方法 |
CN105189423A (zh) * | 2013-03-13 | 2015-12-23 | 阿科玛股份有限公司 | 用于纯化及稳定氢氟烯烃和氢氯氟烯烃的方法 |
CN106536464A (zh) * | 2014-06-09 | 2017-03-22 | 墨西哥氟石股份公司 | 用于纯化被卤化乙烷污染的(氢)氟丙烯的方法 |
CN105246865B (zh) * | 2013-04-23 | 2018-02-23 | 墨西哥化学阿玛科股份有限公司 | 用于纯化(氢)卤烃组合物的方法 |
CN108026003A (zh) * | 2015-09-24 | 2018-05-11 | 阿科玛法国公司 | 纯化和干燥氢氟烯烃物流的方法 |
CN108675914A (zh) * | 2018-06-19 | 2018-10-19 | 宇极(廊坊)新材料有限公司 | 一种制备高纯三氟碘甲烷的方法 |
CN111542581A (zh) * | 2017-11-30 | 2020-08-14 | 霍尼韦尔国际公司 | 热传递组合物、方法和系统 |
CN113727960A (zh) * | 2019-04-19 | 2021-11-30 | 大金工业株式会社 | 1,2-二氟乙烯(hfo-1132)的精制方法 |
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EP2164917B1 (en) * | 2008-03-07 | 2019-04-24 | Arkema Inc. | Halogenated alkene heat transfer compositions with improved oil return |
FR2933402B1 (fr) | 2008-07-03 | 2010-07-30 | Arkema France | Procede de purification de 2,3,3,3-tetrafluoro-1-propene (hfo1234yf) |
US8853473B2 (en) | 2008-08-26 | 2014-10-07 | Daikin Industries, Ltd. | Azeotropic or azeotrope-like composition and process for producing 2,3,3,3-tetrafluoropropene |
MX2011003147A (es) | 2008-09-25 | 2011-05-25 | Central Glass Co Ltd | Proceso para producir 1,3,3,3-tetrafluoropropeno. |
US9540296B2 (en) | 2015-03-19 | 2017-01-10 | Honeywell International Inc. | Process for drying HCFO-1233zd |
US9926244B2 (en) | 2008-10-28 | 2018-03-27 | Honeywell International Inc. | Process for drying HCFO-1233zd |
FR2937906B1 (fr) | 2008-11-03 | 2010-11-19 | Arkema France | Procede de chauffage et/ou climatisation d'un vehicule. |
US20170080773A1 (en) | 2008-11-03 | 2017-03-23 | Arkema France | Vehicle Heating and/or Air Conditioning Method |
GB0918069D0 (en) | 2009-10-15 | 2009-12-02 | Ineos Fluor Holdings Ltd | Process |
US9890096B2 (en) * | 2011-01-19 | 2018-02-13 | Honeywell International Inc. | Methods of making 2,3,3,3-tetrafluoro-2-propene |
FR2973809B1 (fr) | 2011-04-08 | 2015-11-13 | Ceca Sa | Utilisation de zeolithes pour la stabilisation d'huiles |
FR2973717B1 (fr) * | 2011-04-08 | 2013-03-29 | Ceca Sa | Procede de reduction de l'acidite totale de compositions frigorigenes |
JP2013241389A (ja) * | 2012-04-25 | 2013-12-05 | Asahi Glass Co Ltd | フルオロオレフィンを含む流体の乾燥方法、およびフルオロオレフィンの製造方法 |
EP2842928A4 (en) * | 2012-04-27 | 2017-11-08 | Asahi Glass Company, Limited | Method for preservation of tetrafluoropropene and container for preservation of tetrafluoropropene |
JP6107466B2 (ja) | 2012-06-28 | 2017-04-05 | セントラル硝子株式会社 | トランス−1,3,3,3−テトラフルオロプロペンの精製方法 |
KR20150054870A (ko) * | 2012-09-11 | 2015-05-20 | 릴라이언스 인더스트리즈 리미티드 | 냉각제 건조용 표면 변경된 제올라이트 |
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CN109096045A (zh) | 2014-02-20 | 2018-12-28 | Agc株式会社 | 含有三氟乙烯的流体的纯化方法及三氟乙烯的制造方法 |
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FR3032131B1 (fr) | 2015-02-02 | 2019-12-27 | Arkema France | Adsorbants zeolithiques de haute surface externe, leur procede de preparation et leurs utilisations |
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- 2007-06-14 GB GB0711473A patent/GB2439209B/en active Active
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CN102939352A (zh) * | 2010-05-06 | 2013-02-20 | 霍尼韦尔国际公司 | 五氟丙烯和水的类共沸组合物 |
CN103108852A (zh) * | 2010-09-07 | 2013-05-15 | 大金工业株式会社 | 从含氟化合物中的水分除去方法 |
CN103108852B (zh) * | 2010-09-07 | 2015-10-21 | 大金工业株式会社 | 从含氟化合物中的水分除去方法 |
CN105189423A (zh) * | 2013-03-13 | 2015-12-23 | 阿科玛股份有限公司 | 用于纯化及稳定氢氟烯烃和氢氯氟烯烃的方法 |
CN105246865B (zh) * | 2013-04-23 | 2018-02-23 | 墨西哥化学阿玛科股份有限公司 | 用于纯化(氢)卤烃组合物的方法 |
CN108285404A (zh) * | 2013-04-23 | 2018-07-17 | 墨西哥化学阿玛科股份有限公司 | 用于纯化(氢)卤烃组合物的方法 |
CN106536464A (zh) * | 2014-06-09 | 2017-03-22 | 墨西哥氟石股份公司 | 用于纯化被卤化乙烷污染的(氢)氟丙烯的方法 |
CN110002949A (zh) * | 2014-06-09 | 2019-07-12 | 墨西哥氟石股份公司 | 用于纯化被卤化乙烷污染的(氢)氟丙烯的方法 |
CN108026003A (zh) * | 2015-09-24 | 2018-05-11 | 阿科玛法国公司 | 纯化和干燥氢氟烯烃物流的方法 |
CN111542581A (zh) * | 2017-11-30 | 2020-08-14 | 霍尼韦尔国际公司 | 热传递组合物、方法和系统 |
CN108675914A (zh) * | 2018-06-19 | 2018-10-19 | 宇极(廊坊)新材料有限公司 | 一种制备高纯三氟碘甲烷的方法 |
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Also Published As
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US10926215B2 (en) | 2021-02-23 |
US20190083927A1 (en) | 2019-03-21 |
GB2439209B (en) | 2008-11-12 |
ATE508785T1 (de) | 2011-05-15 |
GB0711473D0 (en) | 2007-07-25 |
BRPI0713423A2 (pt) | 2012-03-13 |
CN101472664B (zh) | 2011-11-16 |
US10130909B2 (en) | 2018-11-20 |
KR20090054955A (ko) | 2009-06-01 |
ES2395399T3 (es) | 2013-02-12 |
JP4899013B2 (ja) | 2012-03-21 |
WO2007144632A1 (en) | 2007-12-21 |
US20100162738A1 (en) | 2010-07-01 |
MX2008015858A (es) | 2009-01-30 |
JP2009539598A (ja) | 2009-11-19 |
EP2035117A1 (en) | 2009-03-18 |
US20200101417A1 (en) | 2020-04-02 |
HK1132700A1 (en) | 2010-03-05 |
PT2035117E (pt) | 2011-07-14 |
EP2035117B1 (en) | 2011-05-11 |
GB2439209A (en) | 2007-12-19 |
US10493399B2 (en) | 2019-12-03 |
ZA200810759B (en) | 2009-11-25 |
KR101177924B1 (ko) | 2012-08-28 |
GB0611742D0 (en) | 2006-07-26 |
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