CA2959294A1 - Particules de cuivre metallique et leur procede de production - Google Patents

Particules de cuivre metallique et leur procede de production Download PDF

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Publication number
CA2959294A1
CA2959294A1 CA2959294A CA2959294A CA2959294A1 CA 2959294 A1 CA2959294 A1 CA 2959294A1 CA 2959294 A CA2959294 A CA 2959294A CA 2959294 A CA2959294 A CA 2959294A CA 2959294 A1 CA2959294 A1 CA 2959294A1
Authority
CA
Canada
Prior art keywords
metallic copper
particle
copper particle
metallic
gelatin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2959294A
Other languages
English (en)
Inventor
Kiyonobu Ida
Mitsuru Watanabe
Masanori Tomonari
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ishihara Sangyo Kaisha Ltd
Original Assignee
Ishihara Sangyo Kaisha Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ishihara Sangyo Kaisha Ltd filed Critical Ishihara Sangyo Kaisha Ltd
Publication of CA2959294A1 publication Critical patent/CA2959294A1/fr
Abandoned legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05Metallic powder characterised by the size or surface area of the particles
    • B22F1/052Metallic powder characterised by the size or surface area of the particles characterised by a mixture of particles of different sizes or by the particle size distribution
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/09Mixtures of metallic powders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/10Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
    • B22F1/102Metallic powder coated with organic material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/10Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
    • B22F1/105Metallic powder containing lubricating or binding agents; Metallic powder containing organic material containing inorganic lubricating or binding agents, e.g. metal salts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/17Metallic particles coated with metal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/20Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from solid metal compounds
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B1/00Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
    • H01B1/20Conductive material dispersed in non-conductive organic material
    • H01B1/22Conductive material dispersed in non-conductive organic material the conductive material comprising metals or alloys
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B13/00Apparatus or processes specially adapted for manufacturing conductors or cables
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B5/00Non-insulated conductors or conductive bodies characterised by their form
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/06Metallic powder characterised by the shape of the particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/06Metallic powder characterised by the shape of the particles
    • B22F1/068Flake-like particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B22F2009/245Reduction reaction in an Ionic Liquid [IL]
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2301/00Metallic composition of the powder or its coating
    • B22F2301/10Copper
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10Processes characterised by the sequence of their steps

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Dispersion Chemistry (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Powder Metallurgy (AREA)
  • Conductive Materials (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Non-Insulated Conductors (AREA)

Abstract

La présente invention concerne : des particules de cuivre métallique présentant d'excellentes propriétés de frittage à basse température à des températures inférieures ou égales à 300 °C ; et leur procédé de production. Dans ces particules de cuivre métallique, des particules fines de cuivre métallique sont collées aux surfaces de particules de cuivre métallique de grand diamètre. En ce qui concerne les particules de cuivre métallique devant être produites, de l'oxyde de cuivre et de l'acide hypophosphoreux et/ou un sel de ceux-ci sont mélangés et réduits, de préférence en présence de 1 à 500 % en masse de gélatine et/ou de peptide de collagène. La température de la réaction de réduction est de préférence située dans la plage allant de 20 à 100 °C. Les particules de cuivre métallique produites présentent une valeur de résistivité transversale, une fois chauffées à une température de 300 °C sous une atmosphère d'azote, inférieure ou égale à 1 × 10-2 O·cm.
CA2959294A 2014-08-28 2015-08-26 Particules de cuivre metallique et leur procede de production Abandoned CA2959294A1 (fr)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP2014174251 2014-08-28
JP2014-174251 2014-08-28
JP2015-081081 2015-04-10
JP2015081081 2015-04-10
PCT/JP2015/074025 WO2016031860A1 (fr) 2014-08-28 2015-08-26 Particules de cuivre métallique et leur procédé de production

Publications (1)

Publication Number Publication Date
CA2959294A1 true CA2959294A1 (fr) 2016-03-03

Family

ID=55399746

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2959294A Abandoned CA2959294A1 (fr) 2014-08-28 2015-08-26 Particules de cuivre metallique et leur procede de production

Country Status (8)

Country Link
US (1) US20170252801A1 (fr)
EP (1) EP3187288A4 (fr)
JP (1) JPWO2016031860A1 (fr)
KR (1) KR20170046164A (fr)
CN (1) CN106715009A (fr)
CA (1) CA2959294A1 (fr)
TW (1) TWI658156B (fr)
WO (1) WO2016031860A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117600459A (zh) * 2023-11-06 2024-02-27 广东凯洋新材料有限公司 一种散热支架及其制备方法

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5941588B2 (ja) * 2014-09-01 2016-06-29 Dowaエレクトロニクス株式会社 接合材およびそれを用いた接合方法
JP2018509524A (ja) * 2015-01-09 2018-04-05 クラークソン ユニバーシティ 銀被覆銅フレーク及びその製造方法
JP6746094B2 (ja) * 2016-03-22 2020-08-26 株式会社豊田中央研究所 親水性ポリマー被覆銅ナノ粒子の製造方法
TWI623946B (zh) * 2016-07-05 2018-05-11 國立成功大學 奈米銀漿料之製備方法
US10827747B2 (en) * 2016-08-08 2020-11-10 Universiti Brunei Darussalam Anti-bacterial and anti-fungal photocatalytic coating film and method for producing thereof
JP7007140B2 (ja) * 2016-09-30 2022-01-24 Dowaエレクトロニクス株式会社 接合材およびそれを用いた接合方法
WO2018083996A1 (fr) * 2016-11-02 2018-05-11 富士フイルム株式会社 Microparticules, liquide de dispersion et désodorisant
JP6908398B2 (ja) * 2017-03-08 2021-07-28 株式会社Adeka 樹脂組成物、硬化物を形成する方法および硬化物
CN110870392B (zh) 2017-07-18 2023-04-14 旭化成株式会社 具有导电性图案区域的结构体及其制造方法、层积体及其制造方法、以及铜布线
CN108115127A (zh) * 2017-11-29 2018-06-05 上海师范大学 一种纳米铜仿生材料及其制备方法与应用
US11590569B2 (en) 2017-11-29 2023-02-28 National University Corporation Hokkaido University Low-temperature sinterable copper particle and method for producing sintered body by using the same
KR20240049855A (ko) 2018-01-30 2024-04-17 테크나 플라즈마 시스템 인코포레이티드 다층 세라믹 커패시터의 전극 재료로 사용하기 위한 금속 분말과 제조 방법 및 그 사용 방법
JP6985202B2 (ja) * 2018-03-30 2021-12-22 トヨタ自動車株式会社 金属ナノ粒子の製造方法
JP6526888B1 (ja) * 2018-08-01 2019-06-05 Jx金属株式会社 セラミックス層と銅粉ペースト焼結体の積層体
JP6526889B1 (ja) * 2018-08-01 2019-06-05 Jx金属株式会社 セラミックス層と銅粉ペースト焼結体の積層体
KR102673325B1 (ko) * 2018-09-28 2024-06-10 나믹스 가부시끼가이샤 도전성 페이스트
KR102573004B1 (ko) * 2018-11-29 2023-08-30 가부시끼가이샤 레조낙 접합체 및 반도체 장치의 제조 방법, 및 접합용 구리 페이스트
JP2020100888A (ja) * 2018-12-25 2020-07-02 京セラ株式会社 銅粒子、銅粒子の製造方法、銅ペースト及び半導体装置並びに電気・電子部品
CN110202136B (zh) * 2019-05-21 2021-09-03 深圳第三代半导体研究院 一种低温烧结铜膏及其烧结工艺
CN110181041B (zh) * 2019-05-29 2021-09-03 深圳第三代半导体研究院 一种表面进行抗氧化保护的铜颗粒、低温烧结铜膏及使用其的烧结工艺
CN110202137B (zh) * 2019-05-29 2021-07-20 深圳第三代半导体研究院 一种低温烧结铜膏及其烧结工艺
JP7347980B2 (ja) * 2019-07-18 2023-09-20 株式会社リコー 定着装置および画像形成装置
CN110695373B (zh) * 2019-10-14 2022-05-10 天津大学 具有双层谐波结构的石墨烯包覆稀土元素负载铜复合材料的制备方法
WO2021100320A1 (fr) * 2019-11-18 2021-05-27 日清エンジニアリング株式会社 Microparticules
CN111128702A (zh) * 2019-12-10 2020-05-08 Tcl华星光电技术有限公司 一种金属电极的制备方法
JP7302487B2 (ja) * 2020-01-14 2023-07-04 トヨタ自動車株式会社 複合粒子、及び複合粒子の製造方法
JP6901227B1 (ja) * 2020-03-25 2021-07-14 石原ケミカル株式会社 銅インク及び導電膜形成方法
JP7465747B2 (ja) 2020-07-31 2024-04-11 京セラ株式会社 被覆銅粒子、被覆銅粒子の製造方法、銅ペースト、銅ペーストの製造方法、及び半導体装置
US20220143538A1 (en) * 2020-10-15 2022-05-12 Engineered Materials, Inc. Filtration system and method of use thereof
EP4295975A1 (fr) * 2021-02-22 2023-12-27 Mitsubishi Materials Corporation Pâte de liaison, couche liée, corps lié et procédé de production d'un corps lié
CN115188589B (zh) * 2021-04-02 2023-08-01 北京元六鸿远电子科技股份有限公司 一种mlcc可印刷用铜外电极浆料
JP7000621B1 (ja) * 2021-06-17 2022-01-19 古河ケミカルズ株式会社 銅微粒子の製造方法
CN114346254B (zh) * 2022-01-21 2023-08-18 重庆科技学院 一种在低共熔离子液体中制备纳米铜粉的方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004232012A (ja) * 2003-01-29 2004-08-19 Fuji Photo Film Co Ltd 高濃度金属微粒子分散液の製造方法
JP4242176B2 (ja) * 2003-02-25 2009-03-18 石原産業株式会社 銅微粒子及びその製造方法
JP4384484B2 (ja) * 2003-12-18 2009-12-16 アルプス電気株式会社 導電性組成物の製造方法
KR20070051281A (ko) * 2004-08-20 2007-05-17 이시하라 산교 가부시끼가이샤 구리 미립자 및 구리 미립자의 제조 공정
JP4978844B2 (ja) * 2005-07-25 2012-07-18 住友金属鉱山株式会社 銅微粒子分散液及びその製造方法
JP4894266B2 (ja) * 2006-01-06 2012-03-14 住友金属鉱山株式会社 導電粉の表面処理方法と導電粉及び導電性ペースト
JP4821396B2 (ja) * 2006-03-27 2011-11-24 住友金属鉱山株式会社 導電性組成物及び導電膜形成方法
WO2009116349A1 (fr) * 2008-03-21 2009-09-24 旭硝子株式会社 Charge de remplissage de cuivre enduite de nanoparticules de cuivre, procédé de production de celle-ci, pâte de cuivre et article possédant une pellicule métallique
KR101494045B1 (ko) * 2008-08-29 2015-02-16 이시하라 산교 가부시끼가이샤 금속 구리 분산액 및 그 제조 방법 그리고 그것을 사용하여 형성한 전극, 배선 패턴, 도막, 그 도막을 형성한 장식 물품, 항균성 물품 및 그들의 제조 방법
JPWO2010032841A1 (ja) * 2008-09-19 2012-02-16 旭硝子株式会社 導電性フィラー、導電性ペーストおよび導電膜を有する物品
WO2010035258A2 (fr) * 2008-09-25 2010-04-01 Nanoready Ltd. Nanoparticules de cuivre distinctes
CN103582918A (zh) * 2011-05-23 2014-02-12 旭硝子株式会社 导电浆料及使用该导电浆料的带导电膜的基材以及带导电膜的基材的制造方法
JP5450725B2 (ja) * 2011-08-30 2014-03-26 富士フイルム株式会社 コラーゲンペプチド被覆銅ナノ粒子、コラーゲンペプチド被覆銅ナノ粒子分散物、コラーゲンペプチド被覆銅ナノ粒子の製造方法、導電性インク、導電膜の製造方法、及び導体配線

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117600459A (zh) * 2023-11-06 2024-02-27 广东凯洋新材料有限公司 一种散热支架及其制备方法

Also Published As

Publication number Publication date
JPWO2016031860A1 (ja) 2017-06-15
KR20170046164A (ko) 2017-04-28
TWI658156B (zh) 2019-05-01
TW201623639A (zh) 2016-07-01
WO2016031860A1 (fr) 2016-03-03
CN106715009A (zh) 2017-05-24
EP3187288A4 (fr) 2018-04-11
EP3187288A1 (fr) 2017-07-05
US20170252801A1 (en) 2017-09-07

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