BG61943B1 - Метод за производство на аминоетилетаноламин и/или нахидроксиетилпиперазин - Google Patents
Метод за производство на аминоетилетаноламин и/или нахидроксиетилпиперазин Download PDFInfo
- Publication number
- BG61943B1 BG61943B1 BG101668A BG10166897A BG61943B1 BG 61943 B1 BG61943 B1 BG 61943B1 BG 101668 A BG101668 A BG 101668A BG 10166897 A BG10166897 A BG 10166897A BG 61943 B1 BG61943 B1 BG 61943B1
- Authority
- BG
- Bulgaria
- Prior art keywords
- ethylenediamine
- piperazine
- distillation
- ethoxylated
- material stream
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/04—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reaction of ammonia or amines with olefin oxides or halohydrins
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
- C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
- C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
- C07C215/14—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic the nitrogen atom of the amino group being further bound to hydrocarbon groups substituted by amino groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
- C07D295/084—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/088—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9500444A SE511531C2 (sv) | 1995-02-08 | 1995-02-08 | Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin |
| PCT/EP1996/000207 WO1996024576A1 (en) | 1995-02-08 | 1996-01-11 | Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BG101668A BG101668A (en) | 1998-02-27 |
| BG61943B1 true BG61943B1 (bg) | 1998-10-30 |
Family
ID=20397122
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BG101668A BG61943B1 (bg) | 1995-02-08 | 1997-06-25 | Метод за производство на аминоетилетаноламин и/или нахидроксиетилпиперазин |
Country Status (31)
| Country | Link |
|---|---|
| US (1) | US6013801A (et) |
| EP (1) | EP0821664B1 (et) |
| JP (1) | JP3974939B2 (et) |
| KR (2) | KR19980701986A (et) |
| CN (1) | CN1133618C (et) |
| AR (1) | AR000886A1 (et) |
| AT (1) | ATE191453T1 (et) |
| AU (1) | AU699182B2 (et) |
| BG (1) | BG61943B1 (et) |
| BR (1) | BR9607023A (et) |
| CA (1) | CA2208439C (et) |
| CZ (1) | CZ291435B6 (et) |
| DE (1) | DE69607604T2 (et) |
| DK (1) | DK0821664T3 (et) |
| EE (1) | EE03391B1 (et) |
| ES (1) | ES2146866T3 (et) |
| FI (1) | FI973254A (et) |
| GE (1) | GEP19991727B (et) |
| GR (1) | GR3033408T3 (et) |
| HU (1) | HU218150B (et) |
| MX (1) | MX197570B (et) |
| MY (1) | MY112955A (et) |
| NO (1) | NO306776B1 (et) |
| PL (1) | PL183057B1 (et) |
| PT (1) | PT821664E (et) |
| RU (1) | RU2159226C2 (et) |
| SE (1) | SE511531C2 (et) |
| TW (1) | TW389756B (et) |
| UA (1) | UA51638C2 (et) |
| WO (1) | WO1996024576A1 (et) |
| ZA (1) | ZA96351B (et) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1323706A1 (en) * | 2001-12-28 | 2003-07-02 | Nippon Shokubai Co., Ltd. | Process for producing N-hydroxyalkyl compound, and tris(2-hydroxyethyl) isocyanurate composition |
| DE10335991A1 (de) * | 2003-08-01 | 2005-02-24 | Basf Ag | Verfahren zur Herstellung von Ethylenaminen |
| RU2552535C2 (ru) * | 2010-03-18 | 2015-06-10 | Басф Се | Способ получения бедных побочными продуктами аминокарбоксилатов |
| WO2012055893A1 (de) * | 2010-10-29 | 2012-05-03 | Basf Se | Verfahren zur herstellung von 1,4-bishydroxyethyl-piperazin |
| CN102786425B (zh) * | 2011-05-19 | 2014-06-04 | 中国科学院大连化学物理研究所 | 生产β-羟乙基乙二胺的方法 |
| CN102617363A (zh) * | 2012-03-13 | 2012-08-01 | 河北科技大学 | 一种乙二胺和环氧乙烷合成羟乙基乙二胺的新工艺 |
| JP6070088B2 (ja) * | 2012-05-31 | 2017-02-01 | 東ソー株式会社 | Ｎ−アルキルピペラジン類の精製方法 |
| CN103936601B (zh) * | 2013-01-23 | 2016-08-03 | 中国石油化工股份有限公司 | 乙醇胺生产中的氨回收方法 |
| CN103908872B (zh) * | 2014-04-04 | 2015-12-30 | 江苏蓝电环保股份有限公司 | 一种从工业废气中回收二氧化硫的吸收剂及回收方法 |
| CN103908873B (zh) * | 2014-04-04 | 2016-03-09 | 江苏蓝电环保股份有限公司 | 一种从工业废气中回收二氧化硫的方法 |
| CN104130208B (zh) * | 2014-08-04 | 2016-01-13 | 西安近代化学研究所 | 一种n-甲基哌嗪与n-乙基哌嗪的分离方法 |
| BR112018000361B1 (pt) * | 2015-07-15 | 2022-03-15 | Dow Global Technologies Llc | Processo para produzir compostos de hidroxietil piperazina |
| CN107089916B (zh) * | 2016-06-02 | 2019-06-21 | 补天新材料技术有限公司 | 甲酸有机胺盐类化合物及其作为发泡剂的用途 |
| CN106543104B (zh) * | 2016-11-04 | 2019-02-01 | 山东铂源药业有限公司 | 一种1-(2-羟基乙基)哌嗪的合成方法 |
| CN106866583B (zh) * | 2017-01-22 | 2019-02-19 | 绍兴兴欣新材料股份有限公司 | 一种二(2-羟乙基)哌嗪的制备方法 |
| US11214549B2 (en) * | 2017-07-10 | 2022-01-04 | Nouryon Chemicals International B.V. | Process for making higher ethylene amines |
| BR112021008346A2 (pt) | 2018-10-30 | 2021-08-03 | Dow Global Technologies Llc | processo contínuo para a produção de hidroxietilpiperazina, e, produto de hidroxietilpiperazina. |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE206670C (et) * | ||||
| US3639403A (en) * | 1969-03-26 | 1972-02-01 | Jefferson Chem Co Inc | Method for the preparation of piperazine and substituted piperazines |
| DE2716946C2 (de) * | 1977-04-16 | 1986-05-07 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von monohydroxyalkylierten Aminen |
| US4338443A (en) * | 1980-08-15 | 1982-07-06 | Texaco Inc. | Synthesis of N-(2-hydroxyethyl)piperazine |
| DD206670A3 (de) * | 1982-03-15 | 1984-02-01 | Leuna Werke Veb | Verfahren zur herstellung von n-(beta-hydroxyethyl-)piperazin |
| JPS58162625A (ja) * | 1982-03-23 | 1983-09-27 | Toyo Soda Mfg Co Ltd | ポリウレタン製造用触媒 |
| DE3824304A1 (de) * | 1988-07-18 | 1990-02-22 | Henkel Kgaa | Verfahren zur herstellung von anlagerungsprodukten von ethylenoxid und/oder propylenoxid an amine bzw. amide |
| DE4325848A1 (de) * | 1993-07-31 | 1995-02-02 | Basf Ag | Verfahren zur Herstellung von N-(2-Hydroxyethyl)-piperazin |
-
1995
- 1995-02-08 SE SE9500444A patent/SE511531C2/sv not_active IP Right Cessation
-
1996
- 1996-01-11 PL PL96321187A patent/PL183057B1/pl not_active IP Right Cessation
- 1996-01-11 CN CNB961918551A patent/CN1133618C/zh not_active Expired - Fee Related
- 1996-01-11 ES ES96901303T patent/ES2146866T3/es not_active Expired - Lifetime
- 1996-01-11 GE GEAP19963839A patent/GEP19991727B/en unknown
- 1996-01-11 HU HU9702428A patent/HU218150B/hu not_active IP Right Cessation
- 1996-01-11 CZ CZ19972312A patent/CZ291435B6/cs not_active IP Right Cessation
- 1996-01-11 US US08/875,871 patent/US6013801A/en not_active Expired - Lifetime
- 1996-01-11 EE EE9700170A patent/EE03391B1/et not_active IP Right Cessation
- 1996-01-11 CA CA002208439A patent/CA2208439C/en not_active Expired - Fee Related
- 1996-01-11 KR KR1019970705383A patent/KR19980701986A/ko not_active IP Right Cessation
- 1996-01-11 WO PCT/EP1996/000207 patent/WO1996024576A1/en active IP Right Grant
- 1996-01-11 AT AT96901303T patent/ATE191453T1/de not_active IP Right Cessation
- 1996-01-11 KR KR1019970705383A patent/KR100379669B1/ko active
- 1996-01-11 JP JP52392496A patent/JP3974939B2/ja not_active Expired - Fee Related
- 1996-01-11 DK DK96901303T patent/DK0821664T3/da active
- 1996-01-11 RU RU97114881/04A patent/RU2159226C2/ru not_active IP Right Cessation
- 1996-01-11 BR BR9607023A patent/BR9607023A/pt not_active IP Right Cessation
- 1996-01-11 AU AU45376/96A patent/AU699182B2/en not_active Ceased
- 1996-01-11 MX MX9705702A patent/MX197570B/es not_active IP Right Cessation
- 1996-01-11 DE DE69607604T patent/DE69607604T2/de not_active Expired - Lifetime
- 1996-01-11 PT PT96901303T patent/PT821664E/pt unknown
- 1996-01-11 EP EP96901303A patent/EP0821664B1/en not_active Expired - Lifetime
- 1996-01-12 TW TW085100328A patent/TW389756B/zh not_active IP Right Cessation
- 1996-01-17 ZA ZA96351A patent/ZA96351B/xx unknown
- 1996-02-06 MY MYPI96000426A patent/MY112955A/en unknown
- 1996-02-07 AR ARP960101305A patent/AR000886A1/es unknown
- 1996-11-01 UA UA97063429A patent/UA51638C2/uk unknown
-
1997
- 1997-06-25 BG BG101668A patent/BG61943B1/bg unknown
- 1997-07-30 NO NO973509A patent/NO306776B1/no unknown
- 1997-08-07 FI FI973254A patent/FI973254A/fi not_active IP Right Cessation
-
2000
- 2000-05-12 GR GR20000401096T patent/GR3033408T3/el not_active IP Right Cessation
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