ATE204035T1 - Verfahren zur elektrolytischen abscheidung von kupferschichten - Google Patents

Verfahren zur elektrolytischen abscheidung von kupferschichten

Info

Publication number
ATE204035T1
ATE204035T1 AT97952879T AT97952879T ATE204035T1 AT E204035 T1 ATE204035 T1 AT E204035T1 AT 97952879 T AT97952879 T AT 97952879T AT 97952879 T AT97952879 T AT 97952879T AT E204035 T1 ATE204035 T1 AT E204035T1
Authority
AT
Austria
Prior art keywords
pct
copper layers
substrate
deposition
date jun
Prior art date
Application number
AT97952879T
Other languages
German (de)
English (en)
Inventor
Gerd Senge
Wolfgang Dahms
Original Assignee
Atotech Deutschland Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Atotech Deutschland Gmbh filed Critical Atotech Deutschland Gmbh
Application granted granted Critical
Publication of ATE204035T1 publication Critical patent/ATE204035T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00—Electroplating: Baths therefor
    • C25D3/02—Electroplating: Baths therefor from solutions
    • C25D3/38—Electroplating: Baths therefor from solutions of copper
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00—Electroplating: Baths therefor
    • C25D3/02—Electroplating: Baths therefor from solutions
    • C25D3/56—Electroplating: Baths therefor from solutions of alloys
    • C25D3/58—Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of copper
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/18—Electroplating using modulated, pulsed or reversing current
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/60—Electroplating characterised by the structure or texture of the layers
    • C25D5/605—Surface topography of the layers, e.g. rough, dendritic or nodular layers
    • C25D5/611—Smooth layers
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/627—Electroplating characterised by the visual appearance of the layers, e.g. colour, brightness or mat appearance
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K3/00—Apparatus or processes for manufacturing printed circuits
    • H05K3/22—Secondary treatment of printed circuits
    • H05K3/24—Reinforcing the conductive pattern
    • H05K3/241—Reinforcing the conductive pattern characterised by the electroplating method; means therefor, e.g. baths or apparatus
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K3/00—Apparatus or processes for manufacturing printed circuits
    • H05K3/40—Forming printed elements for providing electric connections to or between printed circuits
    • H05K3/42—Plated through-holes or plated via connections
    • H05K3/423—Plated through-holes or plated via connections characterised by electroplating method

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Manufacturing Of Printed Wiring (AREA)
  • Electroplating And Plating Baths Therefor (AREA)
  • Electrolytic Production Of Metals (AREA)
AT97952879T 1996-12-13 1997-12-04 Verfahren zur elektrolytischen abscheidung von kupferschichten ATE204035T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19653681A DE19653681C2 (de) 1996-12-13 1996-12-13 Verfahren zur elektrolytischen Abscheidung von Kupferschichten mit gleichmäßiger Schichtdicke und guten optischen und metallphysikalischen Eigenschaften und Anwendung des Verfahrens
PCT/EP1997/006786 WO1998026114A1 (de) 1996-12-13 1997-12-04 Verfahren zur elektrolytischen abscheidung von kupferschichten

Publications (1)

Publication Number Publication Date
ATE204035T1 true ATE204035T1 (de) 2001-08-15

Family

ID=7815786

Family Applications (1)

Application Number Title Priority Date Filing Date
AT97952879T ATE204035T1 (de) 1996-12-13 1997-12-04 Verfahren zur elektrolytischen abscheidung von kupferschichten

Country Status (8)

Country Link
US (1) US6129830A (enExample)
EP (1) EP0944749B1 (enExample)
JP (1) JP4221064B2 (enExample)
KR (1) KR100546989B1 (enExample)
AT (1) ATE204035T1 (enExample)
CA (1) CA2275214C (enExample)
DE (2) DE19653681C2 (enExample)
WO (1) WO1998026114A1 (enExample)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19915146C1 (de) * 1999-01-21 2000-07-06 Atotech Deutschland Gmbh Verfahren zum galvanischen Bilden von Leiterstrukturen aus hochreinem Kupfer bei der Herstellung von integrierten Schaltungen
JP4394234B2 (ja) * 2000-01-20 2010-01-06 日鉱金属株式会社 銅電気めっき液及び銅電気めっき方法
US6503375B1 (en) * 2000-02-11 2003-01-07 Applied Materials, Inc Electroplating apparatus using a perforated phosphorus doped consumable anode
JP2001267726A (ja) * 2000-03-22 2001-09-28 Toyota Autom Loom Works Ltd 配線基板の電解メッキ方法及び配線基板の電解メッキ装置
US6491806B1 (en) * 2000-04-27 2002-12-10 Intel Corporation Electroplating bath composition
US6776893B1 (en) * 2000-11-20 2004-08-17 Enthone Inc. Electroplating chemistry for the CU filling of submicron features of VLSI/ULSI interconnect
JP4806498B2 (ja) * 2001-08-01 2011-11-02 凸版印刷株式会社 プリント配線基板の製造装置および製造方法
EP1310582A1 (en) * 2001-11-07 2003-05-14 Shipley Company LLC Process for electrolytic copper plating
US7316772B2 (en) * 2002-03-05 2008-01-08 Enthone Inc. Defect reduction in electrodeposited copper for semiconductor applications
US8002962B2 (en) 2002-03-05 2011-08-23 Enthone Inc. Copper electrodeposition in microelectronics
DE10259362A1 (de) * 2002-12-18 2004-07-08 Siemens Ag Verfahren zum Abscheiden einer Legierung auf ein Substrat
EP1477588A1 (en) * 2003-02-19 2004-11-17 Rohm and Haas Electronic Materials, L.L.C. Copper Electroplating composition for wafers
EP1598449B1 (en) * 2004-04-26 2010-08-04 Rohm and Haas Electronic Materials, L.L.C. Improved plating method
TWI400365B (zh) * 2004-11-12 2013-07-01 Enthone 微電子裝置上的銅電沈積
EP1717351A1 (de) * 2005-04-27 2006-11-02 Enthone Inc. Galvanikbad
US20070158199A1 (en) * 2005-12-30 2007-07-12 Haight Scott M Method to modulate the surface roughness of a plated deposit and create fine-grained flat bumps
US20070178697A1 (en) * 2006-02-02 2007-08-02 Enthone Inc. Copper electrodeposition in microelectronics
ATE484943T1 (de) * 2006-03-30 2010-10-15 Atotech Deutschland Gmbh Elektrolytisches verfahren zum füllen von löchern und vertiefungen mit metallen
US7887693B2 (en) * 2007-06-22 2011-02-15 Maria Nikolova Acid copper electroplating bath composition
US7905994B2 (en) 2007-10-03 2011-03-15 Moses Lake Industries, Inc. Substrate holder and electroplating system
JP2009167506A (ja) * 2008-01-21 2009-07-30 Ebara Udylite Kk 酸性電解銅めっき液およびこれを用いる微細配線回路の作製方法
DE102008031003B4 (de) 2008-06-30 2010-04-15 Siemens Aktiengesellschaft Verfahren zum Erzeugen einer CNT enthaltenen Schicht aus einer ionischen Flüssigkeit
US20100206737A1 (en) * 2009-02-17 2010-08-19 Preisser Robert F Process for electrodeposition of copper chip to chip, chip to wafer and wafer to wafer interconnects in through-silicon vias (tsv)
US8262894B2 (en) 2009-04-30 2012-09-11 Moses Lake Industries, Inc. High speed copper plating bath
EP2392694A1 (en) * 2010-06-02 2011-12-07 ATOTECH Deutschland GmbH Method for etching of copper and copper alloys
EP2518187A1 (en) * 2011-04-26 2012-10-31 Atotech Deutschland GmbH Aqueous acidic bath for electrolytic deposition of copper
EP2620529B1 (en) * 2012-01-25 2014-04-30 Atotech Deutschland GmbH Method for producing matt copper deposits
JP6216522B2 (ja) * 2013-03-14 2017-10-18 大日本印刷株式会社 インターポーザー基板の製造方法。
PH12018502416B1 (en) * 2016-05-19 2023-02-10 Atotech Deutschland Gmbh Method for monitoring the total amount of brighteners in an acidic copper/copper alloy plating bath and controlled process for plating
JP6909582B2 (ja) * 2017-01-18 2021-07-28 株式会社Ｊｃｕ 着色用めっき液および着色方法
KR20210062369A (ko) * 2019-11-21 2021-05-31 에스케이넥실리스 주식회사 찢김 또는 주름 불량을 방지할 수 있는 전해동박, 그것을 포함하는 전극, 그것을 포함하는 이차전지, 및 그것의 제조방법
TW202342827A (zh) * 2022-03-31 2023-11-01 日商奧野製藥工業股份有限公司 Pr脈衝電解用銅鍍敷液、及利用pr脈衝電解法之銅鍍敷方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB662217A (en) * 1948-10-13 1951-12-05 Westinghouse Electric Int Co Improvements in or relating to the electrodeposition of copper
DD215589B5 (de) * 1983-05-11 1994-06-01 Heinz Dr Rer Nat Liebscher Verfahren zur elektrolytischen Metallabscheidung bei erzwungener Konvektion
DD261613A1 (de) * 1987-06-05 1988-11-02 Leipzig Galvanotechnik Verfahren zur elektrolytischen kupferabscheidung aus sauren elektrolyten mit dimensionsstabiler anode
GB8801827D0 (en) * 1988-01-27 1988-02-24 Jct Controls Ltd Improvements in electrochemical processes
CN1045770A (zh) * 1989-03-18 1990-10-03 王英 用膜法蒸馏技术分离浓缩醋酸铵与氢氧化铵的系统
GB8913561D0 (en) * 1989-06-13 1989-08-02 Learonal Uk Plc Method of stabilising an organic additive in an electroplating solution
DE4344387C2 (de) * 1993-12-24 1996-09-05 Atotech Deutschland Gmbh Verfahren zur elektrolytischen Abscheidung von Kupfer und Anordnung zur Durchführung des Verfahrens
JP2866300B2 (ja) * 1994-03-07 1999-03-08 生物系特定産業技術研究推進機構 運搬作業車
JPH0967693A (ja) * 1995-08-29 1997-03-11 Nikko Gould Foil Kk 電解銅箔の製造方法

Also Published As

Publication number Publication date
KR20000053278A (ko) 2000-08-25
JP4221064B2 (ja) 2009-02-12
EP0944749A1 (de) 1999-09-29
DE59704260D1 (de) 2001-09-13
KR100546989B1 (ko) 2006-01-26
US6129830A (en) 2000-10-10
WO1998026114A1 (de) 1998-06-18
DE19653681C2 (de) 2000-04-06
EP0944749B1 (de) 2001-08-08
DE19653681A1 (de) 1998-06-18
JP2001505955A (ja) 2001-05-08
CA2275214A1 (en) 1998-06-18
CA2275214C (en) 2007-10-02

Similar Documents

Publication Publication Date Title
ATE204035T1 (de) Verfahren zur elektrolytischen abscheidung von kupferschichten
EP0242583B1 (en) Selective electrolytic stripping of metal coatings from base metal substrates
DE59406281D1 (de) Verfahren und vorrichtung zur elektrolytischen abscheidung von metallschichten
US6071400A (en) Method and device for the electrochemical treatment with treatment liquid of an item to be treated
EP0413109A2 (en) Fabrication of printed circuit boards using conducting polymer
KR880701066A (ko) 도체회로판의 제조방법.
MY119378A (en) A copper foil for a printed circuit board, a process and an apparatus for producing the same
ATE174074T1 (de) Verfahren und vorrichtung zum kontinuierlichen gleichmässigen elektrolytischen metallisieren oder ätzen
WO1989007162A1 (en) Electrochemical processes
CA1085059A (en) Method of providing printed circuits
GB1268317A (en) Improvements in or relating to the manufacture of conductor plates
ATE221716T1 (de) Verfahren zum metallisieren eines elektrisch nichtleitende oberflächenbereiche aufweisenden substrats
KR20040057979A (ko) 무연 주석합금을 피복하는 방법
GB2203451B (en) Method and apparatus for making the inner crowns of composite-layered crowns for restoring crowns
IE50821B1 (en) Process for the selective chemical deposition and/or electrodeposition of metal coatings,especially for the production of printed circuits
EP0502023B1 (de) Metallisierung von nichtleitern
DE602004003698D1 (de) Verfahren zum auffüllen von mikroblindlöchern
US6632344B1 (en) Conductive oxide coating process
JP2000178752A (ja) 無電解メッキ用パラジウム触媒除去剤
ATE135417T1 (de) Verfahren und vorrichtung zum elektrolytischen austragen von metallen aus einer metallionen enthaltenden lösung sowie elektrode zur durchführung des verfahrens
TWI355219B (en) Micro-etching process of pcb without causing galva
DE1640579A1 (de) Verfahren zur Herstellung flaechenhafter elektrischer Leitungszuege
DE2150748C3 (de) Verfahren und Vorrichtung zur elektrochemischen Bearbeitung der Oberflächen von festen Körpern
SU293312A1 (ru) Способ изготовления печатных плат
JPS62140491A (ja) 回路基体の検査方法