WO2015024831A1 - Pico-prüfleck - Google Patents

Pico-prüfleck Download PDF

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Publication number
WO2015024831A1
WO2015024831A1 PCT/EP2014/067309 EP2014067309W WO2015024831A1 WO 2015024831 A1 WO2015024831 A1 WO 2015024831A1 EP 2014067309 W EP2014067309 W EP 2014067309W WO 2015024831 A1 WO2015024831 A1 WO 2015024831A1
Authority
WO
WIPO (PCT)
Prior art keywords
prüfleckvorrichtung
container
capillary
gas
ppm
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2014/067309
Other languages
German (de)
English (en)
French (fr)
Inventor
Rudi Widt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Inficon GmbH Deutschland
Original Assignee
Inficon GmbH Deutschland
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inficon GmbH Deutschland filed Critical Inficon GmbH Deutschland
Priority to US14/911,872 priority Critical patent/US9933325B2/en
Priority to EP14750496.3A priority patent/EP3036518B1/de
Priority to JP2016535419A priority patent/JP2016528509A/ja
Priority to CN201480045282.5A priority patent/CN105531573B/zh
Publication of WO2015024831A1 publication Critical patent/WO2015024831A1/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/007Leak detector calibration, standard leaks
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/04Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
    • G01M3/20Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material
    • G01M3/207Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material calibration arrangements
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F02COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
    • F02DCONTROLLING COMBUSTION ENGINES
    • F02D41/00Electrical control of supply of combustible mixture or its constituents
    • F02D41/02Circuit arrangements for generating control signals
    • F02D41/14Introducing closed-loop corrections
    • F02D41/1438Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor
    • F02D41/1493Details
    • F02D41/1495Detection of abnormalities in the air/fuel ratio feedback system
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3504Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing gases, e.g. multi-gas analysis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0006Calibrating gas analysers
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/007Arrangements to check the analyser

Definitions

  • the invention relates to atician for testing and calibrating a gas leak detector.
  • Test leaks have a housing filled with a test gas and are provided with a leak having a predetermined, known leakage rate through which the test gas penetrates to the outside.
  • the operability or accuracy of a gas leak detector can be tested by measuring the gas leaving the test leak.
  • EP 0742894 Bl describes a capillary provided with a test leak, which has a comparatively low leakage rate of 10 "7 mbarl / s or more achieved.
  • Such capillaries can not be made arbitrarily small because they are otherwise clogged by humidity and unusable.
  • With the known test leaks it has hitherto been impossible to produce leakage rates of 10 "12 mbarl / s or less. Such leakage rates are required to test Leak detectors for very small leaks.
  • the invention has for its object to provide a scholarleck with a low leakage rate in the range of 10 "12 mbarl / s.
  • the educaleckvortechnische invention is defined by the features of claim 1.
  • Theticianleckvoroplasty invention has a filled with a gas that consists of at least 10% of atmospheric air filled container.
  • the remaining portion of the gas may be, for example, nitrogen.
  • the container wall is penetrated by at least one capillary.
  • the capillary should a leak rate in the range of about 10 "5 to 10" 7 mbarl / s and preferably from about 10 "6 mbarl / s have.
  • Atmospheric air does not lead to clogging of the capillary and typically has a proportion of helium and a proportion of Helium and argon are typical test gases in gas leak detection and the amount of helium in the air contained in the container should be in the range of between three and seven ppm and preferably about 3.5 to 5.5 ppm By “about”, it is meant in each case a deviation of ⁇ 10% in the present description
  • the argon content of the air contained in the container should be in the range of 0.1 to 2% and preferably about 0.8 to 1, 2%. A particularly advantageous proportion of argon is about 1%.
  • the container is a cylinder with an end cover or an end cap.
  • the forehead cap is penetrated by the capillary.
  • the cylinder should not exceed a length of 5 cm and a diameter of about 1 cm.
  • the capillary can be guided inside the cylinder along its central longitudinal axis.
  • the container made of glass and the end cap made of a metal can also be used in particularly small test chambers and filled in a simple manner. Filling is done simply by removing the end cap and allowing the gas to flow into the container with the atmospheric air.
  • the cylindrical sketchleck employer has a small surface area and is due to lack of gaps or wells easy to evacuate in a test chamber.
  • the gas in the container should have a relative humidity of less than 50% and preferably less than 40% in order to avoid clogging of the capillary due to atmospheric moisture.
  • FIG. 1 shows a longitudinal section through theticianleckvorraum.
  • the educaleckvorutter 10 consists of a cylindrical container 12 made of glass with a closed bottom 14 on one end face and an open end on the opposite end face. The open end is sealingly closed with a front cap 16 made of metal. Through the metal cap 16, a capillary 18 is guided along the central longitudinal axis of the cylinder 12.
  • the container 12 is filled with atmospheric air 20 having a helium content of 5 ppm and an argon content of 1%.
  • the capillary 18 has a leak rate of 10 "6 mbarl / s.
  • the humidity of the air is 40%.

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Examining Or Testing Airtightness (AREA)
PCT/EP2014/067309 2013-08-20 2014-08-13 Pico-prüfleck Ceased WO2015024831A1 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
US14/911,872 US9933325B2 (en) 2013-08-20 2014-08-13 Pico test leak
EP14750496.3A EP3036518B1 (de) 2013-08-20 2014-08-13 Pico-prüfleck
JP2016535419A JP2016528509A (ja) 2013-08-20 2014-08-13 ピコ漏洩試験器
CN201480045282.5A CN105531573B (zh) 2013-08-20 2014-08-13 微微级测试泄漏装置

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102013216450.5A DE102013216450A1 (de) 2013-08-20 2013-08-20 Pico-Prüfleck
DE102013216450.5 2013-08-20

Publications (1)

Publication Number Publication Date
WO2015024831A1 true WO2015024831A1 (de) 2015-02-26

Family

ID=51302992

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2014/067309 Ceased WO2015024831A1 (de) 2013-08-20 2014-08-13 Pico-prüfleck

Country Status (6)

Country Link
US (1) US9933325B2 (enExample)
EP (1) EP3036518B1 (enExample)
JP (2) JP2016528509A (enExample)
CN (1) CN105531573B (enExample)
DE (1) DE102013216450A1 (enExample)
WO (1) WO2015024831A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102013216450A1 (de) * 2013-08-20 2015-02-26 Inficon Gmbh Pico-Prüfleck
WO2018181105A1 (ja) * 2017-03-31 2018-10-04 芝浦メカトロニクス株式会社 ヒータ管の気体リーク検出装置及びヒータ管の気体リーク検出方法
CN107314867A (zh) * 2017-06-30 2017-11-03 徐校竹 一种漏水检测装置
DE102020100830A1 (de) * 2020-01-15 2021-07-15 Inficon Gmbh Prüfgasapplikator

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0110004A1 (de) * 1982-11-26 1984-06-13 Leybold Aktiengesellschaft Testleck
EP0352371A2 (en) * 1988-07-27 1990-01-31 VARIAN S.p.A. Detector for helium leaks
DE4038266A1 (de) * 1990-11-30 1992-06-04 Siemens Ag Verfahren und vorrichtung zur pruefung der gasdichtigkeit von bauteilen, insbesondere sf(pfeil abwaerts)6(pfeil abwaerts)-dichtigkeit von kondensatoren
US5663487A (en) * 1994-02-02 1997-09-02 Leybold Aktiengesellschaft Capillary tube determining the leakage rate for a test leak
EP1637861A1 (en) * 2004-09-17 2006-03-22 Ronald Douglas Collins Reference gas leak

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5940137A (ja) * 1982-08-30 1984-03-05 Shimadzu Corp リ−クテスト装置
DE3243752A1 (de) * 1982-11-26 1984-05-30 Leybold-Heraeus GmbH, 5000 Köln Testleck
DE3613694A1 (de) * 1986-04-23 1987-10-29 Leybold Heraeus Gmbh & Co Kg Vorrichtung zur kalibrierung des detektors eines lecksuchgeraetes
JP2625342B2 (ja) * 1993-01-06 1997-07-02 日本電信電話株式会社 質量分析型ガス漏れ検知器に適用されるガス濃度校正法及び校正器具
SE502355C2 (sv) * 1994-02-17 1995-10-09 Hans Stymne Sätt jämte anordning för att avge små mängder gas från ett ämne i kondenserad form till omgivningen med kontrollerbar hastighet
US5417105A (en) * 1994-02-18 1995-05-23 Hughes Aircraft Company Flow accelerator for leak detector probe
JP3897860B2 (ja) * 1997-07-11 2007-03-28 株式会社アルバック 密閉品のリークテスト方法
US6230549B1 (en) * 1997-10-29 2001-05-15 Stant Manufacturing Inc. Hand-held fuel cap leakage tester
DE19906941A1 (de) * 1999-02-19 2000-08-24 Leybold Vakuum Gmbh Testleck
JP2004340721A (ja) * 2003-05-15 2004-12-02 Ulvac Japan Ltd 液晶パネルの封止検査方法
DE10353033A1 (de) * 2003-11-13 2005-06-09 Inficon Gmbh Verfahren zum Betrieb eines Wasserstoff-Testlecks
CN100462706C (zh) * 2005-01-06 2009-02-18 清华大学 标准漏孔
DE102005009713A1 (de) * 2005-03-03 2006-09-07 Inficon Gmbh Lecksuchgerät mit Schnüffelsonde
JP4628193B2 (ja) * 2005-06-13 2011-02-09 旭化成ホームズ株式会社 トレーサーガスの放散方法及び放散容器
DE102005028557A1 (de) * 2005-06-21 2007-01-04 Inficon Gmbh Verfahren zum Kalibrieren eines spektrometrischen Schnüffellecksuchers
DE102006016747A1 (de) * 2006-04-10 2007-10-18 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Verfahren und Vorrichtung zur Leckprüfung
DE102009012213A1 (de) * 2009-03-07 2010-09-09 Inficon Gmbh Testleck
CN201749007U (zh) * 2010-08-12 2011-02-16 爱发科东方真空(成都)有限公司 标准漏孔
DE102010050505A1 (de) * 2010-11-08 2012-05-10 Fogtec Brandschutz Gmbh & Co. Kg Dichtheitsprüfung von Rohrleitungssystem für Brandbekämpfungsanlagen
CN202836897U (zh) * 2012-10-24 2013-03-27 爱发科东方真空(成都)有限公司 检漏仪用内部校准漏孔
DE102012220108A1 (de) * 2012-11-05 2014-05-22 Inficon Gmbh Verfahren zur Prüfung einer Dichtheitsprüfanlage
US9709477B2 (en) * 2013-02-08 2017-07-18 Schlumberger Technology Corporation Apparatus and methodology for measuring properties of microporous material at multiple scales
DE102013216450A1 (de) * 2013-08-20 2015-02-26 Inficon Gmbh Pico-Prüfleck

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0110004A1 (de) * 1982-11-26 1984-06-13 Leybold Aktiengesellschaft Testleck
EP0352371A2 (en) * 1988-07-27 1990-01-31 VARIAN S.p.A. Detector for helium leaks
DE4038266A1 (de) * 1990-11-30 1992-06-04 Siemens Ag Verfahren und vorrichtung zur pruefung der gasdichtigkeit von bauteilen, insbesondere sf(pfeil abwaerts)6(pfeil abwaerts)-dichtigkeit von kondensatoren
US5663487A (en) * 1994-02-02 1997-09-02 Leybold Aktiengesellschaft Capillary tube determining the leakage rate for a test leak
EP1637861A1 (en) * 2004-09-17 2006-03-22 Ronald Douglas Collins Reference gas leak

Also Published As

Publication number Publication date
CN105531573B (zh) 2019-01-15
JP2016528509A (ja) 2016-09-15
JP2019066489A (ja) 2019-04-25
US9933325B2 (en) 2018-04-03
CN105531573A (zh) 2016-04-27
US20160195448A1 (en) 2016-07-07
EP3036518B1 (de) 2018-10-10
JP6722750B2 (ja) 2020-07-15
EP3036518A1 (de) 2016-06-29
DE102013216450A1 (de) 2015-02-26

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