WO2010008092A1 - 水硬性粉体の製造方法 - Google Patents
水硬性粉体の製造方法 Download PDFInfo
- Publication number
- WO2010008092A1 WO2010008092A1 PCT/JP2009/063227 JP2009063227W WO2010008092A1 WO 2010008092 A1 WO2010008092 A1 WO 2010008092A1 JP 2009063227 W JP2009063227 W JP 2009063227W WO 2010008092 A1 WO2010008092 A1 WO 2010008092A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- compound
- glycerin
- oxide
- hydraulic
- oxidation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B7/00—Hydraulic cements
- C04B7/36—Manufacture of hydraulic cements in general
- C04B7/48—Clinker treatment
- C04B7/52—Grinding ; After-treatment of ground cement
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/02—Alcohols; Phenols; Ethers
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/16—Sulfur-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/24—Macromolecular compounds
- C04B24/28—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B24/32—Polyethers, e.g. alkylphenol polyglycolether
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/52—Grinding aids; Additives added during grinding
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/10—Production of cement, e.g. improving or optimising the production methods; Cement grinding
Definitions
- the present invention relates to a hydraulic method for producing a hydraulic compound.
- Hardness is produced by powdering hard compounds such as Portland cement tarinka and blast furnace slurries.
- Portland cement is produced by adding an appropriate amount of tarinka obtained by firing raw materials such as apatite, clay, and iron.
- ethylene glycol triethanol alcohol is used. In the process, it is desirable to make hydraulic compounds as desirable as possible. For this reason, it has been used in the grinding process.
- oligo glycols such as propylene glycol and ethylene glycol
- alkanolamines such as triethylanol
- compounds such as stearic acid and nord
- hydroxyalkylhydrazine tassylbutyl
- glycerin is used for grinding (for example, JP A 60298)
- honglycerin is used in combination with JP A57 095 52
- an organic liquid containing a polyhydric alcohol for example, JP A200 5 8 9 2 8 7) is known.
- ethylene glycol Or triethanolol is said to have a good grinding rate and can be made relatively desirable.
- the present invention relates to a hydraulic method having a step of forming a compound.
- the present invention relates to hydraulic properties obtained by the above-mentioned method. Detailed explanation
- Ethylene glycol which is widely used as a hard compound, must be used in consideration of safety and the effects of the surface, and is a substance that has great restrictions in use. Trieta Norua is also a type of chemical weapons prohibition law.
- a hydraulic method that can secure the integrity of grinding, shorten the time to achieve the desired grinding rate, and improve the degree of hydraulicity obtained, such as cement and other hydraulics I will provide a.
- the number of hydroxyl groups in the alcohol is above 2, and below 20 is preferred. If the number of acid groups is 2 or more, the performance of the compound (a) is sufficiently exhibited, and if it is 20 or less, the function of the compound a is moderate and less performance is exhibited.
- the number of acid groups of compound A) is preferably 0 or less, more preferably 6 or less.
- the number of acid groups in A) is preferably 2 to 20, more preferably 2 to 0 and even more preferably 2 to 6.
- the prime number of the polyvalent alcohol is 2 above, preferably 3 above, and more preferably 4 above.
- the prime number of the compound (A) is preferably 30 or less, more preferably 4 or less, and further preferably 9 or less.
- a more preferred form of compound A) is a compound in which a polyvalent alcohol does not contain any element and is composed of three elements: carbon, hydrogen, and oxygen. It comes from things.
- the prime number of the polyvalent alcohol is preferably 2 to 30, more preferably 3 to 4, more preferably 4 to 4, and still more preferably 4 to 9.
- Alcohols include polyalkoxy groups 3 to 20), polyglycidol groups 3 to 20), ethylene glycol, ethylene glycol, triethylene glycol, propylene glycol, dipropylene glycol polyethylene glycol, polypropylene glycol, 4 Butanediol 6 Hexanediol, Glycerin, Diglycerin, Polyglyceric acid group number 5 to 20), Trityl ethane, Trityl propane, 3 5 Pentatriol, Erythritol, Pentaerythritol, Pentaerythritol, Tan, triglycerin compound, addtle, arabitol, xylitol, and tol are preferred.
- spasses such as glucose, fructose, nnos, indos, sorbus, gloss, talos, tagatos, galactos, alos, psikos, and altros.
- Sugars Arabinose, Ribros, Ribo, Xylose, Xylulose, Lyxus, etc.
- alcohols such as isoluto, trelos, ciutalos, raffinos, gentianos, meletos,
- ethylene glycol Polyglycerin, diglycerin, glycerin and other ethylene glycol, glycerin and their isomers are more preferred, ethylene glycol glycerin is more preferred, and glycerin is more preferred.
- AO can be used under the alkyloxy of polyhydric alcohol.
- AO is preferably selected from ethyleneoxy under E) propioxy (below).
- a compound selected from compounds obtained by adding 0.5 to 6 to 0.5, more preferably 0.5 to 3 on average, of the alkyl oxide EO of alcohol is more preferable.
- Compound a) reduces the energy on the particle surface and improves the pulverization rate, so that (A) acid groups have an average of 0 ⁇ 0, further 0 ⁇ 0 9, and further 0 ⁇ A compound obtained by reacting (oxidizing) B 7 of 0 7 and 0 ⁇ to 0 ⁇ 4 is preferable.
- B) A compound that can be used as an oxidizing agent can be used, and examples thereof include sulfuric anhydride such as gas, fuming, rusulfone, and anhydrous sulfuric acid / Lewis. Of these, B) and gas are preferred.
- the number of (A) and (B) minutes per acid group and the number of (A) and (B) minutes used for the reaction, and the number of acid groups and the amount of sodium sulfate in compound (a) The number that did not react with minutes.
- A) is preferably selected from ethylene glycol glycerin, glycerin O product and glycerin product, and more preferably selected from glycerin, glycerin EO product and glycerin product.
- (A) glycerin glycerin EO A compound selected from compounds obtained by adding 0.5 to 6 on average is more preferred. More preferred are compounds in which EO of glycerin and EO on average are preferably from 0.5 to 3 and more preferably from 0.5 to 5 on average.
- compound (a) has a (A) content of A) glycerin, and A2) the EO of glycerin is selected from POM compounds.
- Compound a) is preferred under compound a) obtained by reacting B) components of .about.0.9, 0.about.0.multidot.7, and 0.about.0.about.4.
- Such a compound a) can be used for hydraulic compounds.
- an index called oxidation can be used, but this oxidation indicates the degree to which the acid group of the A) component was oxidized. 3 ⁇ 0.
- the oxidation is preferably 0-2 to 5 and more preferably 0-2 to 0.
- (A) minutes are selected from A) and (A2) minutes, oxidation, more preferably 0 2 to 2 ⁇ 5, and further 0 ⁇ 2 to 2 ⁇ 0 are preferred.
- Compound (a) is (A) • 0-2 to 8 • 0 on average,
- a compound obtained by reacting B) of 3 to 3 ⁇ 0 is preferred. Above all, it is preferable that the minute) is selected from A) and 2) minutes. In the case where (A) is selected from A) and (A2), a compound obtained by reacting 0, 3 2 and 0 (B) is more preferred.
- Compound (a) is obtained by reacting (A) with B). This can be done according to the law of manufacture. B) S for minutes
- Anhydrous sulfuric acid such as,, fumes, chlorosulfone, anhydrous sulfuric acid and Lewis. More preferable are anhydrous sulfuric acid such as, gas, and fumes.
- oxidation methods include a method using a large excess of acid, a method using sulfonic acid, a phase method using sulfuric anhydride, and a method using gaseous sulfuric anhydride diluted with non-gas.
- Another example is a method using a thin film oxidation reaction. A method is preferred from the viewpoint of suppressing the formation of the product, and a method using gaseous sulfuric anhydride diluted with a gas is preferred from the viewpoint of being less impure and being economical.
- Compound (a) is an oxide containing (A), and usually contains (A) (sterol or complete steal). In addition, the corresponding A) component may be present in the compound a). Ming includes compound (a), which is obtained by reacting (A) and (B).
- a compound can be used.
- Compound a) can be used as from the viewpoint of improving water solubility. Examples include sodium salts and potassium-valent salts. Solubility of compound a) By improving the compound, the compound a) can be made into an aqueous solution with excellent handleability.
- Portland cement is also called tarinka cement clinker, a hydraulic compound obtained by firing raw materials such as limestone, clay, and iron, and there are cases where gypsum is present.
- the bright compound a) is used as a powder during the crushing of the hard compound, preferably tarinka, and preferably in the finish.
- the compound a is preferably 1.00 to 0 2 and more preferably 0 0 to 0 to 0 for a hard compound as a raw material used for pulverization, for example, cement clinker 0 from the viewpoint of desired pulverization in a short time.
- compound a) it is preferable to add compound a) to a material containing a hard compound such as clinker.
- the adding method include a method in which a compound (a) or a compound containing compound a and another component is supplied by or. Add a compound obtained by reacting A and B) to a solid aluminum cup (if neutralized, neutralized solution) 3, measure the weight and let 2 at 5C Measure the weight again, and then calculate it by calculation.
- the compound (a may be an aqueous solution from the viewpoint of easy handling. 40 to 99 of the compound a) is preferable.
- a hard compound is a substance that reacts with water to form a compound and one compound that does not have curability, but when two or more are combined, forms a hydration through water and forms a hydrate.
- alkalinized substances and polyvalent compounds such as SO, A 1 O, PO, and Z are Form.
- An example of the hard compound is slatalinker.
- the hydraulic compound is preferably cement tarinka.
- the condition of pulverization may be adjusted so that a suitable diameter can be obtained.
- a hydraulic compound for example, talinka
- the target brain value can be obtained, for example, by adjusting the interval. Increasing the interval tends to increase the blend value, and shortening the interval tends to decrease the blend value.
- hydraulic compounds are not particularly limited, and examples thereof include cement used as cement. It is desirable to have a higher hardness (for example, in the case of cement tarinka in the case of cement tarinka).
- a clear compound a) which can include tungsten carbide, etc., is used as a hydraulic compound, is excellent in safety, has a good pulverization rate, and can improve the degree of concretion.
- the light compounds a), in particular the compounds a) are suitable as powders for hydraulic compounds, in particular for tarinka. That is, when a hydraulic compound is produced, a method of hydraulic compound using compound a), especially compound (a) is provided as a pulverization. It is preferable to use the above-mentioned compound (a 00 to 0 ⁇ 2, more preferably 0 ⁇ 0 0 5 to 0 ⁇ , and further Z00 2 to 0 ⁇ 06) in solid form.
- the hydraulic properties and strength obtained by the Ming method include Portland cement, blast furnace slurry, alumina cement, fly assy, and limestone.
- the hydraulic compounds used for grinding are: It is a hydraulic material.
- the hydraulic compound when the hydraulic compound includes the cement tarinka, it may be replaced with the amount based on the cement tarinka.
- the amount relative to hydraulic compound 0 may be relative to hydraulic compound cement tarinker 0.
- the hard compound is a cement clinker, and the cement clinker is 0.
- the hard compound is a mixture of cement clinker. Part.
- ⁇ Talinka is C aO 6 5 S O 2 2 2
- Oxidized with C. S was used as the oxidizing agent.
- S was prepared as follows. After mixing with the dissolved moisture, it burned to produce sulfur dioxide (). Then, sulfur dioxide and gas were mixed and passed through a tube filled with vanadium oxide) to produce 5 degrees of S. Furthermore, the SO was mixed with air to prepare the S.
- Glycerol was oxidized using a thin-film oxidation reaction 4 (length 4 m) and S (gas), and the reaction mole (glycerin 0/89, temperature 47 to 68 was oxidized. SO was prepared in the same manner as in the production. Oxide 26 8 7 29 0 3) was added to 7 3 in 8 ⁇ 5 sodium oxide solution to prepare an aqueous solution, and a solution of glycerin oxide (compound a) and oxide 0 ⁇ 9) was added. Obtained. Of solution is 8 ⁇ 7,
- the product was synthesized in the same manner as described above at a temperature of 49 to 6 (mol of glycerin-5 oxide), and a solution of glycerin oxide (compound a) 3) oxidation 2) was obtained.
- the solution was 9 ⁇ 7, 66 ⁇ 9 and sodium was 3 3.
- the yield based on the Stealth combination was confirmed. From the composition ratio determined from the proton spectrum fraction, the oxides of glycerin 9.4 glycerin oxide 3 29, 2 glycerin oxide 7 4,, 2 glycerin oxide 8 9, 3 glycerin oxide 20 6 2 glycerin oxide (7 wt).
- Methylformamide M 7 94 5 S O 87 ⁇ 09 9) was intercalated with C. Furthermore, glycerin 00 0 9) was applied over 30 times. It was 0 until the end. Ion 20000 was poured into the compound and neutralized with 3 2 sodium oxide solution 42 7 4).
- Methylformamide (DM) was added with a Tali evaporator, and further ions were added to obtain a solution 8 83 of a reaction product glycerin oxide (compound (a) of 4) and 0).
- the solution is 3 Was 5C, 2) was 7 3 6, and sodium was 0.3.
- the yield based on Steal was confirmed. From the compositional ratio determined from the Proton SpE ratio, the oxides were glycerin 3 24 and 2 3 glycerin oxide 6 weights).
- the production EO was glycerin (EO 0) 2 9 EO 3 EO 2 22 4 E 3 26 E 4 9 7 O 5 7 EO 6 4 6 E 7 7 E 8 0 5 EO 9 0 2).
- the glycerin EO 3 obtained in () was synthesized at the reaction mole (glycerin 0 oxide 8 8 7) at a temperature of 4 2 to 5 6 and synthesized in the same manner.
- Stainless steel pot 8 liter (300) is used for Seiwa AX 5 company, and stainless steel ball is 30 (• 3 6) is 70, 20 (3 4) is 70, using a total of 0 balls. Lumi's 45. Also discharge the crushed in The time to perform was set to be between.
- the blend value is 3300 m, the blend value after 60, 75, 90 after the start of grinding is measured, and the time to reach the target blend 3300 is final by quadratic regression) It was.
- the Bren value was measured and a cement unit (J S R 520) t was used. In this study, the difference in level appears. The evaluation was performed when the comparison period was set to 0, and the relative 90-degree was evaluated as below, and the value exceeding 90 was determined as acceptable. In comparison, the comparison was 24 minutes. Is described as a standard in.
- the cement that was used was that of the blend 3 3 0 0 0 0 2 obtained above.
- the evaluation was performed when the degree of comparison was 0, and when it was 3 degrees, A was greater than 0, B was 0 to 0 and 0, and C was 0. In the case of 7 degrees, relative over 5 was designated as A, 0 to below B as B, and 0 below as C.
- 29 after comparison, 29 g
- EOP is the number of moles of ethylene oxide.
- the comparison was performed by adding only water to the amount of tarinka by 0.04.
- Comparison 2 is a reaction between a polyhydric alcohol or a polyhydric alcohol and a oxidant. (Compound compound). From this comparison, it can be seen that the degree is improved by reacting with an oxidizing agent.
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Polyethers (AREA)
Abstract
Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09798016.3A EP2301901B1 (en) | 2008-07-18 | 2009-07-16 | Method for producing hydraulic powder |
MX2010013576A MX2010013576A (es) | 2008-07-18 | 2009-07-16 | Metodo para producir polvo hidraulico. |
CN2009801280914A CN102099311B (zh) | 2008-07-18 | 2009-07-16 | 水硬性粉体的制造方法 |
BRPI0913899A BRPI0913899A2 (pt) | 2008-07-18 | 2009-07-16 | métodos para produzir um pó hidráulico, e pó hidráulico |
US13/001,634 US8567703B2 (en) | 2008-07-18 | 2009-07-16 | Method for producing hydraulic powder |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2008187726 | 2008-07-18 | ||
JP2008-187726 | 2008-07-18 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2010008092A1 true WO2010008092A1 (ja) | 2010-01-21 |
Family
ID=41550492
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/JP2009/063227 WO2010008092A1 (ja) | 2008-07-18 | 2009-07-16 | 水硬性粉体の製造方法 |
Country Status (8)
Country | Link |
---|---|
US (1) | US8567703B2 (ja) |
EP (1) | EP2301901B1 (ja) |
JP (1) | JP5283580B2 (ja) |
KR (1) | KR20110052567A (ja) |
CN (1) | CN102099311B (ja) |
BR (1) | BRPI0913899A2 (ja) |
MX (1) | MX2010013576A (ja) |
WO (1) | WO2010008092A1 (ja) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2010024099A (ja) * | 2008-07-18 | 2010-02-04 | Kao Corp | 水硬性組成物用早強剤 |
WO2014148522A1 (ja) * | 2013-03-22 | 2014-09-25 | 花王株式会社 | 水硬性粉体の製造方法 |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2336100A1 (de) * | 2009-12-08 | 2011-06-22 | Sika Technology AG | Zusatzmittel für mineralische Bindemittel mit verringertem Braunverfärbungspotential |
JP5805442B2 (ja) * | 2011-06-24 | 2015-11-04 | 花王株式会社 | 水硬性粉体の製造方法 |
FR2997319B1 (fr) * | 2012-10-26 | 2014-11-14 | Lafarge Sa | Procede, ensemble de broyage et fabrication d'un liant hydraulique |
JP5802815B2 (ja) * | 2013-09-27 | 2015-11-04 | 花王株式会社 | 水硬性粉体の製造方法 |
CN103626421A (zh) * | 2013-11-29 | 2014-03-12 | 安徽新创建材科技有限公司 | 一种增强型水泥助磨剂及其制备方法 |
CN105084821A (zh) * | 2015-08-12 | 2015-11-25 | 安徽砼宇特构科技有限公司 | 高强度钢筋混凝土箱涵及其制备方法 |
CN112159149A (zh) * | 2020-08-26 | 2021-01-01 | 信阳市灵石科技有限公司 | 一种水泥助磨剂及其制备方法 |
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2009
- 2009-07-16 WO PCT/JP2009/063227 patent/WO2010008092A1/ja active Application Filing
- 2009-07-16 MX MX2010013576A patent/MX2010013576A/es active IP Right Grant
- 2009-07-16 EP EP09798016.3A patent/EP2301901B1/en not_active Not-in-force
- 2009-07-16 US US13/001,634 patent/US8567703B2/en not_active Expired - Fee Related
- 2009-07-16 BR BRPI0913899A patent/BRPI0913899A2/pt not_active Application Discontinuation
- 2009-07-16 CN CN2009801280914A patent/CN102099311B/zh active Active
- 2009-07-16 KR KR1020117000532A patent/KR20110052567A/ko not_active Application Discontinuation
- 2009-07-17 JP JP2009168694A patent/JP5283580B2/ja active Active
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JPS6172664A (ja) * | 1984-09-17 | 1986-04-14 | 第一工業製薬株式会社 | 水中コンクリ−ト用混和剤 |
JPS6183659A (ja) * | 1984-10-01 | 1986-04-28 | 鹿島建設株式会社 | セメント添加剤 |
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Publication number | Priority date | Publication date | Assignee | Title |
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JP2010024099A (ja) * | 2008-07-18 | 2010-02-04 | Kao Corp | 水硬性組成物用早強剤 |
WO2014148522A1 (ja) * | 2013-03-22 | 2014-09-25 | 花王株式会社 | 水硬性粉体の製造方法 |
JP2014185049A (ja) * | 2013-03-22 | 2014-10-02 | Kao Corp | 水硬性粉体の製造方法 |
CN105026334A (zh) * | 2013-03-22 | 2015-11-04 | 花王株式会社 | 水硬性粉体的制造方法 |
CN105026334B (zh) * | 2013-03-22 | 2017-06-06 | 花王株式会社 | 水硬性粉体的制造方法 |
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EP2301901B1 (en) | 2014-03-26 |
US20110100264A1 (en) | 2011-05-05 |
MX2010013576A (es) | 2011-02-15 |
BRPI0913899A2 (pt) | 2015-10-27 |
JP2010042986A (ja) | 2010-02-25 |
US8567703B2 (en) | 2013-10-29 |
KR20110052567A (ko) | 2011-05-18 |
CN102099311B (zh) | 2013-12-04 |
JP5283580B2 (ja) | 2013-09-04 |
EP2301901A4 (en) | 2013-01-02 |
CN102099311A (zh) | 2011-06-15 |
EP2301901A1 (en) | 2011-03-30 |
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