WO2008081923A1 - プルシアンブルー型金属錯体ナノ粒子の製造方法、並びにそれにより得られるプルシアンブルー型金属錯体ナノ粒子、その分散液、その発色制御方法、それを用いた電極及び透過光制御装置 - Google Patents

プルシアンブルー型金属錯体ナノ粒子の製造方法、並びにそれにより得られるプルシアンブルー型金属錯体ナノ粒子、その分散液、その発色制御方法、それを用いた電極及び透過光制御装置 Download PDF

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Publication number
WO2008081923A1
WO2008081923A1 PCT/JP2007/075265 JP2007075265W WO2008081923A1 WO 2008081923 A1 WO2008081923 A1 WO 2008081923A1 JP 2007075265 W JP2007075265 W JP 2007075265W WO 2008081923 A1 WO2008081923 A1 WO 2008081923A1
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WO
WIPO (PCT)
Prior art keywords
nanoparticles
prussian blue
type metal
metal complex
blue type
Prior art date
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PCT/JP2007/075265
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English (en)
French (fr)
Inventor
Tohru Kawamoto
Hisashi Tanaka
Shigeo Hara
Masato Kurihara
Masaomi Sakamoto
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National Institute Of Advanced Industrial Science And Technology
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Publication date
Application filed by National Institute Of Advanced Industrial Science And Technology filed Critical National Institute Of Advanced Industrial Science And Technology
Priority to US12/521,520 priority Critical patent/US8349221B2/en
Priority to EP07860468.3A priority patent/EP2116511B1/en
Priority to JP2008552178A priority patent/JP5697068B2/ja
Publication of WO2008081923A1 publication Critical patent/WO2008081923A1/ja

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/08—Simple or complex cyanides of metals
    • C01C3/11—Complex cyanides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/08—Simple or complex cyanides of metals
    • C01C3/12—Simple or complex iron cyanides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/32—Inkjet printing inks characterised by colouring agents
    • C09D11/322—Pigment inks
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
    • G—PHYSICS
    • G02—OPTICS
    • G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
    • G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour 
    • G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect
    • G02F1/1514—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material
    • G02F1/1516—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material comprising organic material
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • G—PHYSICS
    • G02—OPTICS
    • G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
    • G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour 
    • G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect
    • G02F1/153—Constructional details
    • G02F1/157—Structural association of cells with optical devices, e.g. reflectors or illuminating devices
    • G—PHYSICS
    • G02—OPTICS
    • G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
    • G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour 
    • G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect
    • G02F1/1514—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material
    • G02F1/1516—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour  based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material comprising organic material
    • G02F2001/1517—Cyano complex compounds, e.g. Prussian blue
    • G—PHYSICS
    • G02—OPTICS
    • G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F2202/00—Materials and properties
    • G02F2202/36—Micro- or nanomaterials

Abstract

　プルシアンブルー型金属錯体ナノ粒子、その分散液、その発色制御方法、それを用いた電極及び透過光制御装置を提供するものであって、所定の金属原子ＭＡを中心金属とする金属シアノ錯体陰イオンを含有する水溶液と、所定の金属原子ＭＢの陽イオンを含有する水溶液とを混合し、前記金属原子ＭＡ及び金属原子ＭＢを有するプルシアンブルー型金属錯体の結晶を析出させ、次いで、該プルシアンブルー型金属錯体と、所定の金属原子ＭＣを中心金属とする金属シアノ錯体陰イオンを含有する水溶液および／または所定の金属原子ＭＤの陽イオンを含有する水溶液とを混合してプルシアンブルー型金属錯体ナノ粒子を製造する。  
PCT/JP2007/075265 2006-12-28 2007-12-28 プルシアンブルー型金属錯体ナノ粒子の製造方法、並びにそれにより得られるプルシアンブルー型金属錯体ナノ粒子、その分散液、その発色制御方法、それを用いた電極及び透過光制御装置 WO2008081923A1 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US12/521,520 US8349221B2 (en) 2006-12-28 2007-12-28 Method of producing prussian blue-type metal complex nanoparticles, and prussian blue-type metal complex nanoparticles obtained by the method, dispersion of the nanoparticles, method of regulating the color of the nanoparticles, and electrode and transmitted light-regulator each using the nanoparticles
EP07860468.3A EP2116511B1 (en) 2006-12-28 2007-12-28 Method of regulating the color of prussian blue type metal complex nanoparticles, prussian blue type metal complex nanoparticle obtained by the same, dispersion of the nanoparticles, electrode and transmitted-light regulator both employing the nanoparticles
JP2008552178A JP5697068B2 (ja) 2006-12-28 2007-12-28 プルシアンブルー型金属錯体ナノ粒子の製造方法、並びにそれにより得られるプルシアンブルー型金属錯体ナノ粒子、その分散液、その発色制御方法、それを用いた電極及び透過光制御装置

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2006-355513 2006-12-28
JP2006355513 2006-12-28
JP2007-241576 2007-09-18
JP2007241576 2007-09-18

Publications (1)

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WO2008081923A1 true WO2008081923A1 (ja) 2008-07-10

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US (1) US8349221B2 (ja)
EP (1) EP2116511B1 (ja)
JP (1) JP5697068B2 (ja)
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Cited By (19)

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US7678188B2 (en) * 2005-02-17 2010-03-16 National Institute Of Advanced Industrial Science And Technology Ultrafine particles of Prussian blue-type metal complex, dispersion liquid thereof and their production methods
JP2010113892A (ja) * 2008-11-05 2010-05-20 Univ Of Tsukuba 電圧駆動素子、電池、表示装置、磁性制御装置および反転対称性制御装置
JP2010261085A (ja) * 2009-05-08 2010-11-18 Japan Science & Technology Agency グラファイト被覆金属ナノ粒子の製造方法及びグラファイト被覆金属ナノ粒子の薄膜化方法
WO2011030790A1 (ja) * 2009-09-09 2011-03-17 独立行政法人産業技術総合研究所 電気化学素子及びその製造方法
WO2011106309A2 (en) * 2010-02-23 2011-09-01 Kent State University Materials and methods for mri contrast agents and drug delivery
JP2011180469A (ja) * 2010-03-03 2011-09-15 National Institute Of Advanced Industrial Science & Technology プルシアンブルー型金属錯体ナノ粒子を具備する電気化学素子、これを用いたエレクトロクロミック素子及び二次電池
JP2011246303A (ja) * 2010-05-26 2011-12-08 National Institute Of Advanced Industrial Science & Technology プルシアンブルー類似体を用いたリチウムイオン２次電池電極材料
JPWO2009157554A1 (ja) * 2008-06-27 2011-12-15 独立行政法人産業技術総合研究所 プルシアンブルー型金属錯体ナノ粒子構造体の製造方法、これにより得られる構造体、これを用いた構造体配設基板、エレクトロクロミック素子、整流装置、及び光応答素子
JP2012072015A (ja) * 2010-09-28 2012-04-12 National Institute Of Advanced Industrial Science & Technology 金属錯体ナノ粒子及びその製造方法
JP2013201018A (ja) * 2012-03-23 2013-10-03 National Institute Of Advanced Industrial Science & Technology 照明装置
JP2014052645A (ja) * 2013-10-07 2014-03-20 Univ Of Tsukuba 電圧駆動素子および表示装置
JP2015101523A (ja) * 2013-11-27 2015-06-04 国立研究開発法人産業技術総合研究所 プルシアンブルー型錯体ナノ粒子の合成方法及び該方法で合成されたプルシアンブルー型錯体ナノ粒子
JP2018021113A (ja) * 2016-08-02 2018-02-08 国立研究開発法人産業技術総合研究所 エレクトロクロミック材料、これを用いた色可変電極及び素子
WO2018025939A1 (ja) * 2016-08-02 2018-02-08 国立研究開発法人産業技術総合研究所 エレクトロクロミック素子及びエレクトロクロミック材料
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