WO2006050903A3 - Katalysator zur herstellung von kohlenstoffnanoröhrchen durch zersetzung von gasförmigen kohlenstoffverbindungen an einem heterogenen katalysator - Google Patents

Katalysator zur herstellung von kohlenstoffnanoröhrchen durch zersetzung von gasförmigen kohlenstoffverbindungen an einem heterogenen katalysator Download PDF

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Publication number
WO2006050903A3
WO2006050903A3 PCT/EP2005/011925 EP2005011925W WO2006050903A3 WO 2006050903 A3 WO2006050903 A3 WO 2006050903A3 EP 2005011925 W EP2005011925 W EP 2005011925W WO 2006050903 A3 WO2006050903 A3 WO 2006050903A3
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WO
WIPO (PCT)
Prior art keywords
catalyst
decomposition
carbon nanotubes
heterogeneous catalyst
producing carbon
Prior art date
Application number
PCT/EP2005/011925
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English (en)
French (fr)
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WO2006050903A2 (de
Inventor
Sigurd Buchholz
Daniel Gordon Duff
Volker Michele
Leslaw Mleczko
Christian Muennich
Reiner Rudolf
Aurel Wolf
Original Assignee
Bayer Technology Services Gmbh
Sigurd Buchholz
Daniel Gordon Duff
Volker Michele
Leslaw Mleczko
Christian Muennich
Reiner Rudolf
Aurel Wolf
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Bayer Technology Services Gmbh, Sigurd Buchholz, Daniel Gordon Duff, Volker Michele, Leslaw Mleczko, Christian Muennich, Reiner Rudolf, Aurel Wolf filed Critical Bayer Technology Services Gmbh
Priority to KR1020077010697A priority Critical patent/KR101292489B1/ko
Priority to CN200580046507XA priority patent/CN101142020B/zh
Priority to JP2007540559A priority patent/JP5702043B2/ja
Priority to EP05816390A priority patent/EP1812159A2/de
Priority to US11/719,152 priority patent/US9409779B2/en
Priority to TW095104720A priority patent/TW200730245A/zh
Publication of WO2006050903A2 publication Critical patent/WO2006050903A2/de
Publication of WO2006050903A3 publication Critical patent/WO2006050903A3/de

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C01B32/162—Preparation characterised by catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/10—Magnesium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/889—Manganese, technetium or rhenium
    • B01J23/8892—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/889—Manganese, technetium or rhenium
    • B01J23/8898—Manganese, technetium or rhenium containing also molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B82B3/0004—Apparatus specially adapted for the manufacture or treatment of nanostructural devices or systems or methods for manufacturing the same
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y10/00—Nanotechnology for information processing, storage or transmission, e.g. quantum computing or single electron logic
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/20—Carbon compounds, e.g. carbon nanotubes or fullerenes
    • H10K85/221—Carbon nanotubes
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60—Organic compounds having low molecular weight
    • H10K85/615—Polycyclic condensed aromatic hydrocarbons, e.g. anthracene
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/34—Length
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/36—Diameter

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Mathematical Physics (AREA)
  • Theoretical Computer Science (AREA)
  • Composite Materials (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Catalysts (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

Die vorliegende Erfindung betrifft ein Verfahren zur Herstellung von Kohlenstoffnanoröhrchen, insbesondere solcher mit einem Durchmesser von 3-150 nm und einem Aspektverhältnis Länge: Durchmesser (L:D) > 100 durch Zersetzung von Kohlenwasserstoffen an einem heterogenen Katalysator, der Mn, Co, bevorzugt auch Molybdän, sowie ein inertes Trägermaterial enthält sowie den Katalysator und die Kohlenstoffnanoröhrchen selbst und deren Verwendung.
PCT/EP2005/011925 2004-11-13 2005-11-08 Katalysator zur herstellung von kohlenstoffnanoröhrchen durch zersetzung von gasförmigen kohlenstoffverbindungen an einem heterogenen katalysator WO2006050903A2 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
KR1020077010697A KR101292489B1 (ko) 2004-11-13 2005-11-08 불균질 촉매 상 기체 탄소 화합물의 분해에 의한 탄소나노튜브의 제조용 촉매
CN200580046507XA CN101142020B (zh) 2004-11-13 2005-11-08 用于通过在非均相催化剂上分解气态碳化合物而制备碳纳米管的催化剂
JP2007540559A JP5702043B2 (ja) 2004-11-13 2005-11-08 不均一触媒でガス状炭素化合物を分解することによりカーボンナノチューブを製造するための触媒
EP05816390A EP1812159A2 (de) 2004-11-13 2005-11-08 Katalysator zur herstellung von kohlenstoffnanoröhrchen durch zersetzung von gasförmigen kohlenstoffverbindungen an einem heterogenen katalysator
US11/719,152 US9409779B2 (en) 2004-11-13 2005-11-08 Catalyst for producing carbon nanotubes by means of the decomposition of gaseous carbon compounds on a heterogeneous catalyst
TW095104720A TW200730245A (en) 2004-11-13 2006-02-13 Catalyst for producing carbon nanotubules by decomposition of gaseous carbon compouds at a heterogeneous catalyst

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102004054959A DE102004054959A1 (de) 2004-11-13 2004-11-13 Katalysator zur Herstellung von Kohlenstoffnanoröhrchen durch Zersetzung von gas-förmigen Kohlenverbindungen an einem heterogenen Katalysator
DE102004054959.1 2004-11-13

Publications (2)

Publication Number Publication Date
WO2006050903A2 WO2006050903A2 (de) 2006-05-18
WO2006050903A3 true WO2006050903A3 (de) 2006-09-08

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2005/011925 WO2006050903A2 (de) 2004-11-13 2005-11-08 Katalysator zur herstellung von kohlenstoffnanoröhrchen durch zersetzung von gasförmigen kohlenstoffverbindungen an einem heterogenen katalysator

Country Status (8)

Country Link
US (1) US9409779B2 (de)
EP (1) EP1812159A2 (de)
JP (1) JP5702043B2 (de)
KR (1) KR101292489B1 (de)
CN (1) CN101142020B (de)
DE (1) DE102004054959A1 (de)
TW (1) TW200730245A (de)
WO (1) WO2006050903A2 (de)

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US9409779B2 (en) 2016-08-09
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