WO2003030839A1 - Cosmetique contenant de l'eau de mer electrolysee provenant des grands fonds oceaniques - Google Patents

Cosmetique contenant de l'eau de mer electrolysee provenant des grands fonds oceaniques Download PDF

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Publication number
WO2003030839A1
WO2003030839A1 PCT/JP2001/008509 JP0108509W WO03030839A1 WO 2003030839 A1 WO2003030839 A1 WO 2003030839A1 JP 0108509 W JP0108509 W JP 0108509W WO 03030839 A1 WO03030839 A1 WO 03030839A1
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WO
WIPO (PCT)
Prior art keywords
water
acid
cosmetic
oil
present
Prior art date
Application number
PCT/JP2001/008509
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English (en)
Japanese (ja)
Inventor
Kazuo Nakajima
Akiko Usui
Hisanari Shibata
Shunichi Oki
Tamotsu Furumai
Original Assignee
Toyama Chemical Co., Ltd.
Kawaken Fine Chemicals Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to JP2000097915A priority Critical patent/JP2001278735A/ja
Application filed by Toyama Chemical Co., Ltd., Kawaken Fine Chemicals Co., Ltd. filed Critical Toyama Chemical Co., Ltd.
Priority to PCT/JP2001/008509 priority patent/WO2003030839A1/fr
Publication of WO2003030839A1 publication Critical patent/WO2003030839A1/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/83—Electrophoresis; Electrodes; Electrolytic phenomena

Definitions

  • the present invention relates to a cosmetic containing electrolytic deep sea water. More specifically, the present invention relates to an electrolytic deep sea water-containing cosmetic containing electrolyzed water obtained by electrolyzing deep sea water and having excellent moisturizing properties.
  • cosmetics use water obtained by subjecting groundwater or the like to physical filtration and treatment or sterilization, so-called ordinary water, or purified water obtained by distilling and purifying ordinary water.
  • water is used for the purpose of diluting cosmetic preparations.
  • Japanese Patent Application Laid-Open No. 11-12154 discloses that deep sea water enhances the moisturizing ability of cosmetics and prevents bulkiness and rough skin. However, the effect is not fully satisfactory, and the emergence of new water that can enhance the ability to moisturize the skin and hair has been anticipated.
  • An object of the present invention is to provide a cosmetic having excellent moisturizing properties that prevents the skin and hair from becoming bulky and rough, and gives the skin and hair firmness and moisture.
  • the present inventors include, in cosmetics, electrolytic deep sea water obtained by electrolyzing deep sea water or a mixture of deep sea water and working water selected from groundwater, purified water, and tap water. And improved the moisture retention, and completed the present invention.
  • Cosmetics containing electrolytic deep water obtained by electrolyzing deep sea water or a mixed water containing deep sea water have not yet been known at all.
  • the electrolytic deep sea water-containing cosmetic composition of the present invention comprises a cosmetic component and water, wherein the water contains 0.0] to 100% by weight of deep sea water collected from a deep sea part at a depth of 200 m or less.
  • the electrolyzed raw water contained in a given amount is provided with electrolytic water generated on one of the cathode side and the cathode side.
  • the electrolytic water is weakly basic mineral water generated on the negative electrode side.
  • deep sea water means water collected from the deep sea below 200 m deep, and also includes physical filtration, reverse osmosis filtration, electrodialysis or ion exchange. At least one type of treatment selected and concentrated to 1/10 to 1/100, and the precipitates (such as sodium chloride crystals) are removed by filtration. Includes those obtained by diluting the filtrate obtained to the original volume with purified water, groundwater, spring water, tap water, or other common water.
  • the raw water supplied to the electrolyzer contains the deep sea water in a content of 0.01 to 100% by weight, preferably 1.0 to 100% by weight, and is mixed with the deep sea water.
  • the other water used is generally used for cosmetics production, and can be selected from, for example, purified water, groundwater, spring water, tap water, and other common waters, but may be distilled water and / or ion exchange resin. It is preferable to use treated purified water.
  • the deep sea water used in the present invention is not limited to an intake site as long as it is seawater collected from a place 200 meters below the sea level or deeper in the ocean. This includes offshore Muroto-misaki in Kochi Prefecture, Suruga Bay in Shizuoka Prefecture, and Kumejima in Okibashi Prefecture, etc., and globally, those collected from offshore of Nonolle-ichi and offshore of Hawaii.
  • the effect of increasing the moisturizing power of the present invention becomes insufficient.
  • Deep sea water and deep sea water dilution water are electrolyzed as raw water in an electrolyzer by a known method.
  • so-called weakly acidic water is generated on the anode side
  • so-called weakly basic mineral water is generated on the cathode side.
  • the cosmetic of the present invention prepared by blending a water component containing each of the two with a cosmetic component exhibits the moisturizing effect.
  • acidic water and weakly basic Any of mineral water can be selected and used.
  • the weakly basic mineral water and the weakly acidic water are each diluted with a common water to a desired fold, preferably 100 fold or less, to form a cosmetic. Can be used as a water component.
  • the electrolyzer used in the present invention is not particularly limited as long as it is used for electrolyzing water.
  • a two-chamber type separated by a diaphragm a DC voltage is used.
  • a three-pole type that switches between lip-flop circuits to perform alternating current charging Japanese Patent Laid-Open No. 6-254567
  • Examples include a type for continuously supplying water from tap water and the like.
  • the present invention is a preferred electrolyzer, for example, a ferrite electrode, a platinum metal titanium electrode, a titanium platinum fired electrode, or the like as an anode, and a stainless steel electrode as a cathode.
  • a two-tank water-storage type electrolysis apparatus configured by using a platinum-medium titanium electrode, a titanium platinum fired electrode, or the like, and using an ion exchange membrane or the like as a diaphragm is used.
  • cosmetic ingredients in the present invention include hair growth agents, bath agents, and medicated cosmetics specified in the Pharmaceutical Affairs Law, that is, medicated stones, medicated shampoos, medicated rinses, medicated lotions, and medicated cosmetics.
  • Cosmetics can be prepared by using a combination of ordinary water used for general cosmetics and electrolytic deep water. It is also possible to subject the electrolytic deep water to a desalination treatment using a reverse osmosis membrane to control the salt concentration to a desired value, and mix it with a cosmetic ingredient.
  • the cosmetics of the present invention include components usually used in cosmetics, such as animals, plants, fish and shellfish, extracts derived from microorganisms, powder components, liquid fats and oils, solid fats and oils, roux, hydrocarbons, higher fatty acids, and higher alcohols.
  • Esters silicones, anionic surfactants, cationic surfactants, amphoteric surfactants, nonionic surfactants, humectants, water-soluble polymers, thickeners, coating agents, ultraviolet absorbers, anti-inflammatory agents , Sequestering agents, lower alcohols, sugars, amino acids, organic amines, synthetic resin emulsions, pH adjusters, skin nourishes, vitamins, antioxidants, antioxidants, fragrances , And / or two or more kinds of ordinary water may be used as necessary.
  • the cosmetic of the present invention includes, as a part of the cosmetic ingredient, extracts derived from animals, plants, fish and shellfish, and microorganisms, for example, tea extract, aloe extract, ginkgo extract, assembly kiss, mugwort extract, and garlic extract. Extracts such as corn extract, rosemary extract, luffa extract, placenta extract, lactic acid bacteria culture extract and seaweed extract can be used in combination.
  • the powder component that can be used as a cosmetic component in the cosmetic of the present invention includes inorganic powders such as talc, kaolin, mica, sericite (cellite), muscovite, phlogopite, Synthetic mica, biotite, biotite, lithium mica, vercumite, magnesium carbonate, zirconium silicate, aluminum silicate, barium silicate, calcium silicate, zinc silicate, magnesium silicate, strontium silicate, tungsten Acid metal salts, magnesium, silica, zeolite, barium sulfate, calcined calcium sulfate (calcined ⁇ ), phosphoric acid phosphate, fluorine apatite, hydroxyapatite, ceramic knock.
  • inorganic powders such as talc, kaolin, mica, sericite (cellite), muscovite, phlogopite, Synthetic mica, biotite, biotite, lithium mica, vercumite, magnesium carbonate
  • Activated charcoal, activated charcoal, medicinal charcoal, metal stones (zinc myristate, calcium palmitate, aluminum stearate, etc.), boron nitride, etc. are examples of organic powders.
  • Polyamide resin powder Nylon powder
  • Polyethylene powder Polymethyl methacrylate powder
  • Polystyrene powder Copolymer resin powder of styrene and acrylic acid
  • Benzoguanamine Resin powder polytetrafluoroethylene powder
  • cellulose powder cellulose powder.
  • liquid fats and oils used in the cosmetic of the present invention include apogado oil, camellia oil, grape seed oil, turtle oil, madi diana nats oil, corn oil, mink oil, Olive oil, sunflower oil, rapeseed oil, egg yolk oil, sesame oil, parsley oil, wheat germ oil, southern power oil, castor oil, linseed oil, safflower oil, cottonseed oil, eno oil, soybean oil, peanut oil , Teaseed oil, cocoa oil, Komenu oil, Shinagiri oil, Japanese krill oil, jojoba oil, germ oil, triglycerin, trioctanoic acid glycerin, triisopalmitic acid glycerin No.
  • the solid fat used in the cosmetic of the present invention includes cocoa butter, coconut oil, horse fat, hardened coconut oil, palm oil, tallow, sheep fat, hardened tallow, palm kernel oil, lard, beef bone fat , Butterflies, hardened oil, beef tallow, mokurou, hardened castor oil, and the like.
  • hydrocarbon oil used in the cosmetic of the present invention examples include liquid paraffin, ozokerite, squalene, pristane, and the like.
  • examples include Raffin, Seresin, Screenan, Vaseline, and Micro-Crystallin Wax.
  • the higher fatty acids include rauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, oleic acid, 12-hydroxyxesteric acid, pendecylenic acid, Tall oil fatty acids, coconut oil fatty acids, palm fatty acids, palm kernel fatty acids, isostearic acid, linoleic acid, linoleic acid, eicosapentaenoic acid, docosahexaenoic acid and the like.
  • Examples of the synthetic ester oil used in the cosmetic of the present invention include isopropyl isopropyl myristate, cetyl octanoate, octyl dodecyl myristate, isopyl palmitate, and stearin.
  • silicones used in the cosmetic of the present invention include dimethylsilicone oil, methylpolysiloxane, octamethyltrisiloxane, high-polymerization degree methylsiloxane, decamethylpolysiloxane, dodecamecene. Chilpolysiloxane xantante tramethyltilde hydrazidepolysiloxane, dimethylsiloxane.Methyl (polyoxyethylene) siloxane copolymer, dimethylsiloxane / methyl (polyoxyethylene) siloxane, Examples thereof include a methyl (polyoxypropylene) siloxane copolymer and an amino-modified silicone.
  • anion activator used in the cosmetic of the present invention examples include a fatty acid soap, for example, a base material for a soap, sodium laurate, sodium palmitate, and coconut soap , Higher alkyl sulfates, such as sodium lauryl sulfate, potassium laurino sulfate, triethanolamine lauryl sulfate; alkyl ether sulfates, such as POE Triarylethanol laurate sulfate, POE Sodium laurate sulfate; N-acylaminate, such as lauroylsarco cinnatrium, lauroyl jS—araninna Triuium, Lauroyno N-methyl-1-alanine sodium, sodium rauroylglutamate Monosodium, sodium stearoinoleglutamate Ginatridium, ⁇ -Myristolyl L-Monosodium glutamate, ⁇ -Palmitoinolespartate diethanolamine, Palm fatty acid soap
  • Examples of the cationic surfactant used in the cosmetic of the present invention include alkyltrimethylammonium salts, for example, stearyl trimethylammonium chloride, laminole trimethylammonium chloride.
  • alkyltrimethylammonium salts for example, stearyl trimethylammonium chloride, laminole trimethylammonium chloride.
  • amphoteric surfactant used in the cosmetic of the present invention examples include amide amide amphoteric surfactants, for example, 2-indesyl- ⁇ -carboxymethyl- ⁇ -hydroxishetinoreimidazolium.
  • nonionic surfactant used in the cosmetic of the present invention examples include glycerin fatty acid esters such as glyceryl monostearate and self-emulsifying glyceryl monostearate.
  • Glyceryl monoisostearate polyoxyethylene glyceryl fatty acid esters, such as monostearic acid and glycerol monooleate POE glyceryl acid
  • polyglycerin fatty acid esters for example, diglyceryl monostearate, tetraglyceryl tristearate, decaglyceryl pentastearate
  • Sorbitan fatty acid esters for example, sorbitan monolaurate, sonorebitan sesquistearate, sorbitan monooleate
  • fatty acid esters of polyoxyethylene sorbitan for example, POE sorbitan monococonut fatty acid POE sonorebitan stearate, POE sonorebitan trioleate
  • polyoxyethylene sorbite fatty acid esters for
  • humectant used in the cosmetic of the present invention examples include glycerin, propylene glycol, 1,3-butylene glycol, sonorebitol, sodium lactate, pyrrolidone rubonic acid and salts thereof.
  • water-soluble polymer examples include guar gum, queen seed, pectin, gelatin, xanthan gum, methylcellulose, and cellulose.
  • the thickening agent used in the cosmetic of the present invention include coconut oil fatty acid monoethanolamide, diethanolamide laurate, isopropanol amide laurate, and polyoxyethylene. Examples include coconut oil monoethanolamide, polyoxypropylene oil fatty acid monoethanolamide, and the like.
  • Examples of the coating agent used in the cosmetic of the present invention include polyvinyl alcohol, polyvinylpyrrolidone, cationi-deno-senorerose, anioni-dani senorerose, and silicone.
  • Examples of the ultraviolet absorber used in the cosmetic of the present invention include 2-hydroxy-14-methoxybenzophenone, 2-hydroxy-14-methoxybenzophenone-15-snorrefonic acid and Salts, benzophenone derivatives such as dihydroxydimethoxybenzophenone, paraaminobenzoic acid derivatives, paraaminobenzoic acid derivatives such as paraaminobenzoic acid and ethyl ethyl paraaminobenzoate.
  • Ethyl lamethoxycinnamate isopropyl paramethoxycinnamate, octyl lamethoxycinnamate, methoxycinnamic acid derivatives, salicylic acid derivatives such as octyl salicylate, phenyl salicylate, perocanic acid and derivatives, 4-tert —Butyl-4′-methoxydibenzoinolemethane, 2- (hydroxy-5′-methinolephenyl) benzotriazole, methyl anthranilate, and the like.
  • anti-inflammatory agent used in the cosmetic of the present invention examples include glycyrrhizic acid and derivatives thereof, glycyrrhetinic acid and its derivatives, alantoin, hydrocortisone acetate, and azulene.
  • Examples of the metal sequestering agent used in the cosmetic of the present invention include ethylenediaminetetraacetic acid and sodium salt, phosphoric acid, cunic acid, ascorbic acid, diconic acid, dalconic acid, and polylactic acid.
  • Examples include sodium phosphate and sodium metaphosphate.
  • Examples of the lower alcohol used in the cosmetic of the present invention include ethanol, propyl alcohol, ethylene glycol, and diethyl glycol.
  • Sugars include glucose, lactose, sucrose, starch, carboxymethyl starch, Cyclodextrin and the like.
  • amino acids used in the cosmetic of the present invention include aspartic acid and salts, alanine, arginine, lysine and salts, glycine, cystine, threonine, serine, methionine, and the like. .
  • organic amines examples include monoethanolamine, diethanolamine, triethanolamine, diisopropanolamine, and triethylamine.
  • Examples of the synthetic resin emulsion used in the cosmetic of the present invention include polyacrylic acid ester copolymer and polybutyl acetate.
  • Examples of the pH adjuster include citric acid, hydrochloric acid, sulfuric acid, and sulfuric acid. Phosphoric acid, sodium hydroxide, ammonia and the like.
  • antioxidant used in the cosmetic of the present invention examples include vitamin E, dibutylhydroxytoluene, butylhydroxyanisole, and gallic esters.
  • antioxidant aid examples include ascorbic acid, phytic acid, cephalic acid, maleic acid and the like, but the ingredients are not limited to these.
  • the electrolyzed deep ocean water which is a weakly basic mineral water generated on the negative electrode side
  • the pH of the weakly basic water fraction is greater than 7 and less than or equal to 10 and the oxidation-reduction potential during production is +300 mV to 1500 mV, and this basic mineral water is used as the water component of the cosmetic of the present invention.
  • the pH value is preferably in the range of 8 to 10.
  • the moisturizing effect of the weakly acidic marine electrolyzed water generated on the positive electrode side is superior to that of ordinary water, and has a more moisturizing effect than deep sea water.
  • the pH of the weakly acidic marine electrolyzed water fraction is less than 7 and is 4 or more, and the oxidation-reduction potential at the time of production shows +500 mV to +100 mV.
  • the pH value is preferably in the range of 4 to 6.
  • Deep seawater collected from a depth of 200m or less in Toyama Bay at a depth of 200m or less in a continuous two-layer electrolyzer Raw water prepared by diluting it 80 times with groundwater is supplied at about 7.2 to 8.5 liter / min. , And water was passed to the anode side and the cathode side. Electrolysis was performed by passing a current of 1.7 to 2.OA at the constant current setting using a stabilized DC power source to the cathode and anode.
  • the pH of the weakly basic mineral water obtained from the cathode side was 8.85, and the oxidation-reduction potential was 133 mV.
  • the pH of the mineral water obtained by heat-sterilizing the mineral water at 85 ° C or higher for 30 minutes or more was 8.90.
  • Test method Wash the forearms of 10 panelists with tap water, wipe off moisture with a towel, drop a few drops on each forearm, apply with palms, and evaluate the moisture retention according to the following rating did. The evaluation was the sum of the scores of each panelist.
  • An emulsion composition having the composition shown in Table 5 below was prepared by the following method, and the feeling of use was evaluated as panelists for 10 women aged 20 to 55 years.
  • test sample 10 females aged 20 to 55 years old were applied to the test sample per day, and an appropriate amount of the test emulsion was applied to the face every morning and before going to bed. One week later, evaluation was performed according to the following evaluation criteria.
  • the highest point of the evaluation is 30 points and the lowest point is 10 points.
  • the results are shown in Table 5.
  • Lotion A lotion composition having the composition shown in Table 6 below was prepared as described below, and the feeling of use was evaluated as follows, using 10 women aged 20 to 55 as panelists.
  • test sample For each test sample, apply an appropriate amount of the test milk to the face daily in the morning and before going to bed as a panel of 10 women from the age of 20 to 55 years. evaluated.
  • Cream A cream composition having the composition shown in Table 7 below was prepared by the following method, and the feeling of use was evaluated as follows, using 10 women aged 20 to 55 as panelists.
  • the components 201 to 206 shown in Table 7 were dissolved by heating to 80 ° C and kept at a temperature of 80 ° C (oil phase).
  • the seeds were mixed in a separate container and selected from among components 207-208 and 209-213] and heated to 80 ° C to dissolve (aqueous phase).
  • the solution of the above-mentioned components 201 to 206 was added to this solution and emulsified. This emulsion was aged for 30 minutes, cooled to room temperature, defoamed, and used as a sample for evaluation.
  • Test sample For each product, apply an appropriate amount of the test milk to the face daily in the morning and before going to bed as a panel of 10 women aged 20 to 55 years, and evaluate it according to the following evaluation criteria one week later. did.
  • shampoo A shampoo composition having the composition shown in Table 8 below was prepared by the following method, and the feeling of use was evaluated by the following method using 10 women aged 20 to 55 as panelists. How to adjust shampoo
  • the highest point of the evaluation is 30 points, and the lowest point is 1 () point.
  • Table 8 shows the results.
  • a rinse composition having the composition shown in Table 9 below was prepared by the following method, and the feeling of use was evaluated by the following method using 10 women from 20 to 55 years as panelists.
  • components 407 to 408 and one selected from 409 to 413 were mixed and dissolved by heating to 80 ° C (aqueous phase).
  • the solution of the above components 401 to 406 was added to this solution and emulsified. This emulsion was aged for 30 minutes, cooled to room temperature, defoamed, and used as an evaluation sample.
  • the highest point of the evaluation is 30 points, and the lowest point is 10 points.
  • Table 9 shows the results.
  • a hair lotion having the following composition was prepared. 501 Succinylated carboxymethyl chitosan solution 2.0% by weight 2% aqueous solution (Note 13)
  • a serum having the following composition was prepared.
  • the above components 601 to 608 were heated and mixed to 80 ° C, uniformly dissolved, cooled, and filled in a container. It was recognized that the use of this product increased skin firmness and improved skin roughness.
  • the cosmetics containing the electrolytic deep sea water of the present invention can improve the moisturizing property of the skin or hair, improve firmness, hydration, luster, smoothness, etc., and are practically excellent. It is.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
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Abstract

L'invention porte sur un cosmétique comprenant de l'eau de mer électrolysée provenant des grands fonds océaniques. Pour préparer ce cosmétique, on soumet l'eau de mer, prélevée à au moins 200m d profondeur dans une partie des grands fonds océaniques, à une électrolyse et on y ajoute les composants cosmétiques désirés. Le cosmétique de cette invention confère à la peau et aux cheveux de meilleures propriétés de rétention de l'humidité, ce qui les rend plus souples, plus soyeux, brillants, lisses, etc.
PCT/JP2001/008509 2000-03-30 2001-09-28 Cosmetique contenant de l'eau de mer electrolysee provenant des grands fonds oceaniques WO2003030839A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
JP2000097915A JP2001278735A (ja) 2000-03-30 2000-03-30 電解海洋深層水含有化粧料
PCT/JP2001/008509 WO2003030839A1 (fr) 2000-03-30 2001-09-28 Cosmetique contenant de l'eau de mer electrolysee provenant des grands fonds oceaniques

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2000097915A JP2001278735A (ja) 2000-03-30 2000-03-30 電解海洋深層水含有化粧料
PCT/JP2001/008509 WO2003030839A1 (fr) 2000-03-30 2001-09-28 Cosmetique contenant de l'eau de mer electrolysee provenant des grands fonds oceaniques

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WO2003030839A1 true WO2003030839A1 (fr) 2003-04-17

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JP2016069323A (ja) * 2014-09-30 2016-05-09 株式会社レドックス スキンケア用又は毛髪手入れ用液体組成物
KR101800681B1 (ko) * 2016-02-04 2017-11-23 주식회사 헤어레시피 손상모 재생 및 모발 보호 기능이 우수한 헤어 케어 트리트먼트용 조성물
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