UA76480C2 - Method for the preparation of gliadin-and glutenin-rich fractions out of gluten in an aqueous medium and in the presence of an acid - Google Patents
Method for the preparation of gliadin-and glutenin-rich fractions out of gluten in an aqueous medium and in the presence of an acid Download PDFInfo
- Publication number
- UA76480C2 UA76480C2 UA2004020922A UA2004020922A UA76480C2 UA 76480 C2 UA76480 C2 UA 76480C2 UA 2004020922 A UA2004020922 A UA 2004020922A UA 2004020922 A UA2004020922 A UA 2004020922A UA 76480 C2 UA76480 C2 UA 76480C2
- Authority
- UA
- Ukraine
- Prior art keywords
- gluten
- gliadin
- glutenin
- acid
- dispersion
- Prior art date
Links
- 108010068370 Glutens Proteins 0.000 title abstract description 40
- 235000021312 gluten Nutrition 0.000 title abstract description 40
- 238000000034 method Methods 0.000 title abstract description 31
- 108010050792 glutenin Proteins 0.000 title abstract description 24
- 239000002253 acid Substances 0.000 title abstract description 12
- 238000002360 preparation method Methods 0.000 title abstract description 4
- 239000012736 aqueous medium Substances 0.000 title abstract description 3
- 108010061711 Gliadin Proteins 0.000 abstract description 30
- 239000006185 dispersion Substances 0.000 abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 13
- 239000000203 mixture Substances 0.000 abstract description 11
- 239000000126 substance Substances 0.000 abstract description 4
- 238000010008 shearing Methods 0.000 abstract description 3
- 241000209140 Triticum Species 0.000 description 15
- 235000021307 Triticum Nutrition 0.000 description 15
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 14
- 239000013049 sediment Substances 0.000 description 14
- 238000002156 mixing Methods 0.000 description 13
- 239000006228 supernatant Substances 0.000 description 13
- 238000005119 centrifugation Methods 0.000 description 10
- 235000018102 proteins Nutrition 0.000 description 9
- 108090000623 proteins and genes Proteins 0.000 description 9
- 102000004169 proteins and genes Human genes 0.000 description 9
- 235000011007 phosphoric acid Nutrition 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical class CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 7
- 238000000605 extraction Methods 0.000 description 7
- 239000002244 precipitate Substances 0.000 description 7
- HZWWPUTXBJEENE-UHFFFAOYSA-N 5-amino-2-[[1-[5-amino-2-[[1-[2-amino-3-(4-hydroxyphenyl)propanoyl]pyrrolidine-2-carbonyl]amino]-5-oxopentanoyl]pyrrolidine-2-carbonyl]amino]-5-oxopentanoic acid Chemical compound C1CCC(C(=O)NC(CCC(N)=O)C(=O)N2C(CCC2)C(=O)NC(CCC(N)=O)C(O)=O)N1C(=O)C(N)CC1=CC=C(O)C=C1 HZWWPUTXBJEENE-UHFFFAOYSA-N 0.000 description 6
- 238000005194 fractionation Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 102000006395 Globulins Human genes 0.000 description 4
- 108010044091 Globulins Proteins 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 102000009027 Albumins Human genes 0.000 description 3
- 108010088751 Albumins Proteins 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 235000011054 acetic acid Nutrition 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- -1 polypropylene Polymers 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- 238000001694 spray drying Methods 0.000 description 3
- 235000014101 wine Nutrition 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000007696 Kjeldahl method Methods 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 125000000218 acetic acid group Chemical class C(C)(=O)* 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 238000011534 incubation Methods 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000008399 tap water Substances 0.000 description 2
- 235000020679 tap water Nutrition 0.000 description 2
- 229940081330 tena Drugs 0.000 description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical group [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 244000117499 Colubrina elliptica Species 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- 101100075837 Drosophila melanogaster Mabi gene Proteins 0.000 description 1
- 235000011449 Rosa Nutrition 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000002224 dissection Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 235000012208 gluconic acid Nutrition 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 235000002949 phytic acid Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000006920 protein precipitation Effects 0.000 description 1
- 238000011110 re-filtration Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000012958 reprocessing Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/14—Vegetable proteins
- A23J3/18—Vegetable proteins from wheat
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/12—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from cereals, wheat, bran, or molasses
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Peptides Or Proteins (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE2001/0541A BE1014340A3 (nl) | 2001-08-10 | 2001-08-10 | Methode voor het bereiden van gliadine- en gluteninerijke fracties uit gluten in een waterig midden en in aanwezigheid van een zuur. |
| PCT/EP2002/008542 WO2003013266A1 (en) | 2001-08-10 | 2002-07-30 | Method for the preparation of gliadin-and glutenin-rich fractions out of gluten in an aqueous medium and in the presence of an acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA76480C2 true UA76480C2 (en) | 2006-08-15 |
Family
ID=3897079
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UA2004020922A UA76480C2 (en) | 2001-08-10 | 2002-07-30 | Method for the preparation of gliadin-and glutenin-rich fractions out of gluten in an aqueous medium and in the presence of an acid |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US7385037B2 (da) |
| EP (1) | EP1414310B1 (da) |
| JP (1) | JP4208712B2 (da) |
| CN (1) | CN1256890C (da) |
| AT (1) | ATE332085T1 (da) |
| AU (1) | AU2002331371B2 (da) |
| BE (1) | BE1014340A3 (da) |
| CA (1) | CA2456042C (da) |
| CY (1) | CY1105289T1 (da) |
| DE (1) | DE60212974T2 (da) |
| DK (1) | DK1414310T3 (da) |
| ES (1) | ES2268079T3 (da) |
| PL (1) | PL204548B1 (da) |
| PT (1) | PT1414310E (da) |
| RU (1) | RU2297774C2 (da) |
| UA (1) | UA76480C2 (da) |
| WO (1) | WO2003013266A1 (da) |
| ZA (1) | ZA200400641B (da) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL1945041T3 (pl) | 2005-11-07 | 2011-05-31 | Syral Belgium Nv | Produkt cukierniczy do żucia i sposób wytwarzania takiego produktu cukierniczego do żucia |
| CN100494962C (zh) * | 2005-12-26 | 2009-06-03 | 中国科学院遗传与发育生物学研究所 | 小麦高、低分子量麦谷蛋白亚基的分离分析方法 |
| CN101117389B (zh) * | 2007-07-20 | 2010-05-26 | 浙江大学 | 溶解小麦储藏蛋白的水性溶剂组合物及其用途 |
| JP5614645B2 (ja) * | 2010-10-22 | 2014-10-29 | アサマ化成株式会社 | 酸性水可溶性タンパク質の製造方法及び酸性水可溶性タンパク質 |
| JP5809446B2 (ja) * | 2011-05-24 | 2015-11-10 | ホシザキ電機株式会社 | 低アレルゲングルテンの製造方法 |
| CN107927546A (zh) * | 2017-11-23 | 2018-04-20 | 宁夏德富胜粮油食品有限公司 | 一种拉面粉及其制作方法 |
| US11440269B2 (en) * | 2020-03-14 | 2022-09-13 | Kurtis Zhang | Process of making a gluten-based biodegradable material |
| CN113519685B (zh) * | 2021-06-24 | 2022-10-28 | 天津商业大学 | 一种尿素结晶法分离谷朊粉中酸溶性麦谷蛋白的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0824870A3 (en) * | 1994-06-03 | 1999-03-31 | Asama Chemical Co., Ltd. | Wheat gluten fractions |
| US5610277A (en) * | 1995-09-11 | 1997-03-11 | Midwest Grain Products | Alcohol-free wet extraction of gluten dough into gliadin and glutenin |
| JP2896422B2 (ja) * | 1996-11-21 | 1999-05-31 | アサマ化成株式会社 | グルテニンを主成分とする分画物の製造方法 |
| JP2954542B2 (ja) * | 1996-11-22 | 1999-09-27 | アサマ化成株式会社 | グリアジン主体の抽出液の抽出方法 |
| JP4171521B2 (ja) * | 1998-10-06 | 2008-10-22 | アサマ化成株式会社 | パンの製造方法 |
-
2001
- 2001-08-10 BE BE2001/0541A patent/BE1014340A3/nl active
-
2002
- 2002-07-30 PL PL367841A patent/PL204548B1/pl unknown
- 2002-07-30 DK DK02767291T patent/DK1414310T3/da active
- 2002-07-30 CA CA002456042A patent/CA2456042C/en not_active Expired - Fee Related
- 2002-07-30 CN CN02815673.0A patent/CN1256890C/zh not_active Expired - Fee Related
- 2002-07-30 US US10/485,884 patent/US7385037B2/en not_active Expired - Fee Related
- 2002-07-30 RU RU2004106796/13A patent/RU2297774C2/ru not_active IP Right Cessation
- 2002-07-30 AT AT02767291T patent/ATE332085T1/de not_active IP Right Cessation
- 2002-07-30 UA UA2004020922A patent/UA76480C2/uk unknown
- 2002-07-30 JP JP2003518294A patent/JP4208712B2/ja not_active Expired - Fee Related
- 2002-07-30 EP EP02767291A patent/EP1414310B1/en not_active Expired - Lifetime
- 2002-07-30 DE DE60212974T patent/DE60212974T2/de not_active Expired - Lifetime
- 2002-07-30 AU AU2002331371A patent/AU2002331371B2/en not_active Ceased
- 2002-07-30 ES ES02767291T patent/ES2268079T3/es not_active Expired - Lifetime
- 2002-07-30 PT PT02767291T patent/PT1414310E/pt unknown
- 2002-07-30 WO PCT/EP2002/008542 patent/WO2003013266A1/en active IP Right Grant
-
2004
- 2004-01-27 ZA ZA2004/00641A patent/ZA200400641B/en unknown
-
2006
- 2006-09-15 CY CY20061101327T patent/CY1105289T1/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PT1414310E (pt) | 2006-11-30 |
| AU2002331371B2 (en) | 2006-09-14 |
| DE60212974D1 (de) | 2006-08-17 |
| EP1414310A1 (en) | 2004-05-06 |
| JP2004537572A (ja) | 2004-12-16 |
| BE1014340A3 (nl) | 2003-09-02 |
| RU2297774C2 (ru) | 2007-04-27 |
| PL367841A1 (en) | 2005-03-07 |
| RU2004106796A (ru) | 2005-05-10 |
| US20040198956A1 (en) | 2004-10-07 |
| CA2456042A1 (en) | 2003-02-20 |
| CA2456042C (en) | 2010-02-02 |
| DK1414310T3 (da) | 2006-07-31 |
| US7385037B2 (en) | 2008-06-10 |
| ATE332085T1 (de) | 2006-07-15 |
| CY1105289T1 (el) | 2010-03-03 |
| EP1414310B1 (en) | 2006-07-05 |
| ZA200400641B (en) | 2005-03-30 |
| ES2268079T3 (es) | 2007-03-16 |
| JP4208712B2 (ja) | 2009-01-14 |
| PL204548B1 (pl) | 2010-01-29 |
| WO2003013266A1 (en) | 2003-02-20 |
| DE60212974T2 (de) | 2007-01-04 |
| CN1256890C (zh) | 2006-05-24 |
| CN1541068A (zh) | 2004-10-27 |
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