SK282510B6 - Spôsob sulfinylácie heterocyklických zlúčenín a intermediárne sulfínamidy - Google Patents

Spôsob sulfinylácie heterocyklických zlúčenín a intermediárne sulfínamidy Download PDF

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Publication number
SK282510B6
SK282510B6 SK234-95A SK23495A SK282510B6 SK 282510 B6 SK282510 B6 SK 282510B6 SK 23495 A SK23495 A SK 23495A SK 282510 B6 SK282510 B6 SK 282510B6
Authority
SK
Slovakia
Prior art keywords
group
groups
haloalkyl
alkyl
amino
Prior art date
Application number
SK234-95A
Other languages
English (en)
Slovak (sk)
Other versions
SK23495A3 (en
Inventor
Michel Casado
Roy Pierre Le
Virginie Pevere
Original Assignee
Rhone-Poulenc Agrochimie
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Application filed by Rhone-Poulenc Agrochimie filed Critical Rhone-Poulenc Agrochimie
Publication of SK23495A3 publication Critical patent/SK23495A3/sk
Publication of SK282510B6 publication Critical patent/SK282510B6/sk

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18One oxygen or sulfur atom
    • C07D231/20One oxygen atom attached in position 3 or 5
    • C07D231/22One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D233/00Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/88Nitrogen atoms, e.g. allantoin
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/38Nitrogen atoms
    • C07D231/40Acylated on said nitrogen atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44Oxygen and nitrogen or sulfur and nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrrole Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Coloring (AREA)
  • Cephalosporin Compounds (AREA)
SK234-95A 1994-02-22 1995-02-20 Spôsob sulfinylácie heterocyklických zlúčenín a intermediárne sulfínamidy SK282510B6 (sk)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9402222A FR2716453B1 (fr) 1994-02-22 1994-02-22 Procédé de sulfinylation de composés hétérocycliques.

Publications (2)

Publication Number Publication Date
SK23495A3 SK23495A3 (en) 1995-09-13
SK282510B6 true SK282510B6 (sk) 2002-10-08

Family

ID=9460460

Family Applications (1)

Application Number Title Priority Date Filing Date
SK234-95A SK282510B6 (sk) 1994-02-22 1995-02-20 Spôsob sulfinylácie heterocyklických zlúčenín a intermediárne sulfínamidy

Country Status (24)

Country Link
US (1) US5618945A (ko)
EP (1) EP0668269B1 (ko)
JP (3) JP3963965B2 (ko)
KR (1) KR100370990B1 (ko)
CN (1) CN1056833C (ko)
AT (1) ATE218127T1 (ko)
AU (1) AU678876B2 (ko)
BR (1) BR9500858A (ko)
CA (1) CA2143135C (ko)
CZ (1) CZ294640B6 (ko)
DE (1) DE69526815T2 (ko)
DK (1) DK0668269T3 (ko)
ES (1) ES2173932T3 (ko)
FI (1) FI113764B (ko)
FR (1) FR2716453B1 (ko)
HU (1) HU214283B (ko)
IL (1) IL112708A (ko)
PL (1) PL183151B1 (ko)
PT (1) PT668269E (ko)
RO (1) RO113639B1 (ko)
RU (1) RU2136665C1 (ko)
SK (1) SK282510B6 (ko)
UA (1) UA44226C2 (ko)
ZA (1) ZA951468B (ko)

Families Citing this family (31)

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Publication number Priority date Publication date Assignee Title
AU6523398A (en) * 1997-04-07 1998-10-30 Mitsubishi Corporation Pyrazole derivatives, process for preparing the same, intermediates, and pest control agent containing the same as active ingredient
FR2784101B1 (fr) * 1998-09-14 2000-11-17 Rhodia Chimie Sa Procede de condensation de derive(s) aromatique(s) et d'un derive sulfinique dont la chaine carbonee est attachee a la fonction sulfinique par un atome de carbone perhalogene
GB9907458D0 (en) * 1999-03-31 1999-05-26 Rhone Poulenc Agrochimie Processes for preparing pesticidal intermediates
MXPA01013211A (es) 1999-06-29 2002-08-12 Mitsubishi Chem Corp Derivados de pirazol y procedimiento para producir los mismos, pesticidas que contienen los mismos como el ingrediente activo.
BR9917518B1 (pt) * 1999-10-22 2009-08-11 processos para a preparação de pesticidas 1-arilpirazóis e seus intermediários.
EP1331222A1 (en) * 2002-01-28 2003-07-30 Virbac S.A. Environment friendly reagents and process for halogenoalkylsulfinylation of organic compounds
AU2004234057A1 (en) * 2003-04-29 2004-11-11 Akzo Nobel N.V. Antisolvent solidification process
US7687533B2 (en) * 2004-03-18 2010-03-30 Pfizer Inc. N-(1-arylpyrazol-4l) sulfonamides and their use as parasiticides
EP1968578A4 (en) 2005-12-14 2011-02-23 Makhteshim Chem Works Ltd POLYMORPHIC AND AMORPHOUS FORMS OF 5-AMINO-L- [2,6-DICHLORO-4- (TRIFLUOROMETHYL) PHENYL] -4- [(TRIFLUOROMETHYL) SULFINYL] -IH-PYRAZOLE-3-CARBONITRIL
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
CA2667559A1 (en) * 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
EP2083627A1 (en) 2006-11-10 2009-08-05 Basf Se Crystalline modification of fipronil
UA110598C2 (uk) 2006-11-10 2016-01-25 Басф Се Спосіб одержання кристалічної модифікації фіпронілу
WO2008055883A1 (en) 2006-11-10 2008-05-15 Basf Se Crystalline modification of fipronil
JP5450079B2 (ja) * 2006-11-10 2014-03-26 ビーエーエスエフ ソシエタス・ヨーロピア ピラゾール誘導体のスルフィニル化の方法
EA018047B1 (ru) * 2006-11-10 2013-05-30 Басф Се Способ сульфинилирования производной пиразола
JP5877624B2 (ja) 2006-11-10 2016-03-08 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se フィプロニルの結晶変態
US7378547B1 (en) 2006-11-28 2008-05-27 E.I. Du Pont De Nemours And Company Process for the synthesis of hydroxy aromatic acids
FR2925493B1 (fr) * 2007-12-19 2011-09-30 Vetoquinol Procede de preparation du fipronil et d'analogues de celui-ci.
MX2011003455A (es) * 2008-10-02 2011-05-23 Merial Ltd Metodo para producir y purificar acido trifluorometanosulfinico.
CN103313604B (zh) 2011-01-14 2016-03-02 K·H·伽达 [5-氨基-1-(2,6-二氯-4-三氟甲苯基)-3-腈-4-三氟甲基亚磺酰基吡唑]中的多晶体
CN102093295A (zh) * 2011-03-10 2011-06-15 江苏长青农化股份有限公司 一种农药杀虫剂氟虫腈的合成方法
TWI579274B (zh) 2012-04-20 2017-04-21 龍馬躍公司 製備1-芳基-5-烷基吡唑化合物的改良方法
US8993613B2 (en) 2013-04-17 2015-03-31 The Hartz Mountain Corporation Ectoparasiticidal formulations
CN104557713B (zh) * 2013-10-22 2018-08-21 江苏托球农化股份有限公司 高纯度氟虫腈制备方法
EP3412659A1 (en) * 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
CN107963993A (zh) * 2018-01-06 2018-04-27 江苏托球农化股份有限公司 一种高纯度氟虫腈的制备方法
WO2020188376A1 (en) * 2019-03-19 2020-09-24 Gharda Chemicals Limited A process for synthesis of fipronil
CN113149873A (zh) * 2021-03-10 2021-07-23 浙江埃森化学有限公司 一种三氟甲基亚磺酰氯的制备方法
CN115650919A (zh) * 2022-04-13 2023-01-31 华东理工大学 一种自三氯甲基亚磺酰氯制备氟虫腈的方法
CN115353490A (zh) * 2022-09-26 2022-11-18 安徽美诺华药物化学有限公司 一种氟虫腈的纯化工艺

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5187185A (en) * 1988-12-09 1993-02-16 Rhone-Poulenc Ag Company Pesticidal 1-arylpyrroles
JPS55157570A (en) * 1979-05-26 1980-12-08 Nissan Chem Ind Ltd Sulfamylimidazole derivative, and agricultural and horticultural fungicide
US5232940A (en) * 1985-12-20 1993-08-03 Hatton Leslie R Derivatives of N-phenylpyrazoles
GB8713768D0 (en) * 1987-06-12 1987-07-15 May & Baker Ltd Compositions of matter
DE3820190A1 (de) * 1988-06-14 1989-12-21 Cassella Ag Pyrrolderivate, ihre herstellung und ihre verwendung als pharmazeutische wirkstoffe
CA2004776C (fr) * 1988-12-13 2000-04-25 Claude Wakselman Procede de preparation de perfluoroalkylthioethers
US5223525A (en) * 1989-05-05 1993-06-29 Rhone-Poulenc Ag Company Pesticidal 1-arylimidazoles
GB9120641D0 (en) * 1991-09-27 1991-11-06 Ici Plc Heterocyclic compounds

Also Published As

Publication number Publication date
DE69526815T2 (de) 2002-11-14
PT668269E (pt) 2002-09-30
RU2136665C1 (ru) 1999-09-10
KR100370990B1 (ko) 2003-04-21
CN1110682A (zh) 1995-10-25
JPH07278106A (ja) 1995-10-24
FI113764B (fi) 2004-06-15
IL112708A0 (en) 1995-05-26
SK23495A3 (en) 1995-09-13
DK0668269T3 (da) 2002-06-17
FI950800A (fi) 1995-08-23
HU214283B (hu) 1998-03-02
KR950032134A (ko) 1995-12-20
CZ294640B6 (cs) 2005-02-16
PL307393A1 (en) 1995-09-04
CN1056833C (zh) 2000-09-27
FI950800A0 (fi) 1995-02-21
ZA951468B (en) 1996-02-16
UA44226C2 (uk) 2002-02-15
PL183151B1 (pl) 2002-05-31
JP2007153906A (ja) 2007-06-21
FR2716453B1 (fr) 1996-03-29
HUT69333A (en) 1995-09-28
ATE218127T1 (de) 2002-06-15
AU1238395A (en) 1995-08-31
FR2716453A1 (fr) 1995-08-25
DE69526815D1 (de) 2002-07-04
AU678876B2 (en) 1997-06-12
HU9500522D0 (en) 1995-04-28
CZ46195A3 (en) 1995-10-18
RU95102481A (ru) 1996-11-20
EP0668269B1 (fr) 2002-05-29
BR9500858A (pt) 1995-10-24
CA2143135A1 (fr) 1995-08-23
JP4731503B2 (ja) 2011-07-27
JP3963965B2 (ja) 2007-08-22
EP0668269A1 (fr) 1995-08-23
ES2173932T3 (es) 2002-11-01
JP4447478B2 (ja) 2010-04-07
JP2005187478A (ja) 2005-07-14
CA2143135C (fr) 2010-01-19
RO113639B1 (ro) 1998-09-30
IL112708A (en) 2005-05-17
US5618945A (en) 1997-04-08

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Expiry date: 20150220