RU2013151602A - Формованное изделие, содержащее материал с пористой ароматической каркасной структурой (пакс) - Google Patents
Формованное изделие, содержащее материал с пористой ароматической каркасной структурой (пакс) Download PDFInfo
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Abstract
1. Формованное изделие из композиции, содержащей(a) полимер с пористой ароматической ковалентной каркасной структурой, где полимер содержит по меньшей мере одну мономерную единицу, где по меньшей мере одна мономерная единица содержит по меньшей мере одно ароматическое кольцо, и по меньшей мере одну мономерную единицу, имеющую по меньшей мере три места связывания с соседними мономерными единицами в полимере и сердцевине, где по меньшей мере три места связывания расположены на по меньшей мере одном атоме сердцевины и где по меньшей мере один атом не имеет ковалентных связей с водородом;(b) по меньшей мере одну связующую добавку.2. Формованное изделие по п.1, где по меньшей мере одна мономерная единица имеет четыре места связывания.3. Формованное изделие по п.1 или 2, где по меньшей мере одно ароматическое кольцо выбирают из группы, включающей бензол, нафталин, бифенил, пиридин, пиримидин, пиридазин, пиразин и триазин.4. Формованное изделие по п.1 или 2, где по меньшей мере один атом в сердцевине является четвертичным атомом углерода.5. Формованное изделие по п.1 или 2, где сердцевину по меньшей мере одной мономерной единицы выбирают из группы, включающейгде n является целым числом 0, 1, 2 или 3;каждый R независимо выбирается из группы, включающей R, NH, NHR, NR , C(O)OH, C(O)OR, ОН и OR;Rявляется метилом или этилом; Х является фениленом или -≡- ипунктирные линии означают места связывания.6. Формованное изделие по п.1 или 2, где полимером является гомополимер.7. Формованное изделие по п.6, где гомополимер состоит из мономерной единицыи8. Формованное изделие по п.1 или 2, где по меньшей мере одним связующим агентом является кислородсодержащий связующи�
Claims (16)
1. Формованное изделие из композиции, содержащей
(a) полимер с пористой ароматической ковалентной каркасной структурой, где полимер содержит по меньшей мере одну мономерную единицу, где по меньшей мере одна мономерная единица содержит по меньшей мере одно ароматическое кольцо, и по меньшей мере одну мономерную единицу, имеющую по меньшей мере три места связывания с соседними мономерными единицами в полимере и сердцевине, где по меньшей мере три места связывания расположены на по меньшей мере одном атоме сердцевины и где по меньшей мере один атом не имеет ковалентных связей с водородом;
(b) по меньшей мере одну связующую добавку.
2. Формованное изделие по п.1, где по меньшей мере одна мономерная единица имеет четыре места связывания.
3. Формованное изделие по п.1 или 2, где по меньшей мере одно ароматическое кольцо выбирают из группы, включающей бензол, нафталин, бифенил, пиридин, пиримидин, пиридазин, пиразин и триазин.
4. Формованное изделие по п.1 или 2, где по меньшей мере один атом в сердцевине является четвертичным атомом углерода.
5. Формованное изделие по п.1 или 2, где сердцевину по меньшей мере одной мономерной единицы выбирают из группы, включающей
где n является целым числом 0, 1, 2 или 3;
каждый R независимо выбирается из группы, включающей R1, NH2, NHR1, NR1 2, C(O)OH, C(O)OR1, ОН и OR1;
R1 является метилом или этилом; Х является фениленом или -≡- и
пунктирные линии означают места связывания.
6. Формованное изделие по п.1 или 2, где полимером является гомополимер.
8. Формованное изделие по п.1 или 2, где по меньшей мере одним связующим агентом является кислородсодержащий связующий агент.
9. Формованное изделие по п.1 или 2, где по меньшей мере один связующий агент выбирают из группы, включающей кислородсодержащее соединение алюминия, оксид кремния и органическое соединение кремния.
10. Формованное изделие по п.1 или 2, где по меньшей мере один связующий агент выбирается из Pural® SB, Ludox® AS 40, Silres® MSE100, тетраэтилортосиликата.
11. Формованное изделие по п.1 или 2, где количество полимера с пористой ароматической ковалентной каркасной структурой по отношению к общей массе формованного изделия составляет от 40 до 99%.
12. Формованное изделие по п.1 или 2, где количество по меньшей мере одной связующей добавки по отношению к общей массе формованного изделия составляет от 1 до 60%.
13. Способ получения формованного изделия по п.1, включающий стадии
(а) смешивания композиции, содержащей полимер с пористой ароматической ковалентной каркасной структурой по п.1 и по меньшей мере одну связывающую добавку по п.1; и
(b) формования композиции в формованное изделие.
14. Способ по п.13, где формование включает стадию экструзии.
15. Применение формованного изделия по п.1 для поглощения по меньшей мере одного вещества для целей его хранения, разделения, контролируемого высвобождения, химической реакции или применения в качестве подложки.
16. Применение по п.15, где по меньшей мере одним веществом является газ или смесь газов.
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PCT/IB2012/051966 WO2012143878A1 (en) | 2011-04-21 | 2012-04-19 | Shaped body containing porous aromatic framework (paf) material |
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EP (1) | EP2699341A4 (ru) |
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CN (1) | CN103635255A (ru) |
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US9987583B2 (en) | 2013-11-22 | 2018-06-05 | The Regents Of The University Of California | Polymers functionalized with brønsted acid groups |
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CN105885019B (zh) * | 2016-04-15 | 2018-04-24 | 东南大学 | 基于三苯胺共轭聚合物电致变色材料及其制备方法和应用 |
CN105949440B (zh) * | 2016-04-27 | 2018-01-02 | 吉林大学 | 一种含氨基的多孔芳香骨架材料paf11‑nh2及其制备方法 |
CN105778063B (zh) * | 2016-04-27 | 2018-02-02 | 吉林大学 | 一种含有硫脲催化位点的多孔芳香骨架材料、制备方法及其在催化反应中的应用 |
US9757710B1 (en) | 2016-08-19 | 2017-09-12 | Ford Global Technologies, Llc | Solvent-supported compaction of metal-organic frameworks |
CN108117537B (zh) * | 2016-11-30 | 2020-03-31 | 中国科学院大连化学物理研究所 | 基于四硫富瓦烯单元的三维共价有机框架材料及合成方法 |
CN107029800A (zh) * | 2017-04-19 | 2017-08-11 | 江苏万德环保科技有限公司 | 一种以有机多孔材料为载体低温抗硫脱硝催化剂及其制备方法 |
CN110591107B (zh) * | 2019-09-20 | 2021-04-27 | 南京邮电大学 | 基于二聚叔醇的超分子有机框架材料的纳米晶体及其制备方法和应用 |
CN110467733B (zh) * | 2019-09-20 | 2021-04-27 | 南京邮电大学 | 基于二聚叔醇的超分子有机框架材料及其制备方法和应用 |
CN113117656B (zh) * | 2019-12-31 | 2022-08-05 | 东北师范大学 | 一种含多功能基多孔吸附剂及其制备方法和应用 |
CN113265033B (zh) * | 2020-02-14 | 2022-06-10 | 台州学院 | 一种共轭有机微孔聚合物及其制备方法 |
JP7484051B2 (ja) | 2020-08-24 | 2024-05-16 | 大成建設株式会社 | ガス貯蔵放出材料 |
CN112194113A (zh) * | 2020-09-30 | 2021-01-08 | 辽宁大学 | 一种基于多孔芳香骨架的形貌可控的碳材料及其制备方法和应用 |
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JP2014512442A (ja) | 2014-05-22 |
EP2699341A1 (en) | 2014-02-26 |
BR112013027141A2 (pt) | 2017-01-10 |
US20120270731A1 (en) | 2012-10-25 |
KR20140035379A (ko) | 2014-03-21 |
WO2012143878A1 (en) | 2012-10-26 |
CN103635255A (zh) | 2014-03-12 |
US8703644B2 (en) | 2014-04-22 |
AU2012245970A1 (en) | 2013-11-07 |
MX2013012119A (es) | 2014-01-23 |
CA2833683A1 (en) | 2012-10-26 |
EP2699341A4 (en) | 2014-09-17 |
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