PL223350B1 - Kompozycja pestycydowa zawierająca glifosat - Google Patents

Info

Publication number

PL223350B1

PL223350B1 PL365245A PL36524501A PL223350B1 PL 223350 B1 PL223350 B1 PL 223350B1 PL 365245 A PL365245 A PL 365245A PL 36524501 A PL36524501 A PL 36524501A PL 223350 B1 PL223350 B1 PL 223350B1

Authority

PL

Poland

Prior art keywords

glyphosate

surfactant

composition

salt

formulations

Prior art date

2000-05-19

Links

• Espacenet
• Global Dossier
• Discuss

• 239000004094 surface-active agent Substances 0.000 title claims abstract description 303
• 239000003090 pesticide formulation Substances 0.000 title description 3
• 239000000203 mixture Substances 0.000 claims abstract description 968
• XDDAORKBJWWYJS-UHFFFAOYSA-N glyphosate Chemical compound OC(=O)CNCP(O)(O)=O XDDAORKBJWWYJS-UHFFFAOYSA-N 0.000 claims abstract description 357
• 239000005562 Glyphosate Substances 0.000 claims abstract description 242
• 229940097068 glyphosate Drugs 0.000 claims abstract description 242
• 239000002253 acid Substances 0.000 claims abstract description 41
• 238000003860 storage Methods 0.000 claims abstract description 14
• 230000000361 pesticidal effect Effects 0.000 claims abstract description 13
• LIOPHZNMBKHGAV-UHFFFAOYSA-M potassium;2-(phosphonomethylamino)acetate Chemical class [K+].OC(=O)CNCP(O)([O-])=O LIOPHZNMBKHGAV-UHFFFAOYSA-M 0.000 claims description 76
• 150000001412 amines Chemical class 0.000 claims description 65
• 239000000243 solution Substances 0.000 claims description 63
• 239000007864 aqueous solution Substances 0.000 claims description 40
• 238000000034 method Methods 0.000 claims description 36
• 125000004432 carbon atom Chemical group C* 0.000 claims description 33
• 125000000217 alkyl group Chemical group 0.000 claims description 30
• 239000001257 hydrogen Substances 0.000 claims description 18
• 229910052739 hydrogen Inorganic materials 0.000 claims description 18
• 125000003342 alkenyl group Chemical group 0.000 claims description 11
• 159000000001 potassium salts Chemical class 0.000 claims description 8
• 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
• 239000008194 pharmaceutical composition Substances 0.000 claims 1
• 230000002363 herbicidal effect Effects 0.000 abstract description 132
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 64
• 239000004009 herbicide Substances 0.000 abstract description 49
• ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 abstract description 32
• 239000012141 concentrate Substances 0.000 abstract description 29
• ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract description 12
• 239000011591 potassium Substances 0.000 abstract description 11
• 229910052700 potassium Inorganic materials 0.000 abstract description 10
• NRZWQKGABZFFKE-UHFFFAOYSA-N trimethylsulfonium Chemical class C[S+](C)C NRZWQKGABZFFKE-UHFFFAOYSA-N 0.000 abstract description 9
• WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 abstract description 8
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract description 5
• 229910052708 sodium Inorganic materials 0.000 abstract description 5
• 239000011734 sodium Substances 0.000 abstract description 5
• QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 abstract description 4
• 125000005537 sulfoxonium group Chemical group 0.000 abstract description 3
• HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 abstract description 2
• NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 abstract 2
• PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 abstract 1
• 238000009472 formulation Methods 0.000 description 211
• 241000196324 Embryophyta Species 0.000 description 201
• 239000004973 liquid crystal related substance Substances 0.000 description 152
• 150000003839 salts Chemical class 0.000 description 132
• JJWLVOIRVHMVIS-UHFFFAOYSA-O isopropylaminium Chemical compound CC(C)[NH3+] JJWLVOIRVHMVIS-UHFFFAOYSA-O 0.000 description 123
• 230000009036 growth inhibition Effects 0.000 description 113
• 239000004615 ingredient Substances 0.000 description 93
• 230000000052 comparative effect Effects 0.000 description 88
• -1 glyphosate acid Chemical class 0.000 description 87
• 241001465754 Metazoa Species 0.000 description 83
• 239000003760 tallow Substances 0.000 description 81
• 238000011282 treatment Methods 0.000 description 80
• 239000000546 pharmaceutical excipient Substances 0.000 description 74
• 238000010561 standard procedure Methods 0.000 description 66
• 238000012360 testing method Methods 0.000 description 64
• IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 63
• 244000058871 Echinochloa crus-galli Species 0.000 description 59
• 238000002360 preparation method Methods 0.000 description 58
• 235000008247 Echinochloa frumentacea Nutrition 0.000 description 56
• 150000001875 compounds Chemical class 0.000 description 44
• 235000019864 coconut oil Nutrition 0.000 description 42
• 239000003240 coconut oil Substances 0.000 description 42
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 38
• 230000012010 growth Effects 0.000 description 35
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 35
• 229920001223 polyethylene glycol Polymers 0.000 description 35
• QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 31
• 125000001183 hydrocarbyl group Chemical group 0.000 description 31
• 239000000047 product Substances 0.000 description 31
• XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 30
• 239000000126 substance Substances 0.000 description 29
• ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 28
• 239000001993 wax Substances 0.000 description 27
• 235000008504 concentrate Nutrition 0.000 description 25
• 230000000694 effects Effects 0.000 description 25
• 239000003093 cationic surfactant Substances 0.000 description 24
• 240000006995 Abutilon theophrasti Species 0.000 description 23
• 150000003973 alkyl amines Chemical group 0.000 description 22
• 229910052757 nitrogen Inorganic materials 0.000 description 21
• 230000015572 biosynthetic process Effects 0.000 description 20
• 230000005764 inhibitory process Effects 0.000 description 20
• 239000000523 sample Substances 0.000 description 19
• 239000002904 solvent Substances 0.000 description 19
• ZITBHNVGLSVXEF-UHFFFAOYSA-N 2-[2-(16-methylheptadecoxy)ethoxy]ethanol Chemical compound CC(C)CCCCCCCCCCCCCCCOCCOCCO ZITBHNVGLSVXEF-UHFFFAOYSA-N 0.000 description 18
• IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 17
• LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 17
• ZEKANFGSDXODPD-UHFFFAOYSA-N glyphosate-isopropylammonium Chemical compound CC(C)N.OC(=O)CNCP(O)(O)=O ZEKANFGSDXODPD-UHFFFAOYSA-N 0.000 description 17
• 239000000787 lecithin Substances 0.000 description 17
• 235000010445 lecithin Nutrition 0.000 description 17
• 229940067606 lecithin Drugs 0.000 description 17
• 239000007921 spray Substances 0.000 description 17
• 235000003403 Limnocharis flava Nutrition 0.000 description 16
• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
• MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 15
• 229920002257 Plurafac® Polymers 0.000 description 15
• KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 14
• UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 14
• 150000002148 esters Chemical class 0.000 description 14
• 239000007788 liquid Substances 0.000 description 14
• XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 12
• BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 12
• 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 12
• XXUJMEYKYHETBZ-UHFFFAOYSA-N ethyl 4-nitrophenyl ethylphosphonate Chemical compound CCOP(=O)(CC)OC1=CC=C([N+]([O-])=O)C=C1 XXUJMEYKYHETBZ-UHFFFAOYSA-N 0.000 description 12
• 239000007787 solid Substances 0.000 description 12
• 238000006243 chemical reaction Methods 0.000 description 11
• 150000002431 hydrogen Chemical group 0.000 description 11
• 238000005507 spraying Methods 0.000 description 11
• 238000012546 transfer Methods 0.000 description 11
• OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 10
• 238000005481 NMR spectroscopy Methods 0.000 description 10
• 101100205952 Schizosaccharomyces pombe (strain 972 / ATCC 24843) tam12 gene Proteins 0.000 description 10
• 239000004480 active ingredient Substances 0.000 description 10
• 238000007865 diluting Methods 0.000 description 10
• 235000013399 edible fruits Nutrition 0.000 description 10
• 230000005484 gravity Effects 0.000 description 10
• BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 10
• 150000003242 quaternary ammonium salts Chemical class 0.000 description 10
• 230000002829 reductive effect Effects 0.000 description 10
• 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 10
• QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 9
• YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 9
• 108090000790 Enzymes Proteins 0.000 description 9
• 102000004190 Enzymes Human genes 0.000 description 9
• 239000002671 adjuvant Substances 0.000 description 9
• KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
• 229940088598 enzyme Drugs 0.000 description 9
• JJWLVOIRVHMVIS-UHFFFAOYSA-N isopropylamine Chemical class CC(C)N JJWLVOIRVHMVIS-UHFFFAOYSA-N 0.000 description 9
• 239000000693 micelle Substances 0.000 description 9
• 239000002736 nonionic surfactant Substances 0.000 description 9
• 241000894007 species Species 0.000 description 9
• MPNXSZJPSVBLHP-UHFFFAOYSA-N 2-chloro-n-phenylpyridine-3-carboxamide Chemical compound ClC1=NC=CC=C1C(=O)NC1=CC=CC=C1 MPNXSZJPSVBLHP-UHFFFAOYSA-N 0.000 description 8
• YYROPELSRYBVMQ-UHFFFAOYSA-N 4-toluenesulfonyl chloride Chemical compound CC1=CC=C(S(Cl)(=O)=O)C=C1 YYROPELSRYBVMQ-UHFFFAOYSA-N 0.000 description 8
• VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 8
• 239000005977 Ethylene Substances 0.000 description 8
• 241000745991 Phalaris Species 0.000 description 8
• GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 8
• 150000001298 alcohols Chemical class 0.000 description 8
• 230000001965 increasing effect Effects 0.000 description 8
• 239000012071 phase Substances 0.000 description 8
• DYWNLSQWJMTVGJ-UHFFFAOYSA-N (1-hydroxy-1-phenylpropan-2-yl)azanium;chloride Chemical compound Cl.CC(N)C(O)C1=CC=CC=C1 DYWNLSQWJMTVGJ-UHFFFAOYSA-N 0.000 description 7
• NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 7
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• WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 7
• 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 7
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