NO20053585L - Fremgangsmate for karbonylering av metanol ved fremstilling av eddiksyre i en vannfattig prosess med regulering av vannbalansen. - Google Patents

Fremgangsmate for karbonylering av metanol ved fremstilling av eddiksyre i en vannfattig prosess med regulering av vannbalansen.

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Publication number
NO20053585L
NO20053585L NO20053585A NO20053585A NO20053585L NO 20053585 L NO20053585 L NO 20053585L NO 20053585 A NO20053585 A NO 20053585A NO 20053585 A NO20053585 A NO 20053585A NO 20053585 L NO20053585 L NO 20053585L
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NO
Norway
Prior art keywords
water
carbonylation
methanol
acetic acid
production
Prior art date
Application number
NO20053585A
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English (en)
Other versions
NO333287B1 (no
Inventor
Michael E Huckman
Hosea Cheung
Paull G Torrence
Original Assignee
Celanese Int Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Celanese Int Corp filed Critical Celanese Int Corp
Publication of NO20053585L publication Critical patent/NO20053585L/no
Publication of NO333287B1 publication Critical patent/NO333287B1/no

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/50Use of additives, e.g. for stabilisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

Fremgangsmåte for fremstilling av eddiksyre ved karbonylering av metanol og reaktive derivater av denne, i en reaksjonsblanding hvor det anvendes en rhodiumbasert katalysator og vannfattige betingelser. Det oppnås reaksjonshastigheter på minst 15 gmol/l/h. De høye reaksjonshastigheter skjer ved vannkonsentrasjoner på under 2,0 vekt%. Under bestemte betingelser holdes vannkonsentrasjonen i reaksjonsblandingen på ønsket nivå i reaksjonssystemet ved hjelp av minst ett prosesstrinn som innbefatter å tilsette en forbindelse som metylacetat, dimetyleter, eddiksyreanhydrid eller blandinger av disse. Prosesstrinnet med å tilsette disse komponenter til reaksjonsblandingen kan bli kombinert med andre prosesstrinn for å regulere vannkonsentrasjoner i reaksjonsblandinger for karbonylering av metanol.
NO20053585A 2002-12-23 2005-07-22 Fremgangsmate for fremstilling av eddiksyre ved katalytisk karbonyleringsreaksjon NO333287B1 (no)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/328,065 US7005541B2 (en) 2002-12-23 2002-12-23 Low water methanol carbonylation process for high acetic acid production and for water balance control
PCT/US2003/037020 WO2004060846A1 (en) 2002-12-23 2003-11-18 A low water methanol carbonylation process for high acetic acid production and for water balance control

Publications (2)

Publication Number Publication Date
NO20053585L true NO20053585L (no) 2005-07-22
NO333287B1 NO333287B1 (no) 2013-04-29

Family

ID=32594369

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20053585A NO333287B1 (no) 2002-12-23 2005-07-22 Fremgangsmate for fremstilling av eddiksyre ved katalytisk karbonyleringsreaksjon

Country Status (22)

Country Link
US (1) US7005541B2 (no)
EP (1) EP1590313B1 (no)
JP (3) JP4588458B2 (no)
KR (1) KR100987864B1 (no)
CN (1) CN100341836C (no)
AT (1) ATE386009T1 (no)
AU (1) AU2003291106C1 (no)
BR (1) BR0317704A (no)
CA (1) CA2507497C (no)
DE (1) DE60319148T2 (no)
ES (1) ES2300637T3 (no)
MX (1) MXPA05006845A (no)
MY (1) MY146585A (no)
NO (1) NO333287B1 (no)
NZ (1) NZ541220A (no)
PL (1) PL208839B1 (no)
RS (1) RS52570B (no)
RU (1) RU2329249C2 (no)
TW (1) TWI290918B (no)
UA (1) UA80312C2 (no)
WO (1) WO2004060846A1 (no)
ZA (1) ZA200504110B (no)

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