MX2010003148A - Procedimiento para la preparacion de diamidas de acido sulfonico. - Google Patents

Procedimiento para la preparacion de diamidas de acido sulfonico.

Info

Publication number
MX2010003148A
MX2010003148A MX2010003148A MX2010003148A MX2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A MX 2010003148 A MX2010003148 A MX 2010003148A
Authority
MX
Mexico
Prior art keywords
sup
formula
atoms
iii
sulfonic acid
Prior art date
Application number
MX2010003148A
Other languages
English (en)
Inventor
Jan Hendrik Wevers
Michael Keil
Joachim Gebhardt
Thomas Schmidt
Sandra L Hr
Axel Pleschke
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2010003148A publication Critical patent/MX2010003148A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/34Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/541,3-Diazines; Hydrogenated 1,3-diazines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C307/00Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C307/04Diamides of sulfuric acids
    • C07C307/06Diamides of sulfuric acids having nitrogen atoms of the sulfamide groups bound to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C381/00Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D239/00Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/52Two oxygen atoms
    • C07D239/54Two oxygen atoms as doubly bound oxygen atoms or as unsubstituted hydroxy radicals

Abstract

Procedimiento para la preparaci?n de diamidas de ?cido sulf?nico de la f?rmula I R1R2N-S(O)2-NH2 (I), en donde R1 y R2 representan, independientemente el uno del otro, un radical alquilo primario con 1 a 8 ?tomos de carbono, un radical alquilo secundario con 3 a 8 ?tomos de carbono o un radical cicloalquilo con 5 a 8 ?tomos de carbono, o forman, junto con el ?tomo de nitr?geno, un heterociclo de nitr?geno, saturado, de 5 a 8 miembros, que puede presentar como miembro de anillo, junto con el ?tomo de nitr?geno, otro hetero?tomo seleccionado de entre O y S, pudiendo el heterociclo de nitr?geno presentar 1, 2, 3 ? 4 grupos alquilo, cada cual con 1 a 4 ?tomos de carbono como sustituyentes, y que comprende i) hacer reaccionar con cloruro de sulfurilo una amina secundaria de la f?rmula II R1R2NH (II), en la que R1 y R2 tienen los significados antedichos, en un disolvente org?nico inerte y en presencia de una amina terciaria, para convertirla en un cloruro de sulfamo?lo de la f?rmula III R1R2N-S(O)2-CI (III), en la que R1 y R2 tienen los significado antedichos, y ii) hacer reaccionar con amoniaco el cloruro de sulfamo?lo de la f?rmula III obtenido en el pasa i), y en el que el paso ii) se aplica, en el disolvente inerte, en particular el disolvente arom?tico, el cloruro de sulfamo?lo de la f?rmula III en la forma de la soluci?n obtenida en el paso i).
MX2010003148A 2007-10-12 2008-10-10 Procedimiento para la preparacion de diamidas de acido sulfonico. MX2010003148A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP07118416 2007-10-12
PCT/EP2008/063630 WO2009050120A1 (de) 2007-10-12 2008-10-10 Verfahren zur herstelung von sulfonsäurediamiden

Publications (1)

Publication Number Publication Date
MX2010003148A true MX2010003148A (es) 2010-04-01

Family

ID=39186045

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2010003148A MX2010003148A (es) 2007-10-12 2008-10-10 Procedimiento para la preparacion de diamidas de acido sulfonico.

Country Status (9)

Country Link
US (1) US9920002B2 (es)
EP (1) EP2200978A1 (es)
JP (1) JP5465672B2 (es)
CN (1) CN101821233B (es)
AR (1) AR068849A1 (es)
BR (1) BRPI0818408B1 (es)
IL (1) IL204595A (es)
MX (1) MX2010003148A (es)
WO (1) WO2009050120A1 (es)

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CA2821516A1 (en) * 2005-12-01 2007-06-07 Basf Se Process for producing fluorinated m-nitrobenzoyl chlorides
CN103130727B (zh) * 2013-02-27 2015-07-08 江苏省农用激素工程技术研究中心有限公司 苯嘧磺草胺中间体的制备方法
JP6141762B2 (ja) * 2013-12-27 2017-06-07 富士フイルム株式会社 染料化合物及びその製造方法、着色硬化性組成物、カラーフィルタ及びその製造方法、画像表示装置、並びに固体撮像素子
CN107827786A (zh) * 2017-11-24 2018-03-23 常州沃腾化工科技有限公司 N‑甲基‑n‑异丙基胺基磺酰胺的生产方法
EP3587396A1 (en) 2018-06-27 2020-01-01 Basf Se A method of isolating a n-(3-nitrobenzoyl)sulfamide
US11267707B2 (en) * 2019-04-16 2022-03-08 Honeywell International Inc Purification of bis(fluorosulfonyl) imide
CN112679292B (zh) * 2020-12-25 2022-05-20 复旦大学 一种磺酰仲胺类化合物的合成方法
CN113185467B (zh) * 2021-04-20 2022-03-08 江苏乾元生物科技有限公司 一种苯嘧磺草胺的制备方法
CN115246791A (zh) * 2021-04-26 2022-10-28 四川奥兰多化工有限公司 一种合成6-三氟甲基尿嘧啶的方法及其中间体
CN114478326B (zh) * 2022-01-21 2023-10-03 安徽宁亿泰科技有限公司 一种苯嘧磺草胺关键中间体的合成方法

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Also Published As

Publication number Publication date
JP5465672B2 (ja) 2014-04-09
IL204595A (en) 2014-03-31
AR068849A1 (es) 2009-12-09
CN101821233A (zh) 2010-09-01
BRPI0818408A2 (pt) 2015-09-15
IL204595A0 (en) 2010-11-30
US20100222586A1 (en) 2010-09-02
BRPI0818408B1 (pt) 2024-01-09
BRPI0818408A8 (pt) 2016-11-22
US9920002B2 (en) 2018-03-20
EP2200978A1 (de) 2010-06-30
CN101821233B (zh) 2016-06-29
WO2009050120A1 (de) 2009-04-23
JP2011500536A (ja) 2011-01-06

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