BRPI0818408A8 - Processos para preparar diamidas sulfúricas e ingredientes herbricidas atvos. - Google Patents
Processos para preparar diamidas sulfúricas e ingredientes herbricidas atvos.Info
- Publication number
- BRPI0818408A8 BRPI0818408A8 BRPI0818408A BRPI0818408A BRPI0818408A8 BR PI0818408 A8 BRPI0818408 A8 BR PI0818408A8 BR PI0818408 A BRPI0818408 A BR PI0818408A BR PI0818408 A BRPI0818408 A BR PI0818408A BR PI0818408 A8 BRPI0818408 A8 BR PI0818408A8
- Authority
- BR
- Brazil
- Prior art keywords
- iii
- formula
- carbon atoms
- ingredients
- processes
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- 150000001470 diamides Chemical class 0.000 title abstract 2
- 239000004615 ingredient Substances 0.000 title abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 4
- -1 sulfonic acid amines Chemical class 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 229910052757 nitrogen Inorganic materials 0.000 abstract 2
- 125000004433 nitrogen atom Chemical group N* 0.000 abstract 2
- QAHVHSLSRLSVGS-UHFFFAOYSA-N sulfamoyl chloride Chemical compound NS(Cl)(=O)=O QAHVHSLSRLSVGS-UHFFFAOYSA-N 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000004397 aminosulfonyl group Chemical group NS(=O)(=O)* 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000003849 aromatic solvent Substances 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 125000005842 heteroatom Chemical group 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 229910017464 nitrogen compound Inorganic materials 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 150000003335 secondary amines Chemical class 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- 229910052717 sulfur Inorganic materials 0.000 abstract 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C307/04—Diamides of sulfuric acids
- C07C307/06—Diamides of sulfuric acids having nitrogen atoms of the sulfamide groups bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
- C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
- C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
- C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
- C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
- C07D239/52—Two oxygen atoms
- C07D239/54—Two oxygen atoms as doubly bound oxygen atoms or as unsubstituted hydroxy radicals
Abstract
PROCESSOS PARA PREPARAR DIAMIDAS SULFÚRICAS E INGREDIENTES HERBICIDAS ATIVOS. A presente invenção se refere a um método para produzir aminas de dcido sulfônico da formula geral (I) R1R2N-S(O)2-NH2(I), onde R1 e R2 são independentes um do outro e representa um radical alquila primário tendo de 1 a 8 átomos de carbono, um radical alguila secunddário tendo de 3 a 8 átomos de carbono, ou um radical cicloalquila tendo de 5 a 8 átomos de carbono, ou, junto com átomo de nitrogénio, formam um composto heterociclico de nitrogênio saturado de 5 a 8 membros gue pode compreender, além do atomo de nitrogênio, um heteroátomo adicional, selecionado dentre O e S, como um membro de anel, onde o composto heterociclico de nitrogênio é insubstituido, ou pode compreender 1, 2, 3 ou 4 grupos alquila cada um tendo 1 a 4 átomos de carbono como substituintes. O método compreende as seguintes etapas: i) conversão de uma amina secundária da formula (Il), R1R2NH (Il), onde R1 e R2 tém o significado indicado acima, tendo cloreto de sulfurila em um solvente inorte, particularmente aromático, na presença de uma amina tercidria, para formar um sulfamoila da fórmula (III) R1R2N-S(O2)-CI (III) onde R1 e R2 tém o significado indicado acima, e (iii) conversão do cloreto de sulfamoila da fórmula (III) obtido na etapa i) usando amônia, onde na etapa ii) o cloreto de sulfamoila da fórmula (III) é usado na forma de solução obtida na etapa i) no solvente inerte, particularmente aromático..
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP07118416.2 | 2007-10-12 | ||
EP07118416 | 2007-10-12 | ||
PCT/EP2008/063630 WO2009050120A1 (de) | 2007-10-12 | 2008-10-10 | Verfahren zur herstelung von sulfonsäurediamiden |
Publications (3)
Publication Number | Publication Date |
---|---|
BRPI0818408A2 BRPI0818408A2 (pt) | 2015-09-15 |
BRPI0818408A8 true BRPI0818408A8 (pt) | 2016-11-22 |
BRPI0818408B1 BRPI0818408B1 (pt) | 2024-01-09 |
Family
ID=39186045
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0818408-9A BRPI0818408B1 (pt) | 2007-10-12 | 2008-10-10 | Processos para preparar diamidas sulfúricas e ingredientes herbicidas ativos |
Country Status (9)
Country | Link |
---|---|
US (1) | US9920002B2 (pt) |
EP (1) | EP2200978A1 (pt) |
JP (1) | JP5465672B2 (pt) |
CN (1) | CN101821233B (pt) |
AR (1) | AR068849A1 (pt) |
BR (1) | BRPI0818408B1 (pt) |
IL (1) | IL204595A (pt) |
MX (1) | MX2010003148A (pt) |
WO (1) | WO2009050120A1 (pt) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU2006319263B2 (en) * | 2005-12-01 | 2012-06-28 | Basf Se | Method for producing sulfonamides |
CN103130727B (zh) * | 2013-02-27 | 2015-07-08 | 江苏省农用激素工程技术研究中心有限公司 | 苯嘧磺草胺中间体的制备方法 |
JP6141762B2 (ja) * | 2013-12-27 | 2017-06-07 | 富士フイルム株式会社 | 染料化合物及びその製造方法、着色硬化性組成物、カラーフィルタ及びその製造方法、画像表示装置、並びに固体撮像素子 |
CN107827786A (zh) * | 2017-11-24 | 2018-03-23 | 常州沃腾化工科技有限公司 | N‑甲基‑n‑异丙基胺基磺酰胺的生产方法 |
EP3587396A1 (en) | 2018-06-27 | 2020-01-01 | Basf Se | A method of isolating a n-(3-nitrobenzoyl)sulfamide |
US11267707B2 (en) * | 2019-04-16 | 2022-03-08 | Honeywell International Inc | Purification of bis(fluorosulfonyl) imide |
CN112679292B (zh) * | 2020-12-25 | 2022-05-20 | 复旦大学 | 一种磺酰仲胺类化合物的合成方法 |
CN113185467B (zh) * | 2021-04-20 | 2022-03-08 | 江苏乾元生物科技有限公司 | 一种苯嘧磺草胺的制备方法 |
CN115246791A (zh) * | 2021-04-26 | 2022-10-28 | 四川奥兰多化工有限公司 | 一种合成6-三氟甲基尿嘧啶的方法及其中间体 |
CN114478326B (zh) * | 2022-01-21 | 2023-10-03 | 安徽宁亿泰科技有限公司 | 一种苯嘧磺草胺关键中间体的合成方法 |
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DE1240853B (de) * | 1962-12-06 | 1967-05-24 | Smith Kline French Lab | Verfahren zur Herstellung von Sulfurylamiden |
US3198785A (en) * | 1964-04-17 | 1965-08-03 | Sandoz Ag | Sulfamoyl azabicyclononanes and derivatives thereof |
US3709677A (en) * | 1969-06-25 | 1973-01-09 | Sandoz Ag | N-substituted sulfamoyl compounds useful as herbicides |
NL175521C (nl) | 1973-04-26 | 1984-11-16 | Hoechst Ag | Werkwijze voor het bereiden van carbonzuurchloriden. |
DE2933148A1 (de) | 1979-08-16 | 1981-02-26 | Bayer Ag | Verfahren zur herstellung von aromatischen dicarbonsaeuredichloriden iv |
DE3040295A1 (de) | 1980-10-25 | 1982-06-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von aromatischen carbonsaeurechloriden |
JPS61155350A (ja) | 1984-12-28 | 1986-07-15 | Ihara Nikkei Kagaku Kogyo Kk | 脂肪酸クロライド及び芳香族酸クロライドの製造方法 |
EP0333791A1 (de) | 1987-09-23 | 1989-09-27 | Ciba-Geigy Ag | Heterocyclische verbindungen |
US5238908A (en) | 1989-08-31 | 1993-08-24 | Rohm And Haas Company | Herbicidal glutaramic acids and derivatives |
TW224421B (pt) * | 1991-12-24 | 1994-06-01 | Shell Internat Researce Schappel N V | |
PL334846A1 (en) * | 1997-01-23 | 2000-03-27 | Hoffmann La Roche | Sulphamidic inhibitors of metaloproteases |
US20020065270A1 (en) | 1999-12-28 | 2002-05-30 | Moriarty Kevin Joseph | N-heterocyclic inhibitors of TNF-alpha expression |
EP1246823A1 (en) | 1999-12-28 | 2002-10-09 | Pharmacopeia, Inc. | Pyrimidine and triazine kinase inhibitors |
JP2004501084A (ja) | 2000-04-17 | 2004-01-15 | ビーエーエスエフ アクチェンゲゼルシャフト | 除草活性を有する3−ヘテロ環置換ベンゾイソチアゾール及びベンゾイソオキサゾール化合物 |
US6251829B1 (en) | 2000-04-18 | 2001-06-26 | Rohm And Haas Company | Herbicidal benzoyloxy carboxylates and carboxamides |
DK1226127T3 (da) * | 2000-05-04 | 2009-10-19 | Basf Se | Substituerede phenylsulfamoylcarboxamider |
DE60235470D1 (de) | 2001-06-26 | 2010-04-08 | Pharmacopeia Inc | N-heterocyclische inhibitoren der expression von tnf-alpha |
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DK1506169T3 (da) | 2002-05-16 | 2010-04-19 | Basf Se | Fremgangsmåde til fremstilling af sulfonsyrediamider |
WO2004035545A2 (en) | 2002-10-18 | 2004-04-29 | E.I. Du Pont De Nemours And Company | Azolecarboxamide herbicides |
AU2003287972B2 (en) | 2002-10-30 | 2010-04-22 | Basf Aktiengesellschaft | Bifunctional phenyliso(thio)cyanates; method and intermediate products for the production thereof |
WO2004106324A1 (en) | 2003-05-27 | 2004-12-09 | E.I. Dupont De Nemours And Company | Azolecarboxamide herbicides |
JP4351888B2 (ja) * | 2003-09-22 | 2009-10-28 | 富士フイルム株式会社 | スルファモイルオキシ基またはスルフィナモイルオキシ基が置換された芳香族化合物と求核剤との反応による芳香族化合物誘導体の製造方法 |
EP1516870A1 (en) | 2003-09-22 | 2005-03-23 | Fuji Photo Film Co., Ltd. | Process for producing aromatic compound derivative by reaction of aromatic compound substituted with sulfamoyloxy, sulfinamoyloxy, or carbamoyloxy group, with nucleophilic agent |
CA2574406C (en) * | 2004-07-22 | 2013-02-19 | Basf Aktiengesellschaft | Method for the production of 3-phenyl(thio)uracils and dithiouracils |
JP2006083133A (ja) | 2004-09-17 | 2006-03-30 | Sankyo Co Ltd | スルファミド誘導体医薬組成物 |
ITMI20050275A1 (it) | 2005-02-22 | 2006-08-23 | Miteni Spa | Procedimento per la preparazione di derivati dell'acido benzoico attraverso un nuovo intermedio di sintesi |
WO2006125746A1 (de) * | 2005-05-24 | 2006-11-30 | Basf Aktiengesellschaft | Verfahren zur herstellung von 1-alkyl-3-phenyluracilen |
AU2006319263B2 (en) | 2005-12-01 | 2012-06-28 | Basf Se | Method for producing sulfonamides |
-
2008
- 2008-10-10 AR ARP080104453A patent/AR068849A1/es active IP Right Grant
- 2008-10-10 WO PCT/EP2008/063630 patent/WO2009050120A1/de active Application Filing
- 2008-10-10 JP JP2010528412A patent/JP5465672B2/ja active Active
- 2008-10-10 MX MX2010003148A patent/MX2010003148A/es active IP Right Grant
- 2008-10-10 BR BRPI0818408-9A patent/BRPI0818408B1/pt active IP Right Grant
- 2008-10-10 US US12/681,843 patent/US9920002B2/en active Active
- 2008-10-10 EP EP08838788A patent/EP2200978A1/de not_active Withdrawn
- 2008-10-10 CN CN200880111156.XA patent/CN101821233B/zh active Active
-
2010
- 2010-03-18 IL IL204595A patent/IL204595A/en active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
BRPI0818408A2 (pt) | 2015-09-15 |
US20100222586A1 (en) | 2010-09-02 |
WO2009050120A1 (de) | 2009-04-23 |
EP2200978A1 (de) | 2010-06-30 |
CN101821233B (zh) | 2016-06-29 |
BRPI0818408B1 (pt) | 2024-01-09 |
JP5465672B2 (ja) | 2014-04-09 |
IL204595A0 (en) | 2010-11-30 |
CN101821233A (zh) | 2010-09-01 |
IL204595A (en) | 2014-03-31 |
JP2011500536A (ja) | 2011-01-06 |
MX2010003148A (es) | 2010-04-01 |
US9920002B2 (en) | 2018-03-20 |
AR068849A1 (es) | 2009-12-09 |
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Legal Events
Date | Code | Title | Description |
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B15K | Others concerning applications: alteration of classification |
Free format text: AS CLASSIFICACOES ANTERIORES ERAM: C07C 303/34 , C07C 307/06 , C07D 239/54 Ipc: C07C 303/34 (2006.01), C07C 307/06 (2006.01), C07D |
|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] | ||
B12B | Appeal against refusal [chapter 12.2 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 10/10/2008, OBSERVADAS AS CONDICOES LEGAIS. PATENTE CONCEDIDA CONFORME ADI 5.529/DF, QUE DETERMINA A ALTERACAO DO PRAZO DE CONCESSAO. |