EA200401483A1 - Способ получения галогенангидридов сульфаминовой кислоты - Google Patents

Способ получения галогенангидридов сульфаминовой кислоты

Info

Publication number
EA200401483A1
EA200401483A1 EA200401483A EA200401483A EA200401483A1 EA 200401483 A1 EA200401483 A1 EA 200401483A1 EA 200401483 A EA200401483 A EA 200401483A EA 200401483 A EA200401483 A EA 200401483A EA 200401483 A1 EA200401483 A1 EA 200401483A1
Authority
EA
Eurasian Patent Office
Prior art keywords
sub
sulfamoyl
invention further
further relates
reacting
Prior art date
Application number
EA200401483A
Other languages
English (en)
Inventor
Герхард Хампрехт
Михаэль Пуль
Роберт Райнхард
Инго Загассер
Томас Шмидт
Норберт Гётц
Томас Цирке
Original Assignee
Басф Акциенгезельшафт
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Басф Акциенгезельшафт filed Critical Басф Акциенгезельшафт
Publication of EA200401483A1 publication Critical patent/EA200401483A1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/22—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with hetero atoms directly attached to ring nitrogen atoms
    • C07D295/26—Sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C307/02—Monoamides of sulfuric acids or esters thereof, e.g. sulfamic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/46—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with hetero atoms directly attached to the ring nitrogen atom
    • C07D207/48—Sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/92—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with a hetero atom directly attached to the ring nitrogen atom
    • C07D211/96—Sulfur atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Detergent Compositions (AREA)

Abstract

Настоящее изобретение относится к способу получения галогенангидридов сульфаминовой кислоты первичных или вторичных аминов, включающий следующие стадии:i) взаимодействие первичного или вторичного амина A1, по меньшей мере, с эквимолярными количествами SOили источника SOв присутствии, по меньшей мере, эквимолярных количеств третичного амина A2, каждый в пересчете на амин A1, иii) взаимодействие полученной на стадии i) реакционной смеси, по меньшей мере, со стехиометрически требуемым количеством галогенида фосфора.Изобретение относится далее к способу получения амидов сульфокислоты, включающему получение гелогенангидридов сульфаминовой кислоты, проведение стадий i) и ii) и взаимодействие полученного галогенангидрида сульфаминовой кислоты с аммиаком. Изобретение относится к применению этого способа для получения гербицидных действующих веществ со структурой сульфодиамида. Изобретение также относится к новым хлорангидридам сульфаминовой кислоты.Международная заявка была опубликована вместе с отчетом о международном поиске.
EA200401483A 2002-05-16 2003-05-15 Способ получения галогенангидридов сульфаминовой кислоты EA200401483A1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10221910 2002-05-16
PCT/EP2003/005126 WO2003097589A1 (de) 2002-05-16 2003-05-15 Verfahren zur herstellung von sulfamidsäurehalogeniden

Publications (1)

Publication Number Publication Date
EA200401483A1 true EA200401483A1 (ru) 2005-06-30

Family

ID=29432137

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200401483A EA200401483A1 (ru) 2002-05-16 2003-05-15 Способ получения галогенангидридов сульфаминовой кислоты

Country Status (18)

Country Link
US (1) US7232926B2 (ru)
EP (1) EP1506169B1 (ru)
JP (1) JP4384028B2 (ru)
KR (1) KR100973619B1 (ru)
CN (1) CN100509771C (ru)
AT (1) ATE452875T1 (ru)
AU (1) AU2003240656A1 (ru)
BR (1) BR0309922B1 (ru)
CA (1) CA2485360A1 (ru)
DE (1) DE50312258D1 (ru)
DK (1) DK1506169T3 (ru)
EA (1) EA200401483A1 (ru)
ES (1) ES2337779T3 (ru)
IL (1) IL164739A (ru)
MX (1) MXPA04010748A (ru)
PL (1) PL374371A1 (ru)
WO (1) WO2003097589A1 (ru)
ZA (1) ZA200410075B (ru)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE502004005772D1 (de) * 2003-12-03 2008-01-31 Basf Ag Verfahren zur herstellung von 3-phenyl(thio)uracilen und 3-phenyldithiouracilen
KR100651344B1 (ko) * 2004-02-19 2006-11-29 삼성전자주식회사 고속 순방향 패킷 접속 방식을 사용하는 이동 통신시스템에서 데이터 처리 속도를 향상시키는 방법 및 그이동통신시스템
JP4860613B2 (ja) 2004-07-22 2012-01-25 ビーエーエスエフ ソシエタス・ヨーロピア ３−フェニル（チオ）ウラシル類およびジチオウラシル類を製造する方法
US7887824B2 (en) 2004-11-30 2011-02-15 L'oreal Sulfamide derivatives and cosmetic use thereof
FR2878523B1 (fr) * 2004-11-30 2007-09-14 Oreal Nouveaux derives sulfamides et leur utilisation cosmetique
MX2007013961A (es) * 2005-05-24 2008-01-14 Basf Ag Metodo para producir 1-alquil-3-feniluracilos.
AP2344A (en) 2005-07-07 2011-12-28 Basf Ag N-Thio-anthranilamid compounds and their use as pesticides.
CA2821517A1 (en) * 2005-12-01 2007-06-07 Basf Se Process for producing nitrobenzoyl chloride
TWI423766B (zh) * 2006-10-13 2014-01-21 Basf Ag ２-氯-５-〔３，６-二氫-３-甲基-２，６-二酮基-４-（三氟甲基）-１-（２ｈ）-嘧啶基〕-４-氟-ｎ-〔〔甲基（１-甲基乙基）胺基〕磺醯基〕苯甲醯胺之結晶型
KR101508017B1 (ko) * 2006-10-13 2015-04-08 바스프 에스이 2-클로로-5-［3,6-디히드로-3-메틸-2,6-디옥소-4-(트리플루오로-메틸)-1-(2ｈ)-피리미디닐］-4-플루오로-ｎ-［［메틸-(1-메틸에틸)-아미노］술포닐］벤즈아미드의 수화물
AR068849A1 (es) 2007-10-12 2009-12-09 Basf Se Procedimiento para la preparacion de diamidas de acido sulfonico
RU2547433C2 (ru) 2009-08-27 2015-04-10 Басф Се Водный суспензионный концентрированный состав, содержащий сафлуфенацил, его применение и способ борьбы с нежелательной растительностью
WO2011023758A2 (en) 2009-08-27 2011-03-03 Basf Se Aqueous concentrate formulations containing saflufenacil and glyphosate
US8703650B2 (en) 2009-12-09 2014-04-22 Basf Se Liquid suspension concentrate formulations containing saflufenacil
WO2011070054A1 (en) 2009-12-09 2011-06-16 Basf Se Liquid suspension concentrate formulations containing saflufenacil and glyphosate
WO2011104213A2 (de) 2010-02-26 2011-09-01 Bayer Cropscience Ag Herbizide zusammensetzung enthaltend die hydrate von saflufenacil und glyphosate oder glufosinate
CN104487439B (zh) 2012-05-24 2017-06-09 巴斯夫欧洲公司 N‑硫代邻氨基苯甲酰胺化合物及其作为杀害虫剂的用途
WO2015091642A1 (en) 2013-12-19 2015-06-25 BASF Agro B.V. Dilute aqueous compositions of saflufenacil
BR112017015016A2 (pt) 2015-01-15 2018-01-23 Basf Se combinação herbicida, e, métodos para controlar vegetação indesejável e para tratamento de dessecação de vegetação indesejável em cultivos
AU2016208585A1 (en) 2015-01-22 2017-08-03 BASF Agro B.V. Ternary herbicidal combination comprising saflufenacil
AU2016292677B2 (en) 2015-07-10 2020-09-24 BASF Agro B.V. Herbicidal composition comprising cinmethylin and specific quinolinecarboxylic acids
US10813356B2 (en) 2015-07-10 2020-10-27 BASF Agro B.V. Herbicidal composition comprising cinmethylin and dimethenamid
JP6875368B2 (ja) 2015-07-10 2021-05-26 ビーエーエスエフ アグロ ベー．ブイ． シンメチリン及びアセトクロール又はプレチラクロールを含む除草剤組成物
US11219215B2 (en) 2015-07-10 2022-01-11 BASF Agro B.V. Herbicidal composition comprising cinmethylin and specific inhibitors of protoporphyrinogen oxidase
US11219212B2 (en) 2015-07-10 2022-01-11 BASF Agro B.V. Herbicidal composition comprising cinmethylin and imazamox
HUE044213T2 (hu) 2015-07-10 2019-10-28 Basf Agro Bv Cinmetilint és petoxamidot tartalmazó herbicid készítmény
PL3319437T3 (pl) 2015-07-10 2020-03-31 BASF Agro B.V. Kompozycja chwastobójcza zawierająca cynmetylinę i piroksasulfon
CN107846893B (zh) 2015-07-10 2024-02-20 巴斯夫农业公司 包含环庚草醚和苯嘧磺草胺的除草组合物
WO2017009142A1 (en) 2015-07-10 2017-01-19 BASF Agro B.V. Herbicidal composition comprising cinmethylin and specific pigment synthesis inhibitors
ES2918016T3 (es) 2015-07-24 2022-07-13 Basf Se Compuestos de piridina útiles para combatir hongos fitopatógenos
UA121417C2 (uk) 2015-09-03 2020-05-25 Басф Агро Б.В. Композиція мікрочастинок, яка містить сафлуфенацил
WO2018019845A1 (en) 2016-07-29 2018-02-01 Basf Se Method for controlling ppo resistant weeds
JP7171555B2 (ja) * 2016-10-19 2022-11-15 ハイドロ－ケベック スルファミン酸誘導体およびその調製のためのプロセス
CN107827786A (zh) * 2017-11-24 2018-03-23 常州沃腾化工科技有限公司 N‑甲基‑n‑异丙基胺基磺酰胺的生产方法
US20230309560A1 (en) 2019-08-26 2023-10-05 Adama Agan Ltd. Soluble liquid compositions of saflufenacil, method of preparation and use thereof
AR124927A1 (es) 2021-02-24 2023-05-17 Adama Agan Ltd Composiciones herbicidas que comprenden inhibidores de acetolactato sintasa a base de imidazolinona y usos de los mismos
CN116917274A (zh) 2021-03-04 2023-10-20 安道麦阿甘有限公司 苯嘧磺草胺-钠和苯嘧磺草胺-钾的固体形式、其制备方法和用途
CA3228537A1 (en) 2021-08-09 2023-02-16 Adama Agan Ltd. A new process of saflufenacil production using novel intermediates
CN114350340B (zh) * 2022-01-13 2023-01-17 陕西科技大学 一种压裂用增渗剂及其制备方法和应用
WO2023232507A1 (en) 2022-05-30 2023-12-07 BASF Agro B.V. Process for recovering saflufenacil from process streams
WO2024012913A1 (en) 2022-07-13 2024-01-18 BASF Agro B.V. Herbicidal eode formulation comprising several active ingredients
CN115353618B (zh) * 2022-08-18 2024-02-09 吴利军 耐温型页岩抑制剂及其制备方法
WO2024042134A1 (en) 2022-08-26 2024-02-29 BASF Agro B.V. Aqueous herbicide formulations

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE946710C (de) 1954-06-29 1956-08-02 Bayer Ag Verfahren zur Herstellung von N-disubstituierten Sulfamidsaeurechloriden
DE1028129B (de) * 1956-11-03 1958-04-17 Bayer Ag Verfahren zur Herstellung von N-disubstituierten Sulfamidsaeurechloriden
DE1242627B (de) 1964-07-25 1967-06-22 Basf Ag Verfahren zur Herstellung von N-Alkyl- oder -Cycloalkylamidosulfonylchloriden
US3992444A (en) * 1972-12-19 1976-11-16 Basf Aktiengesellschaft Production of sulfamic acid halides
DE2408530A1 (de) * 1974-02-22 1975-09-04 Basf Ag Verfahren zur herstellung von betahalogenalkylaminosulfonylhalogeniden
DE2553461A1 (de) * 1975-11-28 1977-06-08 Basf Ag Sulfamidsaeurehalogenide und verfahren zu ihrer herstellung
DE2634485A1 (de) * 1976-07-31 1978-02-02 Basf Ag Sulfamidsaeurehalogenide und verfahren zu ihrer herstellung
DE2852274A1 (de) * 1978-12-02 1980-06-19 Basf Ag Verfahren zur herstellung von sulfamidsaeurehalogeniden
JPS5592366A (en) * 1978-12-28 1980-07-12 Hokko Chem Ind Co Ltd O-sulfamoylglycolic acid amide derivative
DE3428837A1 (de) * 1984-06-30 1986-01-09 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von n-phenyl(pyridyl)-sulfonyldiamiden
DE4020052A1 (de) * 1990-06-23 1992-01-02 Bayer Ag Verfahren zur herstellung von 2-chlor-5-methyl-pyridin
WO1998028280A1 (en) 1996-12-23 1998-07-02 Fmc Corporation Certain 3-[2,4-disubstituted-5-(substituted amino)phenyl]-1-substituted-6-trifluoromethyl-2,4-(1h,3h)-pyrimidinedione derivatives as herbicides
GB9821199D0 (en) 1998-09-30 1998-11-25 Glaxo Group Ltd Chemical compounds
EA005677B1 (ru) * 2000-05-04 2005-04-28 Басф Акциенгезельшафт Гетероциклилзамещенные фенилсульфамоилкарбоксамиды

Also Published As

Publication number Publication date
KR100973619B1 (ko) 2010-08-02
WO2003097589A1 (de) 2003-11-27
ATE452875T1 (de) 2010-01-15
BR0309922B1 (pt) 2013-04-09
US20050159622A1 (en) 2005-07-21
CA2485360A1 (en) 2003-11-27
IL164739A0 (en) 2005-12-18
PL374371A1 (en) 2005-10-17
CN100509771C (zh) 2009-07-08
KR20040111616A (ko) 2004-12-31
JP2005530794A (ja) 2005-10-13
DE50312258D1 (ru) 2010-02-04
IL164739A (en) 2012-05-31
JP4384028B2 (ja) 2009-12-16
DK1506169T3 (da) 2010-04-19
CN1653043A (zh) 2005-08-10
AU2003240656A1 (en) 2003-12-02
BR0309922A (pt) 2005-02-15
ES2337779T3 (es) 2010-04-29
MXPA04010748A (es) 2005-03-07
EP1506169B1 (de) 2009-12-23
EP1506169A1 (de) 2005-02-16
ZA200410075B (en) 2006-07-26
US7232926B2 (en) 2007-06-19

Similar Documents

Publication Publication Date Title
EA200401483A1 (ru) Способ получения галогенангидридов сульфаминовой кислоты
DE60316728D1 (de) Phosphonium- und imidazoliumsalze und verfahren zu deren herstellung
DE502005006163D1 (de) Verfahren zur herstellung quartärer ammoniumverbindungen hoher reinheit
CO5650237A2 (es) Procedimiento de sintesis selectiva de drivados de 2-amino-5-trifluorometil-pirimidina en presencia de un acido de lewis
TW200504084A (en) Process for preparing acylphosphanes and derivatives thereof
DE60321030D1 (de) Verfahren zur herstellung von (-)-(s)-3-ä1-(dimethylamino)ethylü phenyl-n-ethyl-n-methylcarbamat
FR2814747B1 (fr) Procede de fabrication de polyamides
PL360494A1 (en) Process to prepare sulfonamides
DE59813264D1 (de) Wässrige kationische tensidzubereitungen, ein verfahren zu ihrer herstellung sowie ihre verwendung
EP0301716A3 (en) Polyamidopolyamines
DE602004008496D1 (de) Verfahren zur herstellung von (s)-glyceraldehydacetonid
NO20053176L (no) Fremgangsmate for fremstilling av tolperisonsalter.
ATE419230T1 (de) Verfahren zur herstellung von 2,6-dihalo-para- trifluoromethylanilin
ES2109236T3 (es) Reactivos tioacilantes y compuestos intermedios, tiopeptidos, y metodos para prepararlos y utilizarlos.
ES8405011A1 (es) Procedimiento para la obtencion de sales de yodopropargilamonio.
BR0214956A (pt) Processo para a preparação de derivados da [1,4,5]-oxadiazepina
DK0684227T3 (da) Fremgangsmåde til fremstilling af guanidiner
NO20043047L (no) Mellomprodukter for LHRH-antagonistsyntese, fremgangsmate for fremstilling derav og fremgangsmate for LHRH-antagonistfremstilling
DE50212739D1 (de) Verfahren zur herstellung von isocyanaten
ATE359992T1 (de) Verfahren zur herstellung von sekundären aminen aus nitrilen
DE50206142D1 (de) Verfahren zur herstellung von 1,3-disubstituierten 2-nitroguanidinen
WO2003068726A1 (fr) Derive amide d'amine alicyclique et procede de production de celui-ci
NO20012874L (no) Acylisotiocyanatharpikser og deres anvendelse ved faststoff- bårede synteser av guanidiner
TW200722409A (en) Preparation of thioalkylamines using chlorosulfonic acid
EP0098951A3 (en) Aminobenzamide derivatives and preparation thereof