KR840003634A - 클로로아세트 아미드 유도체의 제조방법 - Google Patents

클로로아세트 아미드 유도체의 제조방법 Download PDF

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KR840003634A
KR840003634A KR1019830000493A KR830000493A KR840003634A KR 840003634 A KR840003634 A KR 840003634A KR 1019830000493 A KR1019830000493 A KR 1019830000493A KR 830000493 A KR830000493 A KR 830000493A KR 840003634 A KR840003634 A KR 840003634A
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세킨저(외 2) 카알
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진 크라머, 한스 루돌프 하우스
산도즈 리미티드
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  • Heterocyclic Compounds Containing Sulfur Atoms (AREA)
  • Thiazole And Isothizaole Compounds (AREA)
  • Furan Compounds (AREA)
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  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

내용 없음

Description

클로로아세트 아미드 유도체의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (1)

  1. 다음 일반식(Ⅱ)의 화합물에서 N-하이드록시 아세틸기중 HO기를 Cl로 치환시키거나, 다음 일반식(Ⅲ)의 화합물을 다음 일반식(Ⅳ)의 화합물의 반응시키거나, 다음 일반식(Ⅴ)의 화합물을 다음 일반식(Ⅵ)화합물의 반응성 유도체와 반응시켜 다음 일반식(Ⅰa)의 화합물을 제조하거나, 다음 일반식(Ⅶ)의 화합물을 클로로아세틸클로라이드 또는 그의 반응작용 유도체와 N-아실화시킴을 특징으로 하여 다음 일반식(Ⅰ)의 화합물을 제조하는 방법.
    상기 일반식에서, Ar은 O,S 및 N 중에서 선택된 1 내지 2개의 환복소원자를 함유하는 5원-헤테로 방향족기로서, 이것이 결합되어 있는 N(Y)COCH2Cl기의 N-원자와 C-환원자에 의해 연결되어 있으며, Ar이 피라졸릴일 경우, 상기 N(Y)COCH2Cl기는 4-위치에 존재하고, Y는 알렌, CH2-CH=C=CH2;C1-8알킬, C3-8알케닐, C3-8알키닐, C3-8사이클로알킬, C5-8사이클로알케닐 또는 C3-8사이클로알킬-C1-5알킬 중에서 선택된 탄화수소(이탄화수소는 비치환되거나 F, Cl 또는 Br 중에서 선택된 할로겐으로 치환됨):
    일반식 CH(R1)-COY1의 기, (여기서 R1은 H 또는 C1-5알킬이고, Y1은 이것이 결합되어 있는 CC-기와 함께 에스테르 또는 아미드작용기를 형성한다.);
    일반식 R2-Az의 기, (여기서 R2는 비치환되거나 C1-5알킬로 치환됨 CH2또는 CH2-CH2이고, AZ는 함유하는 질소원자중 하나가 R2는 결합되어 있는 디-또는 트리아졸 중에서 선택된 방향족 복소환)상기환중 C-원자에 의해 R2와 결합되며 O,S 및 중에서 선택된 1내지 3개의 복소원자를 가진 5-원 복소환, 및 피리미딘기중에서 선택된 방향족 복소환이거나, 또는 CH2기가 O,S 또는 NCH3에 의해 치환될 수 있는 2-옥소-1-피롤리디닐기 또는 이 2-옥소-1-피롤리디닐기의 5-옥소-및/또는 비사이클릭벤즈[c]융합 유도체이다);
    일반식 A-O-R3-의 기, (여기서 R3는 H; C1-8알킬, C3-8알케닐, C3-8알키닐, C3-8사이클로알킬, C5-사이클로알케닐 또는 C3-8사이클로알킬-C-1-5알킬중에서 선택된 탄화수소(이탄화수소는 비치환되거나 치환됨); 또는 일반식의 기[여기서 R4는 C1-5알킬, C3-5알케닐, C3-8알키닐, C5-9사이클로알킬, C3-8사이클로알케닐 또는 C3-8사이클로알킬-C1-5알킬중에서 선택된 탄화수소(이 탄화수소는 비치환되거나 F,Cl 또는 Br중에서 선택된 할로겐으로 치환됨) 또는 알렌이고,R4'는 H 또는 R4에서 정의한 것중 하나이다]이고 A는 탄화수소 잔기로써, R3와 함게 복소원자로서 1내지 2개의 산소를 함유하는 산소함유 포화복소환을 형성할 수 있고, A가 결합되어 있는 N 및 0원자는 3개이하의 C-원자로서 분리된다);
    일반식의 기, (여기서 R4는 전술한 바와같고 R5및 R5'는 독립적으로 H 또는 CH3이거나 R5는 R5'와 함께(CH2)3의 또는 (CH2)4를 나타낸다); 또는 일반식의 기이고(여기서 R6는 H 또는 C1-3알킬이다).L은 N-알킬화반응 조건화에서 분리될 수 있는 이탈기이고, R′은 H또는 C1-3알킬이며, Y2는 Az, OR3또는 N(CH3)COCH3이며, Az'은 함유된 질소원자중 하나에 의해 CHR'과 결합되어 있는 디-또는 트리아졸이다.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019830000493A 1982-02-09 1983-02-08 클로로아세트 아미드 유도체의 제조방법 KR880002359B1 (ko)

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