KR102706473B1 - 수지 첨가제 조성물 및 이것을 사용한 합성 수지 조성물 - Google Patents

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Publication number

KR102706473B1

KR102706473B1 KR1020227040684A KR20227040684A KR102706473B1 KR 102706473 B1 KR102706473 B1 KR 102706473B1 KR 1020227040684 A KR1020227040684 A KR 1020227040684A KR 20227040684 A KR20227040684 A KR 20227040684A KR 102706473 B1 KR102706473 B1 KR 102706473B1

Authority

KR

South Korea

Prior art keywords

molding

mass

tert

parts

synthetic resin

Prior art date

2015-08-20

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• 239000000203 mixture Substances 0.000 title claims abstract description 80
• 229920003002 synthetic resin Polymers 0.000 title claims abstract description 49
• 239000000057 synthetic resin Substances 0.000 title claims abstract description 49
• 229920005989 resin Polymers 0.000 title abstract description 82
• 239000011347 resin Substances 0.000 title abstract description 82
• 239000000654 additive Substances 0.000 title abstract description 61
• 230000000996 additive effect Effects 0.000 title abstract description 54
• -1 phosphate ester Chemical class 0.000 claims abstract description 67
• 229910052751 metal Inorganic materials 0.000 claims abstract description 38
• 239000002184 metal Substances 0.000 claims abstract description 38
• 150000003839 salts Chemical class 0.000 claims abstract description 28
• 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 19
• 239000000194 fatty acid Substances 0.000 claims abstract description 19
• 229930195729 fatty acid Natural products 0.000 claims abstract description 19
• ZHROMWXOTYBIMF-UHFFFAOYSA-M sodium;1,3,7,9-tetratert-butyl-11-oxido-5h-benzo[d][1,3,2]benzodioxaphosphocine 11-oxide Chemical compound [Na+].C1C2=CC(C(C)(C)C)=CC(C(C)(C)C)=C2OP([O-])(=O)OC2=C1C=C(C(C)(C)C)C=C2C(C)(C)C ZHROMWXOTYBIMF-UHFFFAOYSA-M 0.000 claims abstract description 19
• 150000004665 fatty acids Chemical class 0.000 claims abstract description 14
• 238000000465 moulding Methods 0.000 claims description 28
• 125000004432 carbon atom Chemical group C* 0.000 claims description 13
• 238000001746 injection moulding Methods 0.000 claims description 12
• 238000001125 extrusion Methods 0.000 claims description 9
• 125000000217 alkyl group Chemical group 0.000 claims description 8
• 125000004429 atom Chemical group 0.000 claims description 7
• 239000000835 fiber Substances 0.000 claims description 6
• 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 6
• 125000001931 aliphatic group Chemical group 0.000 claims description 5
• 229920005672 polyolefin resin Polymers 0.000 claims description 5
• 125000001118 alkylidene group Chemical group 0.000 claims description 4
• 238000000071 blow moulding Methods 0.000 claims description 3
• 238000010097 foam moulding Methods 0.000 claims description 3
• 229910001386 lithium phosphate Inorganic materials 0.000 claims description 3
• 229920005992 thermoplastic resin Polymers 0.000 claims description 3
• 238000000748 compression moulding Methods 0.000 claims description 2
• 239000000463 material Substances 0.000 claims description 2
• 238000004321 preservation Methods 0.000 claims description 2
• 238000003860 storage Methods 0.000 claims description 2
• 239000008188 pellet Substances 0.000 abstract description 39
• 230000000694 effects Effects 0.000 abstract description 20
• 229910019142 PO4 Inorganic materials 0.000 abstract description 18
• 239000010452 phosphate Substances 0.000 abstract description 18
• 238000002156 mixing Methods 0.000 abstract description 10
• 229910003002 lithium salt Inorganic materials 0.000 abstract description 7
• 238000004519 manufacturing process Methods 0.000 description 20
• 238000000034 method Methods 0.000 description 16
• 239000003963 antioxidant agent Substances 0.000 description 15
• 230000000052 comparative effect Effects 0.000 description 14
• 239000002530 phenolic antioxidant Substances 0.000 description 13
• 239000003484 crystal nucleating agent Substances 0.000 description 12
• 230000003078 antioxidant effect Effects 0.000 description 11
• 239000000975 dye Substances 0.000 description 10
• 239000000843 powder Substances 0.000 description 10
• 239000002216 antistatic agent Substances 0.000 description 9
• 150000001875 compounds Chemical class 0.000 description 9
• 238000002425 crystallisation Methods 0.000 description 9
• 230000008025 crystallization Effects 0.000 description 9
• 229920001577 copolymer Polymers 0.000 description 8
• 239000000049 pigment Substances 0.000 description 8
• 239000003063 flame retardant Substances 0.000 description 7
• JXGYVEVKKCXZAO-UHFFFAOYSA-N 2,6-ditert-butyl-4-[3-[3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)prop-1-ynoxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)prop-1-ynoxymethyl]propoxy]prop-2-ynyl]phenol Chemical compound C(C)(C)(C)C=1C=C(C=C(C=1O)C(C)(C)C)CC#COCC(COC#CCC1=CC(=C(C(=C1)C(C)(C)C)O)C(C)(C)C)(COC#CCC1=CC(=C(C(=C1)C(C)(C)C)O)C(C)(C)C)COC#CCC1=CC(=C(C(=C1)C(C)(C)C)O)C(C)(C)C JXGYVEVKKCXZAO-UHFFFAOYSA-N 0.000 description 6
• JKIJEFPNVSHHEI-UHFFFAOYSA-N Phenol, 2,4-bis(1,1-dimethylethyl)-, phosphite (3:1) Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP(OC=1C(=CC(=CC=1)C(C)(C)C)C(C)(C)C)OC1=CC=C(C(C)(C)C)C=C1C(C)(C)C JKIJEFPNVSHHEI-UHFFFAOYSA-N 0.000 description 6
• OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
• 229910052783 alkali metal Inorganic materials 0.000 description 6
• WPYMKLBDIGXBTP-UHFFFAOYSA-M benzoate Chemical compound [O-]C(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-M 0.000 description 6
• CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 6
• 239000008116 calcium stearate Substances 0.000 description 6
• 235000013539 calcium stearate Nutrition 0.000 description 6
• 238000002347 injection Methods 0.000 description 6
• 239000007924 injection Substances 0.000 description 6
• UADIOTAIECKQLQ-UHFFFAOYSA-M lithium;1,3,7,9-tetratert-butyl-11-oxido-5h-benzo[d][1,3,2]benzodioxaphosphocine 11-oxide Chemical compound [Li+].C1C2=CC(C(C)(C)C)=CC(C(C)(C)C)=C2OP([O-])(=O)OC2=C1C=C(C(C)(C)C)C=C2C(C)(C)C UADIOTAIECKQLQ-UHFFFAOYSA-M 0.000 description 6
• 230000000704 physical effect Effects 0.000 description 6
• FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
• ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 5
• 235000021355 Stearic acid Nutrition 0.000 description 5
• 239000013078 crystal Substances 0.000 description 5
• KJSPVJJOPONRTK-UHFFFAOYSA-M lithium;tetradecanoate Chemical compound [Li+].CCCCCCCCCCCCCC([O-])=O KJSPVJJOPONRTK-UHFFFAOYSA-M 0.000 description 5
• 229910052749 magnesium Inorganic materials 0.000 description 5
• 239000011777 magnesium Substances 0.000 description 5
• QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 5
• OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 5
• NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 5
• OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 description 5
• 229910052698 phosphorus Inorganic materials 0.000 description 5
• 239000011574 phosphorus Substances 0.000 description 5
• 239000008117 stearic acid Substances 0.000 description 5
• FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 4
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
• ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 4
• 229920011250 Polypropylene Block Copolymer Polymers 0.000 description 4
• 239000007983 Tris buffer Substances 0.000 description 4
• 150000001340 alkali metals Chemical class 0.000 description 4
• 229910052782 aluminium Inorganic materials 0.000 description 4
• XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
• IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 4
• UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 4
• POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 4
• ZQPPMHVWECSIRJ-MDZDMXLPSA-N elaidic acid Chemical compound CCCCCCCC\C=C\CCCCCCCC(O)=O ZQPPMHVWECSIRJ-MDZDMXLPSA-N 0.000 description 4
• 229920001971 elastomer Polymers 0.000 description 4
• 239000000945 filler Substances 0.000 description 4
• IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
• QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 4
• 238000002844 melting Methods 0.000 description 4
• 230000008018 melting Effects 0.000 description 4
• VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
• 239000002667 nucleating agent Substances 0.000 description 4
• WQEPLUUGTLDZJY-UHFFFAOYSA-N pentadecanoic acid Chemical compound CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 4
• 150000004671 saturated fatty acids Chemical class 0.000 description 4
• 239000000344 soap Substances 0.000 description 4
• 150000005846 sugar alcohols Polymers 0.000 description 4
• WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 3
• RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 3
• LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 3
• QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 3
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
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• 229940126062 Compound A Drugs 0.000 description 3
• NLDMNSXOCDLTTB-UHFFFAOYSA-N Heterophylliin A Natural products O1C2COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC2C(OC(=O)C=2C=C(O)C(O)=C(O)C=2)C(O)C1OC(=O)C1=CC(O)=C(O)C(O)=C1 NLDMNSXOCDLTTB-UHFFFAOYSA-N 0.000 description 3
• 239000005642 Oleic acid Substances 0.000 description 3
• 229920000388 Polyphosphate Polymers 0.000 description 3
• 239000004743 Polypropylene Substances 0.000 description 3
• XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 3
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
• 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 3
• FQUNFJULCYSSOP-UHFFFAOYSA-N bisoctrizole Chemical compound N1=C2C=CC=CC2=NN1C1=CC(C(C)(C)CC(C)(C)C)=CC(CC=2C(=C(C=C(C=2)C(C)(C)CC(C)(C)C)N2N=C3C=CC=CC3=N2)O)=C1O FQUNFJULCYSSOP-UHFFFAOYSA-N 0.000 description 3
• 239000003054 catalyst Substances 0.000 description 3
• 239000003795 chemical substances by application Substances 0.000 description 3
• GDVKFRBCXAPAQJ-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O GDVKFRBCXAPAQJ-UHFFFAOYSA-A 0.000 description 3
• SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 3
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• WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 3
• 239000004299 sodium benzoate Substances 0.000 description 3
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• 239000012321 sodium triacetoxyborohydride Substances 0.000 description 3
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• 239000011701 zinc Substances 0.000 description 3
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• YWEWWNPYDDHZDI-JJKKTNRVSA-N (1r)-1-[(4r,4ar,8as)-2,6-bis(3,4-dimethylphenyl)-4,4a,8,8a-tetrahydro-[1,3]dioxino[5,4-d][1,3]dioxin-4-yl]ethane-1,2-diol Chemical compound C1=C(C)C(C)=CC=C1C1O[C@H]2[C@@H]([C@H](O)CO)OC(C=3C=C(C)C(C)=CC=3)O[C@H]2CO1 YWEWWNPYDDHZDI-JJKKTNRVSA-N 0.000 description 2
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• IANQTJSKSUMEQM-UHFFFAOYSA-N 1-benzofuran Chemical compound C1=CC=C2OC=CC2=C1 IANQTJSKSUMEQM-UHFFFAOYSA-N 0.000 description 2
• NWDVCUXGELFJOC-UHFFFAOYSA-N 1-n,2-n,3-n-tris(2-methylcyclohexyl)propane-1,2,3-tricarboxamide Chemical compound CC1CCCCC1NC(=O)CC(C(=O)NC1C(CCCC1)C)CC(=O)NC1C(C)CCCC1 NWDVCUXGELFJOC-UHFFFAOYSA-N 0.000 description 2
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• ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 2
• HXIQYSLFEXIOAV-UHFFFAOYSA-N 2-tert-butyl-4-(5-tert-butyl-4-hydroxy-2-methylphenyl)sulfanyl-5-methylphenol Chemical compound CC1=CC(O)=C(C(C)(C)C)C=C1SC1=CC(C(C)(C)C)=C(O)C=C1C HXIQYSLFEXIOAV-UHFFFAOYSA-N 0.000 description 2
• XOUQAVYLRNOXDO-UHFFFAOYSA-N 2-tert-butyl-5-methylphenol Chemical compound CC1=CC=C(C(C)(C)C)C(O)=C1 XOUQAVYLRNOXDO-UHFFFAOYSA-N 0.000 description 2
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• MBMBGCFOFBJSGT-KUBAVDMBSA-N all-cis-docosa-4,7,10,13,16,19-hexaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCC(O)=O MBMBGCFOFBJSGT-KUBAVDMBSA-N 0.000 description 2
• DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 2
• WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 2
• ZGNIGAHODXRWIT-UHFFFAOYSA-K aluminum;4-tert-butylbenzoate Chemical compound [Al+3].CC(C)(C)C1=CC=C(C([O-])=O)C=C1.CC(C)(C)C1=CC=C(C([O-])=O)C=C1.CC(C)(C)C1=CC=C(C([O-])=O)C=C1 ZGNIGAHODXRWIT-UHFFFAOYSA-K 0.000 description 2
• 125000000129 anionic group Chemical group 0.000 description 2
• 150000001450 anions Chemical class 0.000 description 2
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