KR102105599B1 - 에틸렌의 카보닐화를 위한 연속 공정 - Google Patents

에틸렌의 카보닐화를 위한 연속 공정 Download PDF

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KR102105599B1
KR102105599B1 KR1020147020382A KR20147020382A KR102105599B1 KR 102105599 B1 KR102105599 B1 KR 102105599B1 KR 1020147020382 A KR1020147020382 A KR 1020147020382A KR 20147020382 A KR20147020382 A KR 20147020382A KR 102105599 B1 KR102105599 B1 KR 102105599B1
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phosphinomethyl
bis
butylphosphinomethyl
tetramethyl
adamantyl
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KR20140107549A (ko
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네일 틴들
그레이엄 로널드 이스텀
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루사이트 인터내셔널 유케이 리미티드
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/36Preparation of carboxylic acid esters by reaction with carbon monoxide or formates
    • C07C67/38Preparation of carboxylic acid esters by reaction with carbon monoxide or formates by addition to an unsaturated carbon-to-carbon bond
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
KR1020147020382A 2011-12-21 2012-12-20 에틸렌의 카보닐화를 위한 연속 공정 Active KR102105599B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB1122054.8 2011-12-21
GB201122054A GB201122054D0 (en) 2011-12-21 2011-12-21 A continuous process for the carbonylation of ethylene
PCT/GB2012/053204 WO2013093472A1 (en) 2011-12-21 2012-12-20 A continuous process for the carbonylation of ethylene

Publications (2)

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KR20140107549A KR20140107549A (ko) 2014-09-04
KR102105599B1 true KR102105599B1 (ko) 2020-04-28

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KR1020147020382A Active KR102105599B1 (ko) 2011-12-21 2012-12-20 에틸렌의 카보닐화를 위한 연속 공정

Country Status (18)

Country Link
US (1) US9382190B2 (enExample)
EP (1) EP2794548B1 (enExample)
JP (3) JP2015502393A (enExample)
KR (1) KR102105599B1 (enExample)
CN (2) CN106928061B (enExample)
AU (1) AU2012356457B2 (enExample)
BR (1) BR112014015157B1 (enExample)
CA (1) CA2857572C (enExample)
EA (1) EA032583B1 (enExample)
ES (1) ES2742329T3 (enExample)
GB (1) GB201122054D0 (enExample)
IN (1) IN2014DN05822A (enExample)
MX (1) MX348494B (enExample)
MY (1) MY171403A (enExample)
SG (2) SG11201402921RA (enExample)
TW (1) TWI631103B (enExample)
WO (1) WO2013093472A1 (enExample)
ZA (1) ZA201404484B (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB201122054D0 (en) * 2011-12-21 2012-02-01 Lucite Int Uk Ltd A continuous process for the carbonylation of ethylene
CN112898123B (zh) * 2019-11-19 2022-02-11 中国科学院大连化学物理研究所 一种制备丙醇的方法
US20240083926A1 (en) * 2020-12-15 2024-03-14 Agency For Science, Technology And Research Phosphorus compounds and methods thereof
CN115959994B (zh) * 2021-10-13 2025-11-04 上海浦景化工技术股份有限公司 一种制备高纯度mma的系统及方法
CN115957823B (zh) * 2021-10-13 2025-04-08 上海浦景化工技术股份有限公司 一种乙烯羰基化催化剂及其应用
CN116139939B (zh) * 2022-12-28 2025-08-26 浙江新和成股份有限公司 催化剂体系和羰基化反应的方法
CN116082157B (zh) * 2023-01-18 2025-09-16 上海梓龄化工技术有限公司 一种烯属不饱和化合物烷氧羰基化反应制备有机羧酸酯的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011073653A1 (en) * 2009-12-15 2011-06-23 Lucite International Uk Limited Improved carbonylation process

Family Cites Families (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5440901A (en) * 1977-09-07 1979-03-31 Masabumi Isobe Flash tank which houses filler
US4262138A (en) 1979-04-09 1981-04-14 Chem Systems Inc. Preparation of carboxylic acid esters with BF3 complex catalyst
EP0055875B1 (en) 1981-01-06 1986-08-20 Shell Internationale Researchmaatschappij B.V. Process for the carbonylation of olefins
CA1231346A (en) 1982-09-30 1988-01-12 Eit Drent Process for the carbonylation of olefinically unsaturated compounds with a palladium catalyst
JPS62102883A (ja) * 1985-10-30 1987-05-13 Hitachi Ltd 廃液濃縮器
GB8531624D0 (en) 1985-12-23 1986-02-05 Shell Int Research Carbonylation of ethylenically unsaturated compounds
GB8605034D0 (en) 1986-02-28 1986-04-09 Shell Int Research Carbonylation of compounds
KR880007426A (ko) 1986-12-24 1988-08-27 오노 알버어스 팔라듐 촉매를 사용한 올레핀형 불포화 화합물의 카르보닐화 방법
GB8705699D0 (en) 1987-03-11 1987-04-15 Shell Int Research Carbonylation of olefinically unsaturated compounds
KR0144567B1 (ko) 1989-03-03 1998-07-15 오노 알버어스 카르보닐화촉매시스템
CA2034971A1 (en) 1990-02-05 1991-08-06 Eit Drent Carbonylation catalyst system
FI91135C (fi) 1990-03-19 1994-05-25 Valmet Paper Machinery Inc Menetelmä reikien poraamiseksi paperikoneen sylinterin vaippaan ja menetelmässä käytetty laitteisto
CA2055628A1 (en) 1990-12-03 1992-06-04 Eit Drent Carbonylation process and catalyst composition
DE69204691T2 (de) 1991-01-15 1996-04-11 Shell Int Research Verfahren zur Karbonylierung von Olefin.
ES2088082T3 (es) 1991-01-15 1996-08-01 Shell Int Research Carbonilacion de olefinas.
ES2054519T3 (es) 1991-02-15 1994-08-01 Shell Int Research Sistema de catalizador de carbonilacion.
JP3489592B2 (ja) * 1994-02-28 2004-01-19 三菱瓦斯化学株式会社 エステル類の製造方法
GB9425911D0 (en) 1994-12-22 1995-02-22 Ici Plc Process for the carbonylation of olefins and catalyst system for use therein
JP2922848B2 (ja) * 1996-06-14 1999-07-26 株式会社日本触媒 芳香族炭酸エステルの製造方法
GB9705699D0 (en) * 1997-03-19 1997-05-07 Ici Plc Process for the carbonylation of ethylene
US6156934A (en) 1997-03-26 2000-12-05 Shell Oil Company Diphosphines
MY127358A (en) 2000-03-14 2006-11-30 Shell Int Research Process for the carbonylation of ethylenically unsaturated compounds
DE10048874A1 (de) 2000-09-29 2002-04-11 Basf Ag Katalysatorsystem und Verfahren zur Carbonylierung
DE10228293A1 (de) 2001-07-28 2003-02-13 Basf Ag Verfahren zur Herstellung von Dialkylketonen
JP2003267917A (ja) * 2002-03-15 2003-09-25 Mitsubishi Chemicals Corp 蒸留塔の運転停止方法
JP2003113138A (ja) * 2001-10-09 2003-04-18 Mitsubishi Chemicals Corp (メタ)アクリル酸類の蒸留方法
EP1478463B1 (en) 2002-02-19 2012-04-11 Lucite International UK Limited Process for the carbonylation of an ethylenically unsaturated compound and catalyst therefore
EP1554039B1 (en) 2002-09-12 2013-07-03 Lucite International UK Limited A catalyst system comprising a 1,2-bis-(phosphino)metallocene ligand
BRPI0410471A (pt) 2003-05-22 2006-05-30 Shell Int Research processo para a carbonilação de um dieno conjugado, ligante de difosfina bidentada, composição catalìtica, e, composição de produto de carbonilação
GB0403592D0 (en) 2004-02-18 2004-03-24 Lucite Int Uk Ltd A catalyst system
CA2557362A1 (en) 2004-02-26 2005-09-09 Shell Internationale Research Maatschappij B.V. Process for the carbonylation of ethylenically or acetylenically unsaturated compounds
MX2008000817A (es) * 2005-07-18 2008-03-14 Union Engineering As Un metodo para la recuperacion de dioxido de carbon de alta pureza a partir de una fuente gaseosa que comprende compuestos de nitrogeno.
GB0516556D0 (en) * 2005-08-12 2005-09-21 Lucite Int Uk Ltd Improved catalyst system
GB0921875D0 (en) * 2009-12-15 2010-01-27 Lucite Int Uk Ltd A continuous process for the carbonylation of ethylene
GB201122054D0 (en) * 2011-12-21 2012-02-01 Lucite Int Uk Ltd A continuous process for the carbonylation of ethylene

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011073653A1 (en) * 2009-12-15 2011-06-23 Lucite International Uk Limited Improved carbonylation process

Also Published As

Publication number Publication date
EA201491208A1 (ru) 2014-10-30
ZA201404484B (en) 2015-12-23
EA032583B1 (ru) 2019-06-28
CA2857572A1 (en) 2013-06-27
BR112014015157A8 (pt) 2017-07-04
BR112014015157B1 (pt) 2021-08-24
EP2794548A1 (en) 2014-10-29
BR112014015157A2 (pt) 2017-06-13
AU2012356457B2 (en) 2016-11-10
JP2017222683A (ja) 2017-12-21
MX348494B (es) 2017-06-15
SG11201402921RA (en) 2014-08-28
JP2015502393A (ja) 2015-01-22
US20150099896A1 (en) 2015-04-09
JP2019089844A (ja) 2019-06-13
MX2014007326A (es) 2014-09-22
JP6716503B2 (ja) 2020-07-01
WO2013093472A1 (en) 2013-06-27
EP2794548B1 (en) 2019-05-15
SG10201700374VA (en) 2017-03-30
TW201336822A (zh) 2013-09-16
KR20140107549A (ko) 2014-09-04
GB201122054D0 (en) 2012-02-01
CN104011007B (zh) 2017-04-12
ES2742329T3 (es) 2020-02-13
AU2012356457A1 (en) 2014-06-19
MY171403A (en) 2019-10-11
TWI631103B (zh) 2018-08-01
CN106928061A (zh) 2017-07-07
CA2857572C (en) 2021-03-16
CN106928061B (zh) 2020-08-28
IN2014DN05822A (enExample) 2015-06-26
US9382190B2 (en) 2016-07-05
CN104011007A (zh) 2014-08-27

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