KR101635046B1 - 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법 - Google Patents

5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법 Download PDF

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Publication number
KR101635046B1
KR101635046B1 KR1020127015772A KR20127015772A KR101635046B1 KR 101635046 B1 KR101635046 B1 KR 101635046B1 KR 1020127015772 A KR1020127015772 A KR 1020127015772A KR 20127015772 A KR20127015772 A KR 20127015772A KR 101635046 B1 KR101635046 B1 KR 101635046B1
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formula
pyrazole
fluoroalkyl
alkyl
methyl
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Korean (ko)
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KR20120084325A (ko
Inventor
세르기이 파제녹
노르베르트 루이
마르크 코슈텐
귄터 바르텔스
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바이엘 인텔렉쳐 프로퍼티 게엠베하
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16—Halogen atoms or nitro radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Diaphragms For Electromechanical Transducers (AREA)
  • Finger-Pressure Massage (AREA)
  • Vehicle Interior And Exterior Ornaments, Soundproofing, And Insulation (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020127015772A 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법 Active KR101635046B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US26264109P 2009-11-19 2009-11-19
US61/262,641 2009-11-19
EP09176426A EP2325173A1 (de) 2009-11-19 2009-11-19 Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
EP09176426.6 2009-11-19

Related Child Applications (1)

Application Number Title Priority Date Filing Date
KR1020167011442A Division KR101749561B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법

Publications (2)

Publication Number Publication Date
KR20120084325A KR20120084325A (ko) 2012-07-27
KR101635046B1 true KR101635046B1 (ko) 2016-07-01

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KR1020127015772A Active KR101635046B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법
KR1020167011442A Active KR101749561B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법

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KR1020167011442A Active KR101749561B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법

Country Status (13)

Country Link
US (2) US8436191B2 (https=)
EP (2) EP2325173A1 (https=)
JP (1) JP5802213B2 (https=)
KR (2) KR101635046B1 (https=)
CN (1) CN102666492B (https=)
BR (1) BR112012011961B1 (https=)
DK (1) DK2501682T3 (https=)
ES (1) ES2600864T3 (https=)
IL (1) IL219682A (https=)
IN (1) IN2012DN04414A (https=)
MX (2) MX2012005676A (https=)
TW (1) TWI510473B (https=)
WO (1) WO2011061205A1 (https=)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR076839A1 (es) 2009-05-15 2011-07-13 Bayer Cropscience Ag Derivados fungicidas de pirazol carboxamidas
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
MX2012012085A (es) 2010-04-23 2012-11-29 Bayer Ip Gmbh Procedimiento para la preparacion de cloruros y fluoruros de 5-fluoro-1-alquil-3-fluoroalquil-1h-pirazol-4-carbonilo.
JP6101345B2 (ja) * 2012-05-14 2017-03-22 バイエル・クロップサイエンス・アクチェンゲゼルシャフト １−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボニルクロライド類の製造方法
ES2628332T3 (es) 2012-08-07 2017-08-02 Bayer Cropscience Ag Procedimiento de preparación de pirazoles carboxilatos que contienen perfluoroalquilos
ES2610380T3 (es) * 2013-01-17 2017-04-27 Bayer Cropscience Ag Procedimiento de preparación de 5-fluoro-1-metil-3-difluorometil-1H-pirazol-4-carbaldehído
JP6366722B2 (ja) * 2013-09-20 2018-08-01 バイエル・クロップサイエンス・アクチェンゲゼルシャフト ５−フルオロ−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボアルデヒドの製造方法
JP6462703B2 (ja) * 2014-01-24 2019-01-30 バイエル・クロップサイエンス・アクチェンゲゼルシャフト １−アルキル−３−ジフルオロメチル−５−フルオロ−１ｈ−ピラゾール−４−カルバルデヒド類及び１−アルキル−３−ジフルオロメチル−５−フルオロ−１ｈ−ピラゾール−４−カルボキシレート類を調製する方法
JP6431088B2 (ja) 2014-03-24 2018-11-28 バイエル・クロップサイエンス・アクチェンゲゼルシャフト α，α−ジハロアミン類およびケチミン類からの３，５−ビス（ハロアルキル）ピラゾール誘導体の製造方法
EP3015458A1 (en) * 2014-11-03 2016-05-04 Bayer CropScience AG Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from a,a-dihaloamines and ketimines
TWI705055B (zh) 2015-04-29 2020-09-21 德商拜耳作物科學公司 製備5-氟-1h-吡唑-4-羰基氟化物之方法
WO2020093715A1 (en) 2018-11-07 2020-05-14 Fujian Yongjing Technology Co., Ltd New process for manufacture of pyrazoles or pyrimidones
US20230167062A1 (en) 2019-10-29 2023-06-01 Shenyang Sinochem Agrochemicals R&D Co., Ltd. Amide compound containing substituted acetophenone structural fragments and preparation method and application thereof
WO2022233129A1 (en) 2021-05-05 2022-11-10 Fujian Yongjing Technology Co., Ltd New process for the synthesis of 5-fluoro-3- (difuoromethyl) -5-fluoro-1-methyl-1h-pyrazole-4-carboxylic acid derivatives and the free acid thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993011117A1 (en) * 1991-12-06 1993-06-10 Monsanto Company Pyrazole carboxanilide fungicides

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Publication number Priority date Publication date Assignee Title
DE19544800A1 (de) * 1995-12-01 1997-06-05 Bayer Ag Verfahren zur Herstellung von 1,3-Dimethyl-5-fluor-pyrazol-4-carboxaniliden
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
EP1405853B1 (en) * 2001-06-21 2010-11-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
UA78071C2 (en) 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition
RU2346996C2 (ru) 2004-06-29 2009-02-20 ЮРОПИЭН НИКЕЛЬ ПиЭлСи Усовершенствованное выщелачивание основных металлов
AU2005273619B2 (en) 2004-08-18 2009-05-28 Pfizer Inc. Inhibitors of hepatitis C virus RNA-dependent RNA polymerase, and compositions and treatments using the same
US7930013B2 (en) 2005-06-29 2011-04-19 Compumedics Limited Sensor assembly with conductive bridge
DE102005044451A1 (de) * 2005-09-17 2007-03-22 Bayer Cropscience Gmbh Verfahren zum Herstellen von 5-Fluor-1,3-dialkyl-1H-pyrazol-4-carbonsäurefluoriden
EP1767353B1 (en) * 2005-09-27 2011-04-20 FUJIFILM Corporation Lithographic printing method
AR056882A1 (es) 2006-02-01 2007-10-31 Bayer Cropscience Sa Derivados del fungicida n- cicloalquil- bencil- amida
DE102007002674A1 (de) * 2007-01-18 2008-07-24 Bayer Cropscience Ag Verfahren zum Herstellen von substituierten Pyrazolcarbonsäurechloriden
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993011117A1 (en) * 1991-12-06 1993-06-10 Monsanto Company Pyrazole carboxanilide fungicides

Also Published As

Publication number Publication date
CN102666492B (zh) 2016-03-23
TW201127817A (en) 2011-08-16
EP2501682A1 (de) 2012-09-26
US20110207940A1 (en) 2011-08-25
JP5802213B2 (ja) 2015-10-28
TWI510473B (zh) 2015-12-01
US20130165664A1 (en) 2013-06-27
DK2501682T3 (en) 2016-11-14
US8765971B2 (en) 2014-07-01
WO2011061205A1 (de) 2011-05-26
IL219682A (en) 2016-08-31
IL219682A0 (en) 2012-07-31
MX2012005676A (es) 2012-06-19
BR112012011961B1 (pt) 2018-05-08
KR20160054041A (ko) 2016-05-13
KR101749561B1 (ko) 2017-06-21
MX344246B (es) 2016-12-07
EP2325173A1 (de) 2011-05-25
IN2012DN04414A (https=) 2015-08-07
ES2600864T3 (es) 2017-02-13
EP2501682B1 (de) 2016-08-03
US8436191B2 (en) 2013-05-07
JP2013511485A (ja) 2013-04-04
BR112012011961A2 (pt) 2015-09-08
KR20120084325A (ko) 2012-07-27
CN102666492A (zh) 2012-09-12

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