KR101602594B1 - 페놀의 정제 방법 - Google Patents

페놀의 정제 방법 Download PDF

Info

Publication number
KR101602594B1
KR101602594B1 KR1020147025855A KR20147025855A KR101602594B1 KR 101602594 B1 KR101602594 B1 KR 101602594B1 KR 1020147025855 A KR1020147025855 A KR 1020147025855A KR 20147025855 A KR20147025855 A KR 20147025855A KR 101602594 B1 KR101602594 B1 KR 101602594B1
Authority
KR
South Korea
Prior art keywords
phenol
copper
catalyst
reaction
carbonyl compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020147025855A
Other languages
English (en)
Korean (ko)
Other versions
KR20140131361A (ko
Inventor
타츠오 시라하타
마사히로 하타케야마
코조 야스다
Original Assignee
미쓰이 가가쿠 가부시키가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 미쓰이 가가쿠 가부시키가이샤 filed Critical 미쓰이 가가쿠 가부시키가이샤
Publication of KR20140131361A publication Critical patent/KR20140131361A/ko
Application granted granted Critical
Publication of KR101602594B1 publication Critical patent/KR101602594B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/74Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00Purification; Separation; Stabilisation; Use of additives
    • C07B63/02Purification; Separation; Stabilisation; Use of additives by treatment giving rise to a chemical modification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/685Processes comprising at least two steps in series
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/86Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020147025855A 2012-04-13 2013-04-11 페놀의 정제 방법 Expired - Fee Related KR101602594B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2012091712 2012-04-13
JPJP-P-2012-091712 2012-04-13
PCT/JP2013/060899 WO2013154147A1 (ja) 2012-04-13 2013-04-11 フェノールの精製方法

Publications (2)

Publication Number Publication Date
KR20140131361A KR20140131361A (ko) 2014-11-12
KR101602594B1 true KR101602594B1 (ko) 2016-03-10

Family

ID=49327705

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020147025855A Expired - Fee Related KR101602594B1 (ko) 2012-04-13 2013-04-11 페놀의 정제 방법

Country Status (11)

Country Link
US (1) US9029609B2 (https=)
EP (1) EP2837616B1 (https=)
JP (1) JP5828955B2 (https=)
KR (1) KR101602594B1 (https=)
CN (1) CN104203888B (https=)
ES (1) ES2594554T3 (https=)
IN (1) IN2014DN07933A (https=)
SA (1) SA113340468B1 (https=)
SG (1) SG11201406393UA (https=)
TW (1) TWI549936B (https=)
WO (1) WO2013154147A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180087054A (ko) 2017-01-24 2018-08-01 주식회사 엘지화학 페놀의 정제 방법

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6008802B2 (ja) * 2013-07-11 2016-10-19 三井化学株式会社 フェノールの精製方法
CN105116089B (zh) * 2015-08-24 2017-08-01 山东出入境检验检疫局检验检疫技术中心 塑料及塑料制品中2‑苯基‑2‑丙醇总量的测定方法
CN109790096B (zh) * 2016-11-28 2022-03-15 株式会社Lg化学 甲醇、丙酮去除单元及含该单元的苯酚、双酚a生产系统

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006087943A1 (ja) * 2005-02-21 2006-08-24 Mitsui Chemicals, Inc. フェノール類の精製方法

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2346664A (en) * 1941-07-28 1944-04-18 Koppers Co Inc Surrefining of coal-tar derivatives and the like
US3150191A (en) 1960-02-29 1964-09-22 California Research Corp Phenol color reduction
GB920864A (en) * 1960-08-19 1963-03-13 Distillers Co Yeast Ltd Purification of phenol
US3029293A (en) * 1960-08-19 1962-04-10 Hercules Powder Co Ltd Phenol purification
DE1668952A1 (de) 1968-01-13 1969-11-27 Phenolchemie Gmbh Verfahren zur Gewinnung von Reinphenolen aus Rohphenolen,die bei der Spaltung von Hydroperoxiden alkylaromatischer Kohlenwasserstoffe erhalten worden sind
JPS541289B1 (https=) 1970-12-28 1979-01-23
JPS541289A (en) 1977-06-06 1979-01-08 Nippon Shokubai Kagaku Kogyo Co Ltd Catalyst for purifying exhaust gas
JPS58206619A (ja) 1982-05-26 1983-12-01 Dainippon Ink & Chem Inc 新規ポリウレタン樹脂の製造方法
JP2543074B2 (ja) * 1987-04-09 1996-10-16 三井石油化学工業株式会社 フェノ−ル蒸留残渣からの有用物質の回収方法
JPS63252547A (ja) * 1987-04-09 1988-10-19 Mitsui Petrochem Ind Ltd フエノ−ル蒸留残渣分解用触媒
JP2650497B2 (ja) 1990-01-10 1997-09-03 株式会社日立製作所 試料表面観察装置
JP2636575B2 (ja) 1991-08-07 1997-07-30 三菱電機株式会社 誘雷装置
JPH05286879A (ja) * 1992-04-03 1993-11-02 Mitsui Petrochem Ind Ltd 高純度フェノールの製造方法
US5245090A (en) 1992-09-11 1993-09-14 Aristech Chemical Corporation Two-stage cleavage of cumene hydroperoxide
RU2111203C1 (ru) * 1993-12-01 1998-05-20 Закошанский Владимир Михайлович Способ очистки фенола от органических примесей
JP3711664B2 (ja) 1996-10-31 2005-11-02 石川島播磨重工業株式会社 ステンレス鋼に対するニッケル合金の肉盛溶接方法
US6066767A (en) * 1999-02-10 2000-05-23 Illa International, Llc Method of purifying cumene hydroperoxide decomposition products from hydroxyacetone and from other carbonyls
DE10005770A1 (de) * 2000-02-10 2001-08-16 Bayer Ag Verfahren zur Entfernung von gelöstem Sauerstoff aus Phenol
ES2325981T3 (es) * 2000-09-25 2009-09-28 Exxonmobil Chemical Patents Inc. Hidrogenacion de los efluentes de escision en la produccion de fenol.
JP4212250B2 (ja) 2001-03-12 2009-01-21 三洋電機株式会社 端子装置
RU2217408C2 (ru) 2002-02-08 2003-11-27 Общество с ограниченной ответственностью "Петрофенол" Способ и катализатор очистки фенола
CN100457703C (zh) * 2002-02-08 2009-02-04 沙伯基础创新塑料知识产权有限公司 精制苯酚的方法和催化剂
US6486365B1 (en) * 2002-04-04 2002-11-26 General Electric Company Production and purification of phenol: hydroxyacetone removal by hydrotalcite
US8013191B2 (en) * 2006-07-19 2011-09-06 Illa International, Llc Method for removing impurities from phenol
JP5063702B2 (ja) * 2007-11-13 2012-10-31 三井化学株式会社 アルキル化芳香族化合物の製造方法およびフェノールの製造方法
CN102781897B (zh) * 2010-02-26 2016-03-16 科学与工业研究委员会 羟基丙酮或丙二醇的制备方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006087943A1 (ja) * 2005-02-21 2006-08-24 Mitsui Chemicals, Inc. フェノール類の精製方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180087054A (ko) 2017-01-24 2018-08-01 주식회사 엘지화학 페놀의 정제 방법
US11084771B2 (en) 2017-01-24 2021-08-10 Lg Chem, Ltd. Method for purifying phenol

Also Published As

Publication number Publication date
ES2594554T3 (es) 2016-12-21
JPWO2013154147A1 (ja) 2015-12-17
SG11201406393UA (en) 2014-11-27
TW201345885A (zh) 2013-11-16
CN104203888A (zh) 2014-12-10
CN104203888B (zh) 2016-02-03
KR20140131361A (ko) 2014-11-12
US20150065755A1 (en) 2015-03-05
EP2837616A1 (en) 2015-02-18
EP2837616A4 (en) 2015-12-02
US9029609B2 (en) 2015-05-12
SA113340468B1 (ar) 2015-07-07
IN2014DN07933A (https=) 2015-05-01
JP5828955B2 (ja) 2015-12-09
EP2837616B1 (en) 2016-08-31
WO2013154147A1 (ja) 2013-10-17
TWI549936B (zh) 2016-09-21

Similar Documents

Publication Publication Date Title
KR101602594B1 (ko) 페놀의 정제 방법
KR20120004513A (ko) 1,6-헥산디올 및 카프로락톤을 제조하기 위한 방법
KR20120005018A (ko) 1,6-헥산디올을 제조하기 위한 방법
EP2483232B1 (en) Process for preparing alkanediol and dialkyl carbonate
EP2231571B1 (en) Process for the continuous production of high purity phenolic glycol ether
JP5784742B2 (ja) フェニルシクロヘキサンの製造方法
CN100381415C (zh) 苯酚的制备和精制:通过水滑石除去羟基丙酮
US6388144B1 (en) Method for reducing methylbenzofuran levels in high purity phenol
JP5531101B2 (ja) トリメチロールプロパンの色数を改善する方法
JP6294798B2 (ja) 粗フェノール中のヒドロキシアセトンを低減させる方法、ヒドロキシアセトンが少ない粗フェノールの製造方法および高純度フェノールの製造方法
US20050137429A1 (en) Methods for purification of phenol
CN101128411B (zh) 酚类的精制方法
EP3377467B1 (en) Feed sources for butanediol production processes
JP6008802B2 (ja) フェノールの精製方法
JPH04234334A (ja) 粗フェノールの処理方法およびこれを用いた高純度フェノールの製造方法
JPS6312451B2 (https=)
JPH07215897A (ja) シクロヘキサノール、シクロヘキセン及びフェノール類の併産方法

Legal Events

Date Code Title Description
A201 Request for examination
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

D13-X000 Search requested

St.27 status event code: A-1-2-D10-D13-srh-X000

D14-X000 Search report completed

St.27 status event code: A-1-2-D10-D14-srh-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

FPAY Annual fee payment

Payment date: 20190222

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20200221

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

FPAY Annual fee payment

Payment date: 20210219

Year of fee payment: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

FPAY Annual fee payment

Payment date: 20220225

Year of fee payment: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20250305

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

H13 Ip right lapsed

Free format text: ST27 STATUS EVENT CODE: N-4-6-H10-H13-OTH-PC1903 (AS PROVIDED BY THE NATIONAL OFFICE); TERMINATION CATEGORY : DEFAULT_OF_REGISTRATION_FEE

Effective date: 20250305

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20250305