KR101471651B1 - 복합 산화물 분말의 제조방법 및 복합 산화물 분말 - Google Patents
복합 산화물 분말의 제조방법 및 복합 산화물 분말 Download PDFInfo
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- KR101471651B1 KR101471651B1 KR1020147002618A KR20147002618A KR101471651B1 KR 101471651 B1 KR101471651 B1 KR 101471651B1 KR 1020147002618 A KR1020147002618 A KR 1020147002618A KR 20147002618 A KR20147002618 A KR 20147002618A KR 101471651 B1 KR101471651 B1 KR 101471651B1
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- South Korea
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- powder
- composite oxide
- surface area
- oxide powder
- specific surface
- Prior art date
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- 239000000843 powder Substances 0.000 title claims abstract description 105
- 238000004519 manufacturing process Methods 0.000 title claims description 20
- 239000002131 composite material Substances 0.000 claims abstract description 42
- 238000001354 calcination Methods 0.000 claims abstract description 32
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 229910052788 barium Inorganic materials 0.000 claims abstract description 3
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims description 13
- 150000001875 compounds Chemical class 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 239000013078 crystal Substances 0.000 abstract description 10
- 239000000203 mixture Substances 0.000 description 47
- 238000010304 firing Methods 0.000 description 32
- 239000011575 calcium Substances 0.000 description 30
- 239000000919 ceramic Substances 0.000 description 24
- 230000000052 comparative effect Effects 0.000 description 21
- 238000010438 heat treatment Methods 0.000 description 17
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 15
- 239000000463 material Substances 0.000 description 13
- 239000003985 ceramic capacitor Substances 0.000 description 11
- 229910002113 barium titanate Inorganic materials 0.000 description 9
- 230000003247 decreasing effect Effects 0.000 description 6
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 4
- 239000003989 dielectric material Substances 0.000 description 4
- 239000003990 capacitor Substances 0.000 description 3
- 238000003780 insertion Methods 0.000 description 3
- 230000037431 insertion Effects 0.000 description 3
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000006467 substitution reaction Methods 0.000 description 3
- 229910001928 zirconium oxide Inorganic materials 0.000 description 3
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- AOWKSNWVBZGMTJ-UHFFFAOYSA-N calcium titanate Chemical compound [Ca+2].[O-][Ti]([O-])=O AOWKSNWVBZGMTJ-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000005204 segregation Methods 0.000 description 2
- 238000004438 BET method Methods 0.000 description 1
- 238000003991 Rietveld refinement Methods 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920001887 crystalline plastic Polymers 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/003—Titanates
- C01G23/006—Alkaline earth titanates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
- C04B35/465—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates
- C04B35/468—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates
- C04B35/4682—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates based on BaTiO3 perovskite phase
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62645—Thermal treatment of powders or mixtures thereof other than sintering
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/30—Three-dimensional structures
- C01P2002/34—Three-dimensional structures perovskite-type (ABO3)
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/50—Solid solutions
- C01P2002/52—Solid solutions containing elements as dopants
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5409—Particle size related information expressed by specific surface values
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/76—Crystal structural characteristics, e.g. symmetry
- C04B2235/761—Unit-cell parameters, e.g. lattice constants
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Structural Engineering (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Nanotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JPJP-P-2009-162297 | 2009-07-09 | ||
JP2009162297 | 2009-07-09 | ||
PCT/JP2010/060870 WO2011004722A1 (ja) | 2009-07-09 | 2010-06-25 | 複合酸化物粉末の製造方法および複合酸化物粉末 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020127000093A Division KR20120024927A (ko) | 2009-07-09 | 2010-06-25 | 복합 산화물 분말의 제조방법 및 복합 산화물 분말 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20140021074A KR20140021074A (ko) | 2014-02-19 |
KR101471651B1 true KR101471651B1 (ko) | 2014-12-11 |
Family
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Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
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KR1020127000093A KR20120024927A (ko) | 2009-07-09 | 2010-06-25 | 복합 산화물 분말의 제조방법 및 복합 산화물 분말 |
KR1020147002618A KR101471651B1 (ko) | 2009-07-09 | 2010-06-25 | 복합 산화물 분말의 제조방법 및 복합 산화물 분말 |
Family Applications Before (1)
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KR1020127000093A KR20120024927A (ko) | 2009-07-09 | 2010-06-25 | 복합 산화물 분말의 제조방법 및 복합 산화물 분말 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JP5621774B2 (ja) |
KR (2) | KR20120024927A (ja) |
CN (1) | CN102471084B (ja) |
WO (1) | WO2011004722A1 (ja) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005008471A (ja) * | 2003-06-18 | 2005-01-13 | Murata Mfg Co Ltd | 複合酸化物粉末の製造方法、複合酸化物粉末、誘電体磁器組成物、及び積層型電子部品 |
JP2007180398A (ja) | 2005-12-28 | 2007-07-12 | Tdk Corp | コンデンサの製造方法 |
JP2008133163A (ja) | 2006-11-29 | 2008-06-12 | Kyocera Corp | チタン酸バリウム粉末およびその製法、ならびに誘電体磁器 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS63236760A (ja) * | 1987-03-25 | 1988-10-03 | テイカ株式会社 | チタン酸塩焼結体 |
JPH04303512A (ja) * | 1991-03-29 | 1992-10-27 | Sumitomo Metal Mining Co Ltd | 誘電体磁器用仮焼物の製造方法 |
JP3007732B2 (ja) * | 1991-09-26 | 2000-02-07 | 守 大森 | 窒化ケイ素−混合酸化物系焼結体およびその製造方法 |
JPH0660721A (ja) * | 1992-08-04 | 1994-03-04 | Teika Corp | 誘電体磁器およびその製造方法 |
JP2001110237A (ja) * | 1999-10-12 | 2001-04-20 | Jsr Corp | 強誘電体薄膜形成用塗布液、その製造方法及び強誘電体薄膜 |
JP3780851B2 (ja) * | 2000-03-02 | 2006-05-31 | 株式会社村田製作所 | チタン酸バリウムおよびその製造方法ならびに誘電体セラミックおよびセラミック電子部品 |
CN100491497C (zh) * | 2005-01-12 | 2009-05-27 | 孙家跃 | 一种长余辉黄色荧光体及其制备方法 |
JP2006265067A (ja) * | 2005-03-25 | 2006-10-05 | Kyocera Corp | チタン酸バリウム粉末およびその製法、並びにチタン酸バリウム焼結体 |
CN100386405C (zh) * | 2006-02-28 | 2008-05-07 | 华南理工大学 | 一种红色长余辉发光材料及其制备方法 |
CN1876754A (zh) * | 2006-07-07 | 2006-12-13 | 中山大学 | 一种发400nm蓝紫光InGaN芯片用稀土红色发光荧光粉及其制备方法 |
JP2008127265A (ja) * | 2006-11-24 | 2008-06-05 | Fuji Titan Kogyo Kk | 複合酸化物粉末及びその製造方法、複合酸化物粉末を用いたセラミック組成物並びにそれを用いたセラミック電子部品 |
CN101148587A (zh) * | 2007-10-15 | 2008-03-26 | 山东师范大学 | 硼酸盐红色和绿色荧光体及其制备方法 |
JP2009114034A (ja) * | 2007-11-07 | 2009-05-28 | Tdk Corp | チタン酸バリウムの製造方法 |
-
2010
- 2010-06-25 KR KR1020127000093A patent/KR20120024927A/ko active Application Filing
- 2010-06-25 JP JP2011521886A patent/JP5621774B2/ja active Active
- 2010-06-25 WO PCT/JP2010/060870 patent/WO2011004722A1/ja active Application Filing
- 2010-06-25 CN CN201080028180.4A patent/CN102471084B/zh active Active
- 2010-06-25 KR KR1020147002618A patent/KR101471651B1/ko active IP Right Grant
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005008471A (ja) * | 2003-06-18 | 2005-01-13 | Murata Mfg Co Ltd | 複合酸化物粉末の製造方法、複合酸化物粉末、誘電体磁器組成物、及び積層型電子部品 |
JP2007180398A (ja) | 2005-12-28 | 2007-07-12 | Tdk Corp | コンデンサの製造方法 |
JP2008133163A (ja) | 2006-11-29 | 2008-06-12 | Kyocera Corp | チタン酸バリウム粉末およびその製法、ならびに誘電体磁器 |
Also Published As
Publication number | Publication date |
---|---|
JP5621774B2 (ja) | 2014-11-12 |
CN102471084B (zh) | 2014-08-13 |
WO2011004722A1 (ja) | 2011-01-13 |
KR20140021074A (ko) | 2014-02-19 |
KR20120024927A (ko) | 2012-03-14 |
CN102471084A (zh) | 2012-05-23 |
JPWO2011004722A1 (ja) | 2012-12-20 |
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