KR100955353B1 - 화장료의 제조 방법 - Google Patents
화장료의 제조 방법 Download PDFInfo
- Publication number
- KR100955353B1 KR100955353B1 KR1020097023742A KR20097023742A KR100955353B1 KR 100955353 B1 KR100955353 B1 KR 100955353B1 KR 1020097023742 A KR1020097023742 A KR 1020097023742A KR 20097023742 A KR20097023742 A KR 20097023742A KR 100955353 B1 KR100955353 B1 KR 100955353B1
- Authority
- KR
- South Korea
- Prior art keywords
- acid
- extract
- component
- mass
- tetrakistrimethylsiloxysilane
- Prior art date
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 103
- 238000000034 method Methods 0.000 title claims description 55
- 238000004519 manufacturing process Methods 0.000 claims abstract description 63
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 108
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 99
- 239000000203 mixture Substances 0.000 claims description 48
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 24
- 238000002156 mixing Methods 0.000 claims description 23
- 230000008569 process Effects 0.000 claims description 20
- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 claims description 17
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 16
- 239000003377 acid catalyst Substances 0.000 claims description 14
- 125000004432 carbon atom Chemical group C* 0.000 claims description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 claims description 4
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 claims description 3
- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 claims description 3
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 2
- 229940098779 methanesulfonic acid Drugs 0.000 claims description 2
- ZQZCOBSUOFHDEE-UHFFFAOYSA-N tetrapropyl silicate Chemical compound CCCO[Si](OCCC)(OCCC)OCCC ZQZCOBSUOFHDEE-UHFFFAOYSA-N 0.000 claims description 2
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 1
- -1 is preferable Chemical compound 0.000 description 296
- 229920001296 polysiloxane Polymers 0.000 description 167
- 239000000284 extract Substances 0.000 description 112
- RGMZNZABJYWAEC-UHFFFAOYSA-N Methyltris(trimethylsiloxy)silane Chemical compound C[Si](C)(C)O[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C RGMZNZABJYWAEC-UHFFFAOYSA-N 0.000 description 68
- 229940073663 methyl trimethicone Drugs 0.000 description 67
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- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 19
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- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 16
- 238000002360 preparation method Methods 0.000 description 15
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- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 14
- AFDXODALSZRGIH-UHFFFAOYSA-N p-coumaric acid methyl ether Natural products COC1=CC=C(C=CC(O)=O)C=C1 AFDXODALSZRGIH-UHFFFAOYSA-N 0.000 description 14
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- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 description 12
- 239000004166 Lanolin Substances 0.000 description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 12
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- SGVYKUFIHHTIFL-UHFFFAOYSA-N Isobutylhexyl Natural products CCCCCCCC(C)C SGVYKUFIHHTIFL-UHFFFAOYSA-N 0.000 description 11
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- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 11
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- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 description 9
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
Description
Claims (6)
- 화장료를 제조하는 방법에 있어서,(I) 테트라키스트리메틸실록시실란을, 하기 공정 (1)~(4)를 포함하는 방법에 따라 제조하는 공정,(1) 하기 화학식 (A)로 표시되는 테트라알콕시실란과,(화학식 A)(R은 탄소원자수 1~10의 1가 탄화수소기를 나타낸다)테트라알콕시실란 1몰에 대하여 2~10몰의 하기 화학식 (B)로 표시되는 헥사메틸디실록산과,(화학식 B)테트라알콕시실란 1몰에 대하여 0.01~0.5 몰의 산촉매를 혼합하고 0℃ 이상 30℃ 미만의 온도로 처리하는 공정,(2) 공정 (1)에서 수득된 계에, 공정 (1)에서 사용한 테트라알콕시실란 1몰에 대하여, 1몰의 테트라알콕시실란을 가하는 공정,(3) 온도를 0℃ 이상 30℃ 미만으로 유지하면서 공정 (2)에서 수득된 계에, 물 2.5~10.0 몰을 첨가하고, 30 분간 ~ 5 시간 반응시키는 공정 및(4) 30 ~ 100 ℃의 온도에서 30 분간 ~ 5 시간 반응시키는 공정(II) 공정 (I)에서 수득된 테트라키스트리메틸실록시실란을 화장료에 배합하는 공정을 포함하는 것을 특징으로 하는 방법.
- 제 1 항에 있어서,테트라알콕시실란이 테트라메톡시실란, 테트라에톡시실란, 및 테트라프로폭시실란으로 이루어진 군으로부터 선택되는 1 종류 이상인 것을 특징으로 하는 방법.
- 제 1 항에 있어서,공정 (I)의 공정 (1)에서 테트라알콕시실란 1몰에 대하여 0.5~10 몰의 탄소 원자수가 1~6의 1가 저급 알콜을 추가로 혼합하는 것을 특징으로 하는 방법.
- 제 3 항에 있어서,1가 저급 알콜이 메탄올, 에탄올 및 이소프로판올로 이루어진 군으로부터 선택되는 1 종류 이상인 것을 특징으로 하는 방법.
- 제 1 항에 있어서,산 촉매가 황산, 메탄설폰산 및 트리플루오로메탄설폰산으로 이루어진 군으로부터 선택되는 1 종류 이상인 것을 특징으로 하는 방법.
Applications Claiming Priority (14)
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JPJP-P-2003-074978 | 2003-03-19 | ||
JP2003074978 | 2003-03-19 | ||
JPJP-P-2003-123265 | 2003-04-28 | ||
JP2003123262 | 2003-04-28 | ||
JPJP-P-2003-123263 | 2003-04-28 | ||
JP2003123266 | 2003-04-28 | ||
JP2003123264 | 2003-04-28 | ||
JP2003123263 | 2003-04-28 | ||
JPJP-P-2003-123266 | 2003-04-28 | ||
JP2003123265 | 2003-04-28 | ||
JPJP-P-2003-123262 | 2003-04-28 | ||
JPJP-P-2003-123264 | 2003-04-28 | ||
JPJP-P-2003-177608 | 2003-06-23 | ||
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KR1020057017524A Division KR20050107814A (ko) | 2003-03-19 | 2004-03-18 | 화장료 |
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KR20090123025A KR20090123025A (ko) | 2009-12-01 |
KR100955353B1 true KR100955353B1 (ko) | 2010-04-29 |
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KR1020097023742A KR100955353B1 (ko) | 2003-03-19 | 2004-03-18 | 화장료의 제조 방법 |
KR1020057017524A KR20050107814A (ko) | 2003-03-19 | 2004-03-18 | 화장료 |
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KR1020057017524A KR20050107814A (ko) | 2003-03-19 | 2004-03-18 | 화장료 |
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US (2) | US20060222615A1 (ko) |
EP (1) | EP1607081B1 (ko) |
JP (1) | JP4491549B2 (ko) |
KR (2) | KR100955353B1 (ko) |
WO (1) | WO2004082644A1 (ko) |
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US20040197284A1 (en) | 2003-04-04 | 2004-10-07 | Frederic Auguste | Cosmetic composition comprising a volatile fatty phase |
JP4964253B2 (ja) * | 2006-03-01 | 2012-06-27 | イーエルシー マネージメント エルエルシー | 透明なサンスクリーンジェル及びその使用方法 |
JP5165978B2 (ja) * | 2007-09-20 | 2013-03-21 | 株式会社 資生堂 | 油中水型固形乳化化粧料 |
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AU6734700A (en) * | 1999-08-30 | 2001-03-26 | Kanebo Limited | Cosmetics |
JP4949550B2 (ja) * | 2000-12-11 | 2012-06-13 | 信越化学工業株式会社 | 化粧料 |
US20040197284A1 (en) * | 2003-04-04 | 2004-10-07 | Frederic Auguste | Cosmetic composition comprising a volatile fatty phase |
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2004
- 2004-03-18 WO PCT/JP2004/003623 patent/WO2004082644A1/ja active Search and Examination
- 2004-03-18 JP JP2005503733A patent/JP4491549B2/ja not_active Expired - Fee Related
- 2004-03-18 EP EP04721715A patent/EP1607081B1/en not_active Expired - Fee Related
- 2004-03-18 US US10/549,704 patent/US20060222615A1/en not_active Abandoned
- 2004-03-18 KR KR1020097023742A patent/KR100955353B1/ko active IP Right Grant
- 2004-03-18 KR KR1020057017524A patent/KR20050107814A/ko not_active Application Discontinuation
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WO2000064401A1 (en) * | 1999-04-26 | 2000-11-02 | Revlon Consumer Products Corporation | Color cosmetic compositions containing organic oil and silicone mixture |
Also Published As
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KR20090123025A (ko) | 2009-12-01 |
KR20050107814A (ko) | 2005-11-15 |
JPWO2004082644A1 (ja) | 2006-06-22 |
US20060222615A1 (en) | 2006-10-05 |
JP4491549B2 (ja) | 2010-06-30 |
EP1607081A4 (en) | 2009-05-13 |
EP1607081A1 (en) | 2005-12-21 |
WO2004082644A1 (ja) | 2004-09-30 |
US20100087395A1 (en) | 2010-04-08 |
EP1607081B1 (en) | 2012-02-22 |
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