KR100259401B1 - 우수한 자기특성을 가지는 방향성 규소강판의 제조방법 - Google Patents
우수한 자기특성을 가지는 방향성 규소강판의 제조방법 Download PDFInfo
- Publication number
- KR100259401B1 KR100259401B1 KR1019950033157A KR19950033157A KR100259401B1 KR 100259401 B1 KR100259401 B1 KR 100259401B1 KR 1019950033157 A KR1019950033157 A KR 1019950033157A KR 19950033157 A KR19950033157 A KR 19950033157A KR 100259401 B1 KR100259401 B1 KR 100259401B1
- Authority
- KR
- South Korea
- Prior art keywords
- steel sheet
- weight
- silicon steel
- partial pressure
- grain
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229910000976 Electrical steel Inorganic materials 0.000 title claims abstract description 30
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 238000005261 decarburization Methods 0.000 claims abstract description 47
- 229910000831 Steel Inorganic materials 0.000 claims abstract description 44
- 239000010959 steel Substances 0.000 claims abstract description 44
- 238000000034 method Methods 0.000 claims abstract description 27
- 230000008569 process Effects 0.000 claims abstract description 15
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 10
- 239000001257 hydrogen Substances 0.000 claims abstract description 10
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 8
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 7
- 238000000137 annealing Methods 0.000 claims description 36
- 238000005097 cold rolling Methods 0.000 claims description 32
- 230000009467 reduction Effects 0.000 claims description 15
- 238000005098 hot rolling Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 229910052802 copper Inorganic materials 0.000 claims description 5
- 150000002431 hydrogen Chemical class 0.000 claims description 2
- 238000001953 recrystallisation Methods 0.000 abstract description 45
- 230000001590 oxidative effect Effects 0.000 abstract description 21
- 238000010438 heat treatment Methods 0.000 abstract description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 9
- 230000000630 rising effect Effects 0.000 abstract description 8
- 230000008859 change Effects 0.000 abstract description 2
- 239000011162 core material Substances 0.000 abstract description 2
- 239000003112 inhibitor Substances 0.000 description 17
- 239000000047 product Substances 0.000 description 17
- 239000010949 copper Substances 0.000 description 15
- 239000012467 final product Substances 0.000 description 13
- 230000004907 flux Effects 0.000 description 8
- 239000002994 raw material Substances 0.000 description 7
- 229910052711 selenium Inorganic materials 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 238000005096 rolling process Methods 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000005336 cracking Methods 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 3
- 230000002411 adverse Effects 0.000 description 3
- 229910052787 antimony Inorganic materials 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000006148 magnetic separator Substances 0.000 description 3
- 230000000087 stabilizing effect Effects 0.000 description 3
- 238000004804 winding Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000001680 brushing effect Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 238000010494 dissociation reaction Methods 0.000 description 2
- 230000005593 dissociations Effects 0.000 description 2
- 229960005191 ferric oxide Drugs 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000020169 heat generation Effects 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 238000005554 pickling Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910001224 Grain-oriented electrical steel Inorganic materials 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 229910052840 fayalite Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 229910052839 forsterite Inorganic materials 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 235000013980 iron oxide Nutrition 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 230000005381 magnetic domain Effects 0.000 description 1
- 230000005389 magnetism Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000011218 segmentation Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 238000006557 surface reaction Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D3/00—Diffusion processes for extraction of non-metals; Furnaces therefor
- C21D3/02—Extraction of non-metals
- C21D3/04—Decarburising
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
- C21D8/1244—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
- C21D8/1255—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest with diffusion of elements, e.g. decarburising, nitriding
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/46—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electromagnetism (AREA)
- Manufacturing & Machinery (AREA)
- Manufacturing Of Steel Electrode Plates (AREA)
- Soft Magnetic Materials (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP95-161955 | 1995-06-28 | ||
| JP16195595A JP3463417B2 (ja) | 1994-09-30 | 1995-06-28 | 優れた磁気特性が安定して得られる方向性珪素鋼板の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR970001568A KR970001568A (ko) | 1997-01-24 |
| KR100259401B1 true KR100259401B1 (ko) | 2000-06-15 |
Family
ID=15745243
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019950033157A Expired - Lifetime KR100259401B1 (ko) | 1995-06-28 | 1995-09-29 | 우수한 자기특성을 가지는 방향성 규소강판의 제조방법 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5620533A (enExample) |
| EP (1) | EP0752480B9 (enExample) |
| KR (1) | KR100259401B1 (enExample) |
| CN (1) | CN1061100C (enExample) |
| DE (1) | DE69527778T2 (enExample) |
| TW (1) | TW299354B (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3220362B2 (ja) * | 1995-09-07 | 2001-10-22 | 川崎製鉄株式会社 | 方向性けい素鋼板の製造方法 |
| WO1998046803A1 (en) * | 1997-04-16 | 1998-10-22 | Nippon Steel Corporation | Unidirectional electromagnetic steel sheet having excellent film characteristics and magnetic characteristics, its production method and decarburization annealing setup therefor |
| BRPI1010318B1 (pt) * | 2009-04-06 | 2018-02-06 | Nippon Steel & Sumitomo Metal Corporation | Método de tratamento do aço para chapa de aço elétrico com grão orientado e método de produção de chapa de aço elétrico com grão orientado |
| CN103305745B (zh) * | 2012-03-09 | 2016-04-27 | 宝山钢铁股份有限公司 | 一种高质量硅钢常化基板的生产方法 |
| CN103525999A (zh) * | 2013-09-13 | 2014-01-22 | 任振州 | 一种高磁感取向硅钢片的制备方法 |
| CN110283981B (zh) * | 2019-07-24 | 2020-12-11 | 武汉钢铁有限公司 | 一种能提高低温高磁感取向硅钢氧含量的生产方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63162814A (ja) * | 1986-12-26 | 1988-07-06 | Kawasaki Steel Corp | 鉄損劣化の少ない薄手方向性けい素鋼板の製造方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5250529A (en) | 1975-10-20 | 1977-04-22 | Seiko Instr & Electronics | Silver oxide battery |
| GB1558257A (en) * | 1978-01-09 | 1979-12-19 | Korotkova L F | Method of heat treating magnetic circuit sheets in relativvely high-carbon steel |
| US4200477A (en) * | 1978-03-16 | 1980-04-29 | Allegheny Ludlum Industries, Inc. | Processing for electromagnetic silicon steel |
| US4213804A (en) * | 1979-03-19 | 1980-07-22 | Allegheny Ludlum Industries, Inc. | Processing for cube-on-edge oriented silicon steel |
| EP0225619B1 (en) * | 1985-12-06 | 1994-03-09 | Nippon Steel Corporation | Grain-oriented electrical steel sheet having improved glass film properties and low watt loss and a process for producing same |
| EP0305966B1 (en) * | 1987-08-31 | 1992-11-04 | Nippon Steel Corporation | Method for producing grain-oriented electrical steel sheet having metallic luster and excellent punching property |
| JPH01119622A (ja) * | 1987-10-30 | 1989-05-11 | Nippon Steel Corp | 磁気特性およびグラス皮膜特性に優れた一方向性電磁鋼板の製造方法 |
| DE69121953T2 (de) * | 1990-04-13 | 1997-04-10 | Kawasaki Steel Co | Verfahren zum Herstellen kornorientierter Elektrobleche mit geringen Eisenverlusten |
| JPH0756048B2 (ja) | 1990-11-30 | 1995-06-14 | 川崎製鉄株式会社 | 被膜特性と磁気特性に優れた薄型方向性けい素鋼板の製造方法 |
| JPH04350124A (ja) * | 1991-05-28 | 1992-12-04 | Kawasaki Steel Corp | 薄板厚の一方向性珪素鋼板の製造方法 |
| JP3301629B2 (ja) * | 1992-03-16 | 2002-07-15 | 川崎製鉄株式会社 | 金属光沢を有しかつ磁気特性の優れた方向性けい素鋼板の製造方法 |
-
1995
- 1995-09-26 TW TW084110052A patent/TW299354B/zh not_active IP Right Cessation
- 1995-09-26 US US08/533,841 patent/US5620533A/en not_active Expired - Lifetime
- 1995-09-27 DE DE69527778T patent/DE69527778T2/de not_active Expired - Lifetime
- 1995-09-27 EP EP95115257A patent/EP0752480B9/en not_active Expired - Lifetime
- 1995-09-29 KR KR1019950033157A patent/KR100259401B1/ko not_active Expired - Lifetime
- 1995-09-30 CN CN95118685A patent/CN1061100C/zh not_active Expired - Lifetime
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63162814A (ja) * | 1986-12-26 | 1988-07-06 | Kawasaki Steel Corp | 鉄損劣化の少ない薄手方向性けい素鋼板の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| TW299354B (enExample) | 1997-03-01 |
| KR970001568A (ko) | 1997-01-24 |
| CN1061100C (zh) | 2001-01-24 |
| DE69527778T2 (de) | 2002-12-05 |
| EP0752480A1 (en) | 1997-01-08 |
| EP0752480B9 (en) | 2003-04-09 |
| EP0752480B1 (en) | 2002-08-14 |
| DE69527778D1 (de) | 2002-09-19 |
| US5620533A (en) | 1997-04-15 |
| CN1139154A (zh) | 1997-01-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19950929 |
|
| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 19970825 Comment text: Request for Examination of Application Patent event code: PA02011R01I Patent event date: 19950929 Comment text: Patent Application |
|
| E902 | Notification of reason for refusal | ||
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Comment text: Notification of reason for refusal Patent event date: 19990901 Patent event code: PE09021S01D |
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| E701 | Decision to grant or registration of patent right | ||
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