JPWO2018141746A5 - - Google Patents
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- JPWO2018141746A5 JPWO2018141746A5 JP2019541234A JP2019541234A JPWO2018141746A5 JP WO2018141746 A5 JPWO2018141746 A5 JP WO2018141746A5 JP 2019541234 A JP2019541234 A JP 2019541234A JP 2019541234 A JP2019541234 A JP 2019541234A JP WO2018141746 A5 JPWO2018141746 A5 JP WO2018141746A5
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- curable binder
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- sugar
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- 239000000203 mixture Substances 0.000 claims description 51
- 239000011230 binding agent Substances 0.000 claims description 46
- 239000000463 material Substances 0.000 claims description 25
- SRBFZHDQGSBBOR-SQOUGZDYSA-N Xylose Natural products O[C@@H]1CO[C@@H](O)[C@@H](O)[C@@H]1O SRBFZHDQGSBBOR-SQOUGZDYSA-N 0.000 claims description 16
- 239000001913 cellulose Substances 0.000 claims description 16
- 229920002678 cellulose Polymers 0.000 claims description 16
- 235000000346 sugar Nutrition 0.000 claims description 16
- 150000001720 carbohydrates Chemical class 0.000 claims description 15
- 235000014633 carbohydrates Nutrition 0.000 claims description 15
- 150000004676 glycans Polymers 0.000 claims description 14
- 229920001282 polysaccharide Polymers 0.000 claims description 14
- 239000005017 polysaccharide Substances 0.000 claims description 14
- 150000004804 polysaccharides Polymers 0.000 claims description 14
- 239000000835 fiber Substances 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 12
- 229960003487 Xylose Drugs 0.000 claims description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 8
- WQZGKKKJIJFFOK-VFUOTHLCSA-N β-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 5
- BJHIKXHVCXFQLS-UYFOZJQFSA-N Fructose Natural products OC[C@@H](O)[C@@H](O)[C@H](O)C(=O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 4
- 238000009833 condensation Methods 0.000 claims description 4
- 230000005494 condensation Effects 0.000 claims description 4
- 239000007822 coupling agent Substances 0.000 claims description 4
- 239000008121 dextrose Substances 0.000 claims description 4
- 150000007522 mineralic acids Chemical class 0.000 claims description 4
- 238000006116 polymerization reaction Methods 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000002023 wood Substances 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N D-Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 3
- 239000003365 glass fiber Substances 0.000 claims description 3
- 239000008103 glucose Substances 0.000 claims description 3
- 239000002557 mineral fiber Substances 0.000 claims description 3
- 150000002772 monosaccharides Chemical class 0.000 claims description 3
- -1 sawdust Substances 0.000 claims description 3
- HYRUXGRHTJRKNG-SMBWEDIMSA-N (2S,3R,4R,5R,6R)-2-[(2R,3R,4R,5R,6S)-6-[(2R,3R,4R,5R,6R)-4,5-dihydroxy-2-(hydroxymethyl)-6-methoxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)-5-methoxyoxane-3,4-diol Chemical compound O[C@@H]1[C@@H](O)[C@H](OC)O[C@H](CO)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H](O[C@H]2[C@@H]([C@@H](O)[C@@H](OC)[C@@H](CO)O2)O)[C@@H](CO)O1 HYRUXGRHTJRKNG-SMBWEDIMSA-N 0.000 claims description 2
- GZCGUPFRVQAUEE-KCDKBNATSA-N D-(+)-Galactose Natural products OC[C@@H](O)[C@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-KCDKBNATSA-N 0.000 claims description 2
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 claims description 2
- 239000005715 Fructose Substances 0.000 claims description 2
- 229920000057 Mannan Polymers 0.000 claims description 2
- LUEWUZLMQUOBSB-GFVSVBBRSA-N Mannan Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](O[C@H]3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-GFVSVBBRSA-N 0.000 claims description 2
- 229920001131 Pulp (paper) Polymers 0.000 claims description 2
- 239000000654 additive Substances 0.000 claims description 2
- 150000003863 ammonium salts Chemical class 0.000 claims description 2
- 239000003242 anti bacterial agent Substances 0.000 claims description 2
- 239000003429 antifungal agent Substances 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 230000002209 hydrophobic Effects 0.000 claims description 2
- 239000011236 particulate material Substances 0.000 claims description 2
- 239000004576 sand Substances 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- 239000012209 synthetic fiber Substances 0.000 claims description 2
- 229920002994 synthetic fiber Polymers 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- WQZGKKKJIJFFOK-PHYPRBDBSA-N α-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 claims description 2
- 239000012528 membrane Substances 0.000 claims 2
- 239000011347 resin Substances 0.000 claims 2
- 229920005989 resin Polymers 0.000 claims 2
- 239000010425 asbestos Substances 0.000 claims 1
- 239000011491 glass wool Substances 0.000 claims 1
- 229910052895 riebeckite Inorganic materials 0.000 claims 1
- 235000021309 simple sugar Nutrition 0.000 claims 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000002016 disaccharides Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000011094 fiberboard Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011120 plywood Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Description
本発明の結合剤組成物は、その後に電池用セパレーターにおいて、ルーフィング膜もしくは屋根板などのルーフ製品用の基材または他の膜として応用することができる、不織繊維ベール、例えばガラス繊維ベールを製造するために使用することもできる。 The binder composition of the present invention subsequently comprises a non-woven fiber veil, such as a glass fiber veil, which can be subsequently applied as a base material or other film for roofing products such as roofing films or roofing plates in battery separators. It can also be used for manufacturing.
本発明の結合剤組成物に関する乾燥結合強度は、両組成物とも同じ総糖量を有する、標準的なグルコースをベースとする結合剤組成物と比べて、著しく改善していることがさらに見いだされた。
本発明の好ましい実施形態によれば、例えば、以下が提供される。
(項1)
炭水化物成分およびアンモニアとの無機酸の塩を含む硬化性結合剤組成物であって、前記炭水化物成分が、少なくとも部分的にデキストロースおよびキシロースを含む単糖、二糖ならびに多糖を含むセルロース加水分解物の糖である、硬化性結合剤組成物。
(項2)
前記セルロース加水分解物の糖が、前記糖成分の10~100重量%を構成する、上記項1に記載の硬化性結合剤組成物。
(項3)
前記組成物が水性であり、全水性結合剤組成物の重量に基づき、5~95重量%、好ましくは8~90重量%、より好ましくは10~85重量%の、より詳細には、全水性結合剤組成物の重量に基づき、5~25重量%、好ましくは8~20重量%、より好ましくは10~20重量%、もしくはさらには12~18重量%の範囲の、または全水性結合剤組成物の重量に基づき、50~95重量%、好ましくは50~90重量%、より好ましくは55~85重量%、もしくはさらには60~80重量%の範囲の固形分を含む、上記項1または2に記載の硬化性結合剤組成物。
(項4)
前記炭水化物成分が、1~95重量%のグルコースおよび0.5~15重量%のキシロース、好ましくは1~10重量%のキシロースを含み、その残りが、フルクトース、マンノース、ガラクトースおよび/または多糖フラクションである、前記上記項のいずれかに記載の硬化性結合剤組成物。
(項5)
前記多糖フラクションが、アラビナン、ガラクタンおよび/またはマンナンを含む、上記項4に記載の硬化性結合剤組成物。
(項6)
前記多糖の含有量が、1~90重量%の間、好ましくは3~20重量%の間、または3~15重量%の間、または3~10重量%の間で変動する、上記項5に記載の硬化性結合剤組成物。
(項7)
前記多糖フラクションが、2~20、好ましくは2~15で変動する、異なる重合度の多糖のブレンドであり、平均重合度が、3~7の間、好ましくは3~5の間を含む、上記項4から6のいずれかに記載の硬化性結合剤組成物。
(項8)
当技術分野で公知のカップリング剤、染料、抗真菌剤、抗細菌剤、疎水物質および他の添加剤をさらに含む、前記上記項のいずれかに記載の硬化性結合剤組成物。
(項9)
ケイ素含有カップリング剤を、前記結合剤組成物中、固形分の重量に基づき、好ましくは約0.1~約1重量%の範囲で含む、上記項8に記載の硬化性結合剤組成物。
(項10)
上記項1から9のいずれかに記載の硬化性結合剤組成物によって、および/または上記項1から9のいずれかに記載の前記硬化性結合剤組成物の前記炭水化物成分と無機アンモニア塩との縮合から得られる反応生成物、または上記項1から9のいずれかに記載の水性硬化性結合剤組成物を硬化条件に供することにより得られた結合剤によって、一緒に結合された鉱物繊維、合成繊維または天然繊維、セルロース粒子もしくはシート材料を含む、物質のアセンブリ。
(項11)
繊維マットに組織化されて断熱製品に加工されるように一緒に結合された、例えばガラスウールまたは石綿に基づき70~99重量%の範囲の量で鉱物繊維を含む断熱製品である、上記項10に記載の物質のアセンブリ。
(項12)
電池用セパレーターにおいての、ルーフィング膜もしくは屋根板などのルーフ製品用の基材または他の膜としての使用のための、不織繊維ベール、例えばガラス繊維ベールである、上記項10に記載の物質のアセンブリ。
(項13)
結合粒子、例えば、砂粒子もしくはセルロース粒子、例えば、セルロース系繊維、おが屑、木材層もしくはシート、木材パルプ、およびファイバーボード、パーティクルボード、配向性ストランドボードもしくは合板を含む複合木材ボードを製造するために一般に使用される他の材料であり、結合剤含有量が、前記アセンブリの総重量に基づき、約5~30重量%、特に9~20重量%の範囲である、上記項10に記載の物質のアセンブリ。
(項14)
上記項10から13のいずれかに記載の物質のアセンブリの調製方法であって、(i)(a)少なくとも部分的にセルロース加水分解物の糖である炭水化物成分を提供するステップ、(ii)適量の(b)無機アンモニウム塩を提供するステップ、(iii)粒子状物、繊維状もしくはセルロース系粒子状材料、またはシート材料上に、(b)により架橋された(a)であり得る、(a)および(b)を含む水性組成物として、(a)および(b)を逐次的または同時に付与して、樹脂加工材料を生成するステップ、ならびに(v)得られた樹脂加工材料を硬化条件に供して、過剰な水を蒸発させるステップを含む、方法。
(項15)
硬化が、90~200℃の範囲、好ましくは140℃超、より好ましくは190℃未満、通常、160~180℃の間の温度で行われる、上記項14に記載の方法。
(項16)
炭水化物成分およびアンモニアとの無機酸の塩を含む硬化性結合剤組成物中の糖成分としてのセルロース加水分解物の糖の使用であって、前記硬化性結合剤組成物によって、ならびに/または前記硬化性結合剤組成物の前記炭水化物成分と無機アンモニア塩との縮合および/もしくは硬化から得られる反応生成物によって、一緒に結合された鉱物繊維、合成繊維もしくは天然繊維、セルロース粒子、またはシート材料を含む物質のアセンブリの乾燥および/または湿潤強度を改善するための、使用。
It was further found that the dry binding strength of the binder compositions of the present invention was significantly improved compared to standard glucose-based binder compositions having the same total sugar content in both compositions. rice field.
According to a preferred embodiment of the invention, for example, the following are provided.
(Item 1)
A curable binder composition comprising a carbohydrate component and a salt of an inorganic acid with ammonia, wherein the carbohydrate component is a cellulose hydrolyzate containing at least partially dextrose and xylose-containing monosaccharides, disaccharides and polysaccharides. A curable binder composition that is a sugar.
(Item 2)
Item 2. The curable binder composition according to Item 1, wherein the sugar of the cellulose hydrolyzate constitutes 10 to 100% by weight of the sugar component.
(Item 3)
The composition is aqueous, 5 to 95% by weight, preferably 8 to 90% by weight, more preferably 10 to 85% by weight, more particularly totally aqueous, based on the weight of the total aqueous binder composition. Based on the weight of the binder composition, the composition is in the range of 5-25% by weight, preferably 8-20% by weight, more preferably 10-20% by weight, or even 12-18% by weight, or the total aqueous binder composition. Item 1 or 2 above, which comprises a solid content in the range of 50-95% by weight, preferably 50-90% by weight, more preferably 55-85% by weight, or even 60-80% by weight, based on the weight of the object. The curable binder composition according to.
(Item 4)
The carbohydrate component comprises 1-95% by weight glucose and 0.5-15% by weight xylose, preferably 1-10% by weight xylose, the rest of which is fructose, mannose, galactose and / or polysaccharide fraction. The curable binder composition according to any one of the above items.
(Item 5)
Item 4. The curable binder composition according to Item 4, wherein the polysaccharide fraction comprises arabinane, galactan and / or mannan.
(Item 6)
Item 5 above, wherein the content of the polysaccharide varies between 1 and 90% by weight, preferably between 3 and 20% by weight, or between 3 and 15% by weight, or between 3 and 10% by weight. The curable binder composition according to the above.
(Item 7)
The polysaccharide fraction is a blend of polysaccharides having different degrees of polymerization, varying from 2 to 20, preferably from 2 to 15, with an average degree of polymerization of between 3 and 7, preferably between 3 and 5. Item 6. The curable binder composition according to any one of Items 4 to 6.
(Item 8)
The curable binder composition according to any one of the above items, further comprising a coupling agent, a dye, an antifungal agent, an antibacterial agent, a hydrophobic substance and other additives known in the art.
(Item 9)
Item 2. The curable binder composition according to Item 8, wherein the silicon-containing coupling agent is contained in the binder composition in the range of preferably about 0.1 to about 1% by weight based on the weight of the solid content.
(Item 10)
By the curable binder composition according to any one of Items 1 to 9 and / or the carbohydrate component of the curable binder composition according to any one of Items 1 to 9 and an inorganic ammonia salt. Synthetic fibers bonded together by a reaction product obtained from condensation or a binder obtained by subjecting the aqueous curable binder composition according to any one of Items 1 to 9 to curing conditions. Assembly of materials, including fibers or natural fibers, cellulose particles or sheet materials.
(Item 11)
Item 10. Assembly of materials described in.
(Item 12)
Item 10. The material according to item 10 above, which is a non-woven fiber veil, for example a glass fiber veil, for use as a substrate or other film for roofing products such as roofing films or roofing plates in battery separators. assembly.
(Item 13)
To produce composite wood boards including bound particles such as sand or cellulosic particles such as cellulosic fibers, shavings, wood layers or sheets, wood pulp, and fiberboard, particle board, oriented strand board or plywood. Item 2. The material according to item 10 above, which is another commonly used material and has a binder content in the range of about 5-30% by weight, particularly 9-20% by weight, based on the total weight of the assembly. assembly.
(Item 14)
Item 4. The method for preparing an assembly of a substance according to any one of Items 10 to 13, wherein (i) (a) a step of providing a carbohydrate component which is a sugar of a cellulose hydrolyzate at least partially, (ii) an appropriate amount. (B) The step of providing the inorganic ammonium salt, (iii) may be (a) crosslinked by (b) on a particulate, fibrous or cellulosic particulate material, or sheet material. ) And (b) as an aqueous composition containing (a) and (b) sequentially or simultaneously to produce a resin-processed material, and (v) the obtained resin-processed material as curing conditions. A method comprising the steps of providing and evaporating excess water.
(Item 15)
Item 12. The method according to Item 14, wherein the curing is carried out at a temperature in the range of 90 to 200 ° C., preferably more than 140 ° C., more preferably less than 190 ° C., usually between 160 and 180 ° C.
(Item 16)
Use of cellulose hydrolyzate sugar as a sugar component in a curable binder composition comprising a carbohydrate component and a salt of an inorganic acid with ammonia, by and / or said cure. Includes mineral fibers, synthetic or natural fibers, cellulose particles, or sheet materials bonded together by the reaction product obtained from the condensation and / or curing of the carbohydrate component of the sex binder composition with an inorganic ammonia salt. Use to improve the drying and / or wet strength of material assemblies.
Claims (18)
(a)電池用セパレーターにおいて、
(b)ルーフィング膜もしくは屋根板などのルーフ製品用の基材として、または
(c)他の膜として
の使用のためのものである、物質のアセンブリ。 The assembly of the material of claim 10, which is a non-woven fiber veil, eg, a glass fiber veil, wherein the non-woven fiber veil is:
(A) In the battery separator
(B) As a base material for roofing products such as roofing membranes or roofing boards , or
(C) As another membrane
Assembly of material , which is for use in.
前記硬化性結合剤組成物によって、ならびに/または前記硬化性結合剤組成物の前記炭水化物成分と無機アンモニア塩との縮合および/もしくは硬化から得られる反応生成物によって、一緒に結合された鉱物繊維、合成繊維もしくは天然繊維、セルロース粒子、またはシート材料を含む物質のアセンブリの乾燥および/または湿潤強度を改善するための、使用。 The use of the sugar of a cellulose hydrolyzate as a sugar component in a curable binder composition comprising a carbohydrate component and a salt of an inorganic acid with ammonia , wherein the sugar of the cellulose hydrolyzate is dextrose and. Contains monosaccharides, including xylose, as well as polysaccharides,
Mineral fibers bonded together by the curable binder composition and / or by the reaction product obtained from the condensation and / or curing of the carbohydrate component of the curable binder composition with an inorganic ammonia salt. Use to improve the drying and / or wet strength of an assembly of materials containing synthetic or natural fibers, cellulose particles, or sheet materials.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1701569.4 | 2017-01-31 | ||
GBGB1701569.4A GB201701569D0 (en) | 2017-01-31 | 2017-01-31 | Improved binder compositions and uses thereof |
PCT/EP2018/052279 WO2018141746A1 (en) | 2017-01-31 | 2018-01-30 | Improved binder compositions and uses thereof |
Publications (3)
Publication Number | Publication Date |
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JP2020507643A JP2020507643A (en) | 2020-03-12 |
JPWO2018141746A5 true JPWO2018141746A5 (en) | 2022-01-26 |
JP7175902B2 JP7175902B2 (en) | 2022-11-21 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP2019541234A Active JP7175902B2 (en) | 2017-01-31 | 2018-01-30 | Improved binder composition and use thereof |
Country Status (14)
Country | Link |
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US (1) | US11248108B2 (en) |
EP (1) | EP3577266B1 (en) |
JP (1) | JP7175902B2 (en) |
KR (1) | KR102486678B1 (en) |
CN (1) | CN110249087B (en) |
AU (1) | AU2018216930B2 (en) |
BR (1) | BR112019015675A2 (en) |
CA (1) | CA3051505A1 (en) |
DK (1) | DK3577266T3 (en) |
ES (1) | ES2900226T3 (en) |
GB (1) | GB201701569D0 (en) |
PL (1) | PL3577266T3 (en) |
RU (1) | RU2760121C2 (en) |
WO (1) | WO2018141746A1 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
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GB201701569D0 (en) * | 2017-01-31 | 2017-03-15 | Knauf Insulation Ltd | Improved binder compositions and uses thereof |
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