JPS61225217A - ポリフエニレンサルフアイド樹脂からの不純物の除去方法 - Google Patents
ポリフエニレンサルフアイド樹脂からの不純物の除去方法Info
- Publication number
- JPS61225217A JPS61225217A JP60066897A JP6689785A JPS61225217A JP S61225217 A JPS61225217 A JP S61225217A JP 60066897 A JP60066897 A JP 60066897A JP 6689785 A JP6689785 A JP 6689785A JP S61225217 A JPS61225217 A JP S61225217A
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- pps
- polyphenylene sulfide
- sulfide resin
- glycerin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004734 Polyphenylene sulfide Substances 0.000 title claims abstract description 35
- 229920000069 polyphenylene sulfide Polymers 0.000 title claims abstract description 35
- 239000012535 impurity Substances 0.000 title claims abstract description 23
- 239000011347 resin Substances 0.000 title claims abstract description 18
- 229920005989 resin Polymers 0.000 title claims abstract description 18
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 48
- 239000002904 solvent Substances 0.000 claims abstract description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 27
- 235000011187 glycerol Nutrition 0.000 claims abstract description 24
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000012046 mixed solvent Substances 0.000 claims abstract description 16
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims abstract description 9
- 238000005406 washing Methods 0.000 claims abstract description 8
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000001816 cooling Methods 0.000 claims abstract description 6
- YJTKZCDBKVTVBY-UHFFFAOYSA-N 1,3-Diphenylbenzene Chemical group C1=CC=CC=C1C1=CC=CC(C=2C=CC=CC=2)=C1 YJTKZCDBKVTVBY-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 235000010290 biphenyl Nutrition 0.000 claims abstract description 3
- 239000004305 biphenyl Substances 0.000 claims abstract description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 150000002790 naphthalenes Chemical class 0.000 claims description 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract description 10
- 239000011780 sodium chloride Substances 0.000 abstract description 8
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 abstract description 6
- 239000002002 slurry Substances 0.000 abstract description 4
- 125000001475 halogen functional group Chemical group 0.000 abstract 1
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 15
- 239000012065 filter cake Substances 0.000 description 15
- 238000003756 stirring Methods 0.000 description 13
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 12
- 239000012153 distilled water Substances 0.000 description 11
- 235000002639 sodium chloride Nutrition 0.000 description 11
- 238000011282 treatment Methods 0.000 description 11
- 239000000203 mixture Substances 0.000 description 8
- JTPNRXUCIXHOKM-UHFFFAOYSA-N 1-chloronaphthalene Chemical compound C1=CC=C2C(Cl)=CC=CC2=C1 JTPNRXUCIXHOKM-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000002245 particle Substances 0.000 description 5
- 235000019445 benzyl alcohol Nutrition 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000008096 xylene Substances 0.000 description 2
- DLKQHBOKULLWDQ-UHFFFAOYSA-N 1-bromonaphthalene Chemical compound C1=CC=C2C(Br)=CC=CC2=C1 DLKQHBOKULLWDQ-UHFFFAOYSA-N 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 101100074988 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) nmp-1 gene Proteins 0.000 description 1
- 239000005456 alcohol based solvent Substances 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 238000004380 ashing Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 229910052979 sodium sulfide Inorganic materials 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Structures Or Materials For Encapsulating Or Coating Semiconductor Devices Or Solid State Devices (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60066897A JPS61225217A (ja) | 1985-03-29 | 1985-03-29 | ポリフエニレンサルフアイド樹脂からの不純物の除去方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60066897A JPS61225217A (ja) | 1985-03-29 | 1985-03-29 | ポリフエニレンサルフアイド樹脂からの不純物の除去方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61225217A true JPS61225217A (ja) | 1986-10-07 |
| JPH036170B2 JPH036170B2 (enrdf_load_stackoverflow) | 1991-01-29 |
Family
ID=13329175
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60066897A Granted JPS61225217A (ja) | 1985-03-29 | 1985-03-29 | ポリフエニレンサルフアイド樹脂からの不純物の除去方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61225217A (enrdf_load_stackoverflow) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61228023A (ja) * | 1985-04-01 | 1986-10-11 | Kureha Chem Ind Co Ltd | ポリアリ−レンスルフィドの精製法 |
| WO1987005915A1 (en) * | 1986-03-24 | 1987-10-08 | Tohpren Co., Ltd. | Process for removing impurities from polyphenylene sulfide resin |
| JPH02163125A (ja) * | 1988-12-16 | 1990-06-22 | Toray Philips Petorooriamu Kk | ポリアリーレンスルフィドの製造方法 |
| US5128445A (en) * | 1990-06-14 | 1992-07-07 | Phillips Petroleum Company | Method to recover poly(arylene sulfide) polymers with water-polar organic compound |
| US5143554A (en) * | 1989-08-28 | 1992-09-01 | Idemitsu Petrochemical Company Limited | Process for washing powdery and/or granular resins and a washing device therefor |
| WO2007114056A1 (ja) | 2006-03-30 | 2007-10-11 | Asahi Kasei Chemicals Corporation | 樹脂組成物およびその成形品 |
| WO2008102851A1 (ja) | 2007-02-21 | 2008-08-28 | Asahi Kasei E-Materials Corporation | 高分子電解質組成物、高分子電解質膜、膜電極接合体、及び固体高分子電解質型燃料電池 |
| WO2009110480A1 (ja) | 2008-03-03 | 2009-09-11 | 旭化成ケミカルズ株式会社 | 難燃性樹脂組成物 |
| WO2013042746A1 (ja) | 2011-09-21 | 2013-03-28 | 東レ株式会社 | 高分子電解質組成物成形体、およびそれを用いた固体高分子型燃料電池 |
| WO2013100087A1 (ja) | 2011-12-28 | 2013-07-04 | 旭化成イーマテリアルズ株式会社 | レドックスフロー二次電池及びレドックスフロー二次電池用電解質膜 |
| WO2013100082A1 (ja) | 2011-12-28 | 2013-07-04 | 旭化成イーマテリアルズ株式会社 | レドックスフロー二次電池及びレドックスフロー二次電池用電解質膜 |
| US8993670B2 (en) | 2006-02-27 | 2015-03-31 | Asahi Kasei Chemicals Corporation | Glass-fiber reinforced thermoplastic resin composition and molded article thereof |
| DE112017007529T5 (de) | 2017-05-11 | 2020-01-23 | Asahi Kasei Kabushiki Kaisha | Polymerelektrolytmembran, Membran-Elektroden-Baugruppe und Brennstoffzelle mit festem Polymerelektrolyt |
| CN113680128A (zh) * | 2021-07-27 | 2021-11-23 | 山东明化新材料有限公司 | 一种聚芳硫醚树脂的连续洗涤净化系统及净化方法 |
| WO2023013650A1 (ja) | 2021-08-05 | 2023-02-09 | 旭化成株式会社 | アンテナ部材 |
-
1985
- 1985-03-29 JP JP60066897A patent/JPS61225217A/ja active Granted
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61228023A (ja) * | 1985-04-01 | 1986-10-11 | Kureha Chem Ind Co Ltd | ポリアリ−レンスルフィドの精製法 |
| WO1987005915A1 (en) * | 1986-03-24 | 1987-10-08 | Tohpren Co., Ltd. | Process for removing impurities from polyphenylene sulfide resin |
| JPH02163125A (ja) * | 1988-12-16 | 1990-06-22 | Toray Philips Petorooriamu Kk | ポリアリーレンスルフィドの製造方法 |
| US5143554A (en) * | 1989-08-28 | 1992-09-01 | Idemitsu Petrochemical Company Limited | Process for washing powdery and/or granular resins and a washing device therefor |
| US5128445A (en) * | 1990-06-14 | 1992-07-07 | Phillips Petroleum Company | Method to recover poly(arylene sulfide) polymers with water-polar organic compound |
| US8993670B2 (en) | 2006-02-27 | 2015-03-31 | Asahi Kasei Chemicals Corporation | Glass-fiber reinforced thermoplastic resin composition and molded article thereof |
| WO2007114056A1 (ja) | 2006-03-30 | 2007-10-11 | Asahi Kasei Chemicals Corporation | 樹脂組成物およびその成形品 |
| US8658731B2 (en) | 2006-03-30 | 2014-02-25 | Asahi Kasei Chemicals Corporation | Resin composition and molded product thereof |
| US8487035B2 (en) | 2006-03-30 | 2013-07-16 | Asahi Kasei Chemicals Corporation | Resin composition and molded product thereof |
| WO2008102851A1 (ja) | 2007-02-21 | 2008-08-28 | Asahi Kasei E-Materials Corporation | 高分子電解質組成物、高分子電解質膜、膜電極接合体、及び固体高分子電解質型燃料電池 |
| US8304134B2 (en) | 2007-02-21 | 2012-11-06 | Asahi Kasei E-Materials Corporation | Polymer electrolyte composition, polymer electrolyte membrane, membrane electrode assembly and solid polymer electrolyte-based fuel cell |
| WO2009110480A1 (ja) | 2008-03-03 | 2009-09-11 | 旭化成ケミカルズ株式会社 | 難燃性樹脂組成物 |
| WO2013042746A1 (ja) | 2011-09-21 | 2013-03-28 | 東レ株式会社 | 高分子電解質組成物成形体、およびそれを用いた固体高分子型燃料電池 |
| WO2013100087A1 (ja) | 2011-12-28 | 2013-07-04 | 旭化成イーマテリアルズ株式会社 | レドックスフロー二次電池及びレドックスフロー二次電池用電解質膜 |
| WO2013100082A1 (ja) | 2011-12-28 | 2013-07-04 | 旭化成イーマテリアルズ株式会社 | レドックスフロー二次電池及びレドックスフロー二次電池用電解質膜 |
| EP3091600A1 (en) | 2011-12-28 | 2016-11-09 | Asahi Kasei Kabushiki Kaisha | Redox flow secondary battery and electrolyte membrane for redox flow secondary batteries |
| EP3091598A1 (en) | 2011-12-28 | 2016-11-09 | Asahi Kasei Kabushiki Kaisha | Redox flow secondary battery and electrolyte membrane for redox flow secondary batteries |
| EP3091599A1 (en) | 2011-12-28 | 2016-11-09 | Asahi Kasei Kabushiki Kaisha | Redox flow secondary battery and electrolyte membrane for redox flow secondary batteries |
| DE112017007529T5 (de) | 2017-05-11 | 2020-01-23 | Asahi Kasei Kabushiki Kaisha | Polymerelektrolytmembran, Membran-Elektroden-Baugruppe und Brennstoffzelle mit festem Polymerelektrolyt |
| CN113680128A (zh) * | 2021-07-27 | 2021-11-23 | 山东明化新材料有限公司 | 一种聚芳硫醚树脂的连续洗涤净化系统及净化方法 |
| WO2023013650A1 (ja) | 2021-08-05 | 2023-02-09 | 旭化成株式会社 | アンテナ部材 |
| US12057627B1 (en) | 2021-08-05 | 2024-08-06 | Asahi Kasei Kabushiki Kaisha | Antenna member |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH036170B2 (enrdf_load_stackoverflow) | 1991-01-29 |
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