JP6741687B2 - メロナールの調製方法 - Google Patents
メロナールの調製方法 Download PDFInfo
- Publication number
- JP6741687B2 JP6741687B2 JP2017557332A JP2017557332A JP6741687B2 JP 6741687 B2 JP6741687 B2 JP 6741687B2 JP 2017557332 A JP2017557332 A JP 2017557332A JP 2017557332 A JP2017557332 A JP 2017557332A JP 6741687 B2 JP6741687 B2 JP 6741687B2
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- JP
- Japan
- Prior art keywords
- formula
- compound
- tin
- weight
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- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/54—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of compounds containing doubly bound oxygen atoms, e.g. esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/39—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP15166260.8 | 2015-05-04 | ||
| EP15166260 | 2015-05-04 | ||
| PCT/EP2016/060062 WO2016177814A1 (en) | 2015-05-04 | 2016-05-04 | Process for the preparation of melonal |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2018518467A JP2018518467A (ja) | 2018-07-12 |
| JP2018518467A5 JP2018518467A5 (https=) | 2019-06-06 |
| JP6741687B2 true JP6741687B2 (ja) | 2020-08-19 |
Family
ID=53040424
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017557332A Active JP6741687B2 (ja) | 2015-05-04 | 2016-05-04 | メロナールの調製方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10202324B2 (https=) |
| EP (1) | EP3292099B1 (https=) |
| JP (1) | JP6741687B2 (https=) |
| CN (1) | CN107735392B (https=) |
| ES (1) | ES2821890T3 (https=) |
| MX (1) | MX2017014148A (https=) |
| WO (1) | WO2016177814A1 (https=) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016177814A1 (en) | 2015-05-04 | 2016-11-10 | Basf Se | Process for the preparation of melonal |
| RU2732326C2 (ru) | 2015-07-22 | 2020-09-15 | Басф Се | Способ получения фуран-2,5-дикарбоновой кислоты |
| EP3170828A1 (de) * | 2015-11-23 | 2017-05-24 | Basf Se | Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten |
| US10737239B2 (en) | 2015-11-27 | 2020-08-11 | Basf Se | Ultrafast high space-time-yield synthesis of metal-organic frameworks |
| EP3178788A1 (en) | 2015-12-08 | 2017-06-14 | Basf Se | A tin-containing zeolitic material having a bea framework structure |
| US10737944B2 (en) | 2015-12-08 | 2020-08-11 | Basf Se | Tin-containing zeolitic material having a BEA framework structure |
| EP3411357A1 (de) | 2016-02-01 | 2018-12-12 | Basf Se | Verfahren zur herstellung von c4-c15-lactamen |
| MX380770B (es) | 2016-02-19 | 2025-03-12 | Basf Se | Ciclación enzimática de ácido homofarnesílico. |
| MX2018014918A (es) | 2016-05-31 | 2019-09-05 | Basf Se | Esteres de tetrahidropiranilalquilo inferior y su produccion usando un compuesto de ceteno. |
| CN109311789B (zh) | 2016-06-07 | 2023-04-04 | 巴斯夫欧洲公司 | 制备2,3-不饱和醇的方法 |
| JP7039498B2 (ja) | 2016-06-29 | 2022-03-22 | ビーエーエスエフ ソシエタス・ヨーロピア | 液相の存在下でのアルコールの酸化によるアルファ,ベータ不飽和アルデヒドの製造方法 |
| CN109415311B (zh) | 2016-07-08 | 2021-07-23 | 巴斯夫欧洲公司 | 制备有机砜的方法 |
| SG11201811020XA (en) | 2016-07-20 | 2019-02-27 | Basf Se | A process for purifying propylene oxide |
| BR112019001675A2 (pt) | 2016-07-29 | 2019-05-14 | Basf Corporation | processos para a preparação de um material zeolítico, para a preparação de um substrato revestido e para a preparação de um corpo moldado, material zeolítico, método para a redução e utilização de um material zeolítico |
| WO2018096171A1 (en) | 2016-11-28 | 2018-05-31 | Basf Se | Catalyst composite comprising an alkaline earth metal containing cha zeolite and use thereof in a process for the conversion of oxygenates to olefins |
| JP2019536774A (ja) | 2016-11-30 | 2019-12-19 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | Mor骨格構造の銅変性ゼオライトを用いて、モノエタノールアミンをエチレンジアミンに変換する方法 |
| EP3568387B1 (en) | 2016-11-30 | 2021-05-05 | Basf Se | Process for the conversion of ethylene glycol to ethylenediamine employing a zeolite catalyst |
| KR102530741B1 (ko) | 2016-12-13 | 2023-05-09 | 바스프 에스이 | 티탄-함유 제올라이트의 제조 방법 |
| EP3601206B1 (de) | 2017-03-21 | 2021-07-21 | Basf Se | Verfahren zur herstellung einer korrosionsschutzkomponente für ein gefrierschutzmittel |
| WO2018202765A1 (en) | 2017-05-03 | 2018-11-08 | Basf Se | Process for the conversion of ethylene oxide to monoethanolamine and ethylenediamine employing a zeolite |
| MX2020006560A (es) * | 2017-12-21 | 2020-09-24 | Basf Se | Proceso para la preparacion de aldehidos alfa-beta insaturados mediante oxidacion de alcoholes en presencia de una fase liquida. |
| CN114292170B (zh) * | 2022-01-11 | 2023-01-13 | 万华化学集团股份有限公司 | 一种合成甜瓜醛的方法 |
Family Cites Families (89)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140047837A1 (en) | 2012-08-17 | 2014-02-20 | Basf Se | Method of improving nitrite salt compositions for use as heat transfer medium or heat storage medium |
| ES2641843T3 (es) * | 2012-11-05 | 2017-11-14 | Basf Se | Procedimiento de oxidación de compuestos orgánicos de carbonilo |
| CA2896186A1 (en) | 2013-01-25 | 2014-07-31 | Wintershall Holding GmbH | Method for recovering oil |
| KR20160004281A (ko) | 2013-05-06 | 2016-01-12 | 바스프 에스이 | 미세구조화 반응기에서 니트로알칸을 제조하는 방법 |
| CA2899743A1 (en) | 2013-05-23 | 2014-11-27 | Wintershall Holding GmbH | A method of transporting oil |
| US20160122296A1 (en) | 2013-05-29 | 2016-05-05 | Basf Se | Process for the oxidation of sulfoxides |
| US20140357718A1 (en) | 2013-06-03 | 2014-12-04 | Basf Se | Compositions for use in controlling intestinal microflora |
| WO2014199348A2 (en) | 2013-06-13 | 2014-12-18 | Basf Se | Metal doped silicate catalysts for the selective conversion of ethanol to butadiene |
| WO2014199349A2 (en) | 2013-06-13 | 2014-12-18 | Basf Se | Metal impregnated amorphous silicates for the selective conversion of ethanol to butadiene |
| WO2014198901A1 (en) | 2013-06-13 | 2014-12-18 | Basf Se | Process for the preparation of butadiene |
| CN105358517B (zh) | 2013-07-02 | 2017-11-17 | 巴斯夫欧洲公司 | 通过2,3,6‑三甲基苯酚的氧化制备2,3,5‑三甲基苯醌的方法 |
| CA2916886A1 (en) | 2013-07-02 | 2015-01-08 | Basf Se | Process for the preparation of 3-heptanol from a mixture comprising 2-ethylhexanal and 3-heptyl formate |
| CN105556728B (zh) | 2013-07-23 | 2020-06-02 | 国轩高科美国研究院 | 作为锂离子电池中电解质的添加剂的环氧乙烷基衍生物 |
| EP3025388B1 (en) | 2013-07-23 | 2018-01-31 | Gotion, Inc. | Oxiranyl derivatives as additives for electrolytes in lithium-ion batteries |
| MX2016001029A (es) | 2013-07-24 | 2016-09-08 | Basf Se | Un proceso para preparar óxido de propileno. |
| HUE065342T2 (hu) | 2013-07-24 | 2024-05-28 | Basf Se | Titántartalmú zeolit regenerálása |
| EP3024580B1 (en) | 2013-07-24 | 2018-06-13 | Basf Se | A process for the preparation of propylene oxide |
| MY174118A (en) | 2013-07-24 | 2020-03-10 | Basf Se | A process for preparing propylene oxide |
| WO2015018676A1 (de) | 2013-08-06 | 2015-02-12 | Basf Se | Verfahren zur herstellung von trisaziridinomethan |
| WO2015018815A1 (en) | 2013-08-09 | 2015-02-12 | Basf Se | Process for the oxygen free conversion of methane to ethylene on zeolite catalysts |
| WO2015018807A2 (en) | 2013-08-09 | 2015-02-12 | Basf Se | Process for the oxygen free conversion of methane to ethylene on zeolite catalysts |
| CN105636669A (zh) | 2013-08-15 | 2016-06-01 | 巴斯夫欧洲公司 | 指示吸着储存器的填充水平的装置和方法 |
| KR20160043960A (ko) | 2013-08-15 | 2016-04-22 | 바스프 에스이 | 수착 저장소용 충전 장치 및 수착 저장소 |
| EP3033566A1 (en) | 2013-08-15 | 2016-06-22 | Basf Se | Process for filling a sorption store with gas |
| US20160201855A1 (en) | 2013-08-15 | 2016-07-14 | Basf Se | Sorption store with improved heat transfer |
| WO2015025268A1 (en) | 2013-08-22 | 2015-02-26 | Basf Se | Method for purifying a mixture comprising liquid hydrocarbons, especially btx, and water |
| WO2015032851A2 (en) | 2013-09-06 | 2015-03-12 | Basf Se | Silicon-bridged pillared silicate compounds and process for their production |
| ES2774316T3 (es) | 2013-09-23 | 2020-07-20 | Basf Se | Procedimiento para la recuperación de componentes que forman un material estructural organometálico |
| US20150094202A1 (en) | 2013-09-27 | 2015-04-02 | Basf Corporation | Processes for activating adsorbent materials in adsorbed gas systems |
| WO2015059175A1 (en) | 2013-10-23 | 2015-04-30 | Basf Se | Powder or granulate for a zeolitic material and process for its production |
| BR112016007918B1 (pt) | 2013-10-23 | 2020-12-29 | Basf Se | processo para a produção de um corpo de moldagem, corpo de moldagem e uso de um corpo de moldagem |
| JP6526689B2 (ja) | 2013-11-05 | 2019-06-05 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | Mww型の骨格構造を有するスズ含有のゼオライト材料 |
| US9999878B2 (en) | 2013-11-05 | 2018-06-19 | Basf Se | Tin-containing zeolitic material having a BEA framework structure |
| WO2015067657A1 (en) | 2013-11-05 | 2015-05-14 | Basf Se | Process for the oxidation of organic carbonyl compounds |
| AR098619A1 (es) | 2013-12-05 | 2016-06-01 | Basf Se | Método y uso para la producción terciaria de aceite mineral mediante materiales marco metal-orgánicos |
| PL3080079T3 (pl) | 2013-12-11 | 2018-12-31 | Basf Se | Utlenianie 2-merkaptoetanolu |
| EP3110931B1 (en) | 2013-12-20 | 2018-04-18 | Basf Se | Novel aroma chemicals |
| JP6509877B2 (ja) | 2014-01-03 | 2019-05-08 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 有機テンプレートを使用しない合成による二金属交換ゼオライトベータ、およびNOxの選択触媒還元においてそれを使用する方法 |
| ES2679594T3 (es) | 2014-01-17 | 2018-08-29 | Basf Se | Procedimiento para la preparación de arilpropenos |
| WO2015123530A1 (en) | 2014-02-14 | 2015-08-20 | Basf Corporation | Methods and systems for improving capacity of adsorbed gas systems |
| WO2015123531A1 (en) | 2014-02-14 | 2015-08-20 | Basf Corporation | Methods and systems for heating adsorbed gas systems |
| EP2915797A1 (de) | 2014-03-07 | 2015-09-09 | Basf Se | Verfahren zur Herstellung von Menthonen aus Isopulegol in der Gasphase |
| US10888838B2 (en) | 2014-03-27 | 2021-01-12 | Basf Se | Porous films comprising metal-organic framework materials |
| JP6549611B2 (ja) | 2014-04-14 | 2019-07-24 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 匂いの品質が安定した2−置換4−ヒドロキシ−4−メチルテトラヒドロピランの製造 |
| CA2945062A1 (en) | 2014-04-22 | 2015-10-29 | Wintershall Holding GmbH | Solid-stabilized emulsion |
| WO2015162083A1 (en) | 2014-04-22 | 2015-10-29 | Wintershall Holding Ag | Process for recovery of oil |
| WO2015169721A1 (en) | 2014-05-05 | 2015-11-12 | Basf Se | Process for producing 2,6-dimethyl-5-hepten-1-al |
| WO2015169939A1 (en) | 2014-05-09 | 2015-11-12 | Basf Se | Method and device for filling a storage tank by recirculation of gas |
| WO2015177141A1 (en) | 2014-05-20 | 2015-11-26 | Basf Se | Process for the dimerization of activated olefins |
| US10227281B2 (en) | 2014-05-30 | 2019-03-12 | Basf Se | Preparation of 2,6- and 2,7-disubstituted anthraquinone derivates |
| DE102014008081A1 (de) | 2014-05-30 | 2015-11-19 | Basf Se | Verfahren zur Herstellung von Acrylsäure unter Verwendung eines alkali- und erdalkalifreien zeolithischen Materials |
| KR102381010B1 (ko) | 2014-05-30 | 2022-04-01 | 바스프 에스이 | 2,6- 및 2,7-이치환 안트라퀴논 유도체의 제조 |
| DE102014008080A1 (de) | 2014-05-30 | 2015-11-12 | Basf Se | Verfahren zur Herstellung von Acrylsäure unter Verwendung eines aluminiumfreien zeolithischen Materials |
| US10315924B2 (en) | 2014-06-05 | 2019-06-11 | Basf Se | CHA type zeolitic materials and methods for their preparation using combinations of cycloalkyl-and tetraalkylammonium compounds |
| WO2015185633A1 (en) | 2014-06-06 | 2015-12-10 | Basf Se | Synthesis of a boron-containing zeolite with an mww framework structure |
| WO2015197699A1 (en) | 2014-06-25 | 2015-12-30 | Basf Se | Process for preparing furan-2,5-dicarboxylic acid |
| US9171568B1 (en) | 2014-06-25 | 2015-10-27 | Western Digital Technologies, Inc. | Data storage device periodically re-initializing spindle motor commutation sequence based on timing data |
| EP2985364A1 (en) | 2014-08-14 | 2016-02-17 | Basf Se | Process for preparing alcohols by electrochemical reductive coupling |
| EP2985075A1 (en) | 2014-08-15 | 2016-02-17 | Basf Se | Shaped body made of a porous material |
| JP2017527500A (ja) | 2014-09-05 | 2017-09-21 | ビーエーエスエフ コーポレーション | 保存可能期間を延長する吸着材料 |
| MX2017003133A (es) | 2014-09-09 | 2017-06-14 | Basf Se | Metodo para producir una sustancia aromatica. |
| WO2016038019A1 (de) | 2014-09-09 | 2016-03-17 | Basf Se | Verfahren zur herstellung von 2-alkoxycyclohexanol |
| JP6775491B2 (ja) | 2014-09-09 | 2020-10-28 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ホウ素およびチタンを含むmwwゼオライト系材料の製造のための方法 |
| CR20170134A (es) | 2014-09-12 | 2017-06-13 | Basf Se | Método para preparar 2´-o-fucosil-lactosa |
| JP6822948B2 (ja) | 2014-09-26 | 2021-01-27 | ビーエイエスエフ・ソシエタス・エウロパエアBasf Se | 異性体として純粋な又は高度に異性体濃縮されたcis−又はtrans−(2−イソブチル−4−メチルテトラヒドロピラン−4−イル)アセテートの使用 |
| WO2016050690A1 (de) | 2014-09-29 | 2016-04-07 | Basf Se | Verfahren zur biokatalytischen cyclisierung von geranyllinalool und dabei erhaltene cyclisierungsprodukte |
| EP3002003A1 (de) | 2014-09-30 | 2016-04-06 | Basf Se | Verwendung neuartiger cyclischer Carbaldehyde als Aromastoff |
| JP2017533981A (ja) | 2014-10-14 | 2017-11-16 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 香料としてのヘキサデカ−8,15−ジエナールの使用 |
| US10301185B2 (en) | 2014-10-15 | 2019-05-28 | Basf Se | Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom |
| BR112017008176B1 (pt) | 2014-10-23 | 2021-11-03 | Construction Research & Technology Gmbh | Método para produzir carbonato de ácido glicérico, um método que compreende a oxidação de heyns e uma mistura de reação útil para realizar o referido método para produzir carbonato de ácido glicérico |
| BR112017008648B1 (pt) | 2014-10-27 | 2021-08-10 | Dow Global Technologies Llc | Processo contínuo para a preparação de óxido de propileno |
| WO2016071475A1 (de) | 2014-11-07 | 2016-05-12 | Basf Se | Verwendung von 3,3'-dimethoxy-4,4'-dihydroxystilben als aromastoff |
| EP3215247A1 (de) | 2014-11-07 | 2017-09-13 | Basf Se | Verfahren zur gewinnung aromatischer wertprodukte aus ligninhaltigen zusammensetzungen |
| KR20170084167A (ko) | 2014-11-11 | 2017-07-19 | 바스프 에스이 | 다공성 고체의 일체 성형체를 포함하는 저장 용기 |
| WO2016075100A1 (en) | 2014-11-11 | 2016-05-19 | Basf Se | Storage vessel comprising layers of a shaped body of a porous solid separated by a seal |
| WO2016075129A1 (en) | 2014-11-11 | 2016-05-19 | Basf Se | Storage vessel comprising at least one shaped body of a porous solid with spacers |
| WO2016074918A1 (en) | 2014-11-11 | 2016-05-19 | Basf Se | Thermoelectric device |
| US9920007B2 (en) | 2014-11-18 | 2018-03-20 | Basf Se | Process for the preparation of 1-(2,6,6-trimethylcyclohexyl)-alkan-3-ols |
| DE102014017804A1 (de) | 2014-12-02 | 2016-04-21 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
| EP3233778B1 (de) | 2014-12-19 | 2019-02-20 | Basf Se | Verfahren zur herstellung optisch aktiver carbonylverbindungen |
| EP3233780B1 (en) | 2014-12-19 | 2018-08-01 | Basf Se | 1-(7,10,10-trimethyl-4-bicyclo(6.2.0)decanyl)ethanone as novel aroma chemical |
| CN107250090B (zh) | 2014-12-19 | 2020-10-13 | 巴斯夫欧洲公司 | 制备1-[(1r,4r/s,8s)-10,10-二甲基-7-亚甲基-4-双环[6.2.0]癸基]乙酮的方法 |
| WO2016116406A1 (de) | 2015-01-21 | 2016-07-28 | Basf Se | Gasdruckbehälter enthaltend ein gas, ein latentwärmespeichermaterial und einen porösen feststoff |
| WO2016128917A1 (en) | 2015-02-12 | 2016-08-18 | Basf Se | Process for the preparation of a dealuminated zeolitic material having the bea framework structure |
| KR102512661B1 (ko) | 2015-02-13 | 2023-03-21 | 바스프 에스이 | 프로필렌 에폭시화용 티타늄 제올라이트 촉매의 재생 방법 |
| WO2016135133A1 (en) | 2015-02-27 | 2016-09-01 | Basf Se | A vehicle comprising a storage system and a combustion engine, the storage system comprising a container and at least one storage vessel |
| CN107438600B (zh) | 2015-03-05 | 2021-04-13 | 巴斯夫欧洲公司 | 制备四氢吡喃基酯的方法 |
| DE102015103608A1 (de) | 2015-03-11 | 2016-09-15 | Basf Se | Verfahren zur mikrobiellen de novo Synthese von Terpenen |
| WO2016177814A1 (en) | 2015-05-04 | 2016-11-10 | Basf Se | Process for the preparation of melonal |
-
2016
- 2016-05-04 WO PCT/EP2016/060062 patent/WO2016177814A1/en not_active Ceased
- 2016-05-04 JP JP2017557332A patent/JP6741687B2/ja active Active
- 2016-05-04 US US15/571,107 patent/US10202324B2/en active Active
- 2016-05-04 EP EP16722841.0A patent/EP3292099B1/en active Active
- 2016-05-04 ES ES16722841T patent/ES2821890T3/es active Active
- 2016-05-04 MX MX2017014148A patent/MX2017014148A/es unknown
- 2016-05-04 CN CN201680039475.9A patent/CN107735392B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP3292099B1 (en) | 2020-07-22 |
| CN107735392B (zh) | 2021-12-03 |
| MX2017014148A (es) | 2018-03-15 |
| WO2016177814A1 (en) | 2016-11-10 |
| ES2821890T3 (es) | 2021-04-28 |
| EP3292099A1 (en) | 2018-03-14 |
| US20180170850A1 (en) | 2018-06-21 |
| US10202324B2 (en) | 2019-02-12 |
| CN107735392A (zh) | 2018-02-23 |
| JP2018518467A (ja) | 2018-07-12 |
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