JP6620142B2 - ２，２，２−トリフルオロエタンチオールの合成 - Google Patents
２，２，２−トリフルオロエタンチオールの合成 Download PDFInfo
- Publication number
- JP6620142B2 JP6620142B2 JP2017506657A JP2017506657A JP6620142B2 JP 6620142 B2 JP6620142 B2 JP 6620142B2 JP 2017506657 A JP2017506657 A JP 2017506657A JP 2017506657 A JP2017506657 A JP 2017506657A JP 6620142 B2 JP6620142 B2 JP 6620142B2
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- msh
- mixture
- carried out
- reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/26—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/01—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and halogen atoms, or nitro or nitroso groups bound to the same carbon skeleton
- C07C323/02—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and halogen atoms, or nitro or nitroso groups bound to the same carbon skeleton having sulfur atoms of thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/03—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and halogen atoms, or nitro or nitroso groups bound to the same carbon skeleton having sulfur atoms of thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201462034214P | 2014-08-07 | 2014-08-07 | |
| US62/034,214 | 2014-08-07 | ||
| PCT/US2015/043060 WO2016022408A1 (en) | 2014-08-07 | 2015-07-31 | Synthesis of 2,2,2-trifluoroethanethiol |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017523217A JP2017523217A (ja) | 2017-08-17 |
| JP2017523217A5 JP2017523217A5 (enExample) | 2018-03-15 |
| JP6620142B2 true JP6620142B2 (ja) | 2019-12-11 |
Family
ID=55264366
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017506657A Active JP6620142B2 (ja) | 2014-08-07 | 2015-07-31 | ２，２，２−トリフルオロエタンチオールの合成 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US20170210706A1 (enExample) |
| EP (1) | EP3177280B1 (enExample) |
| JP (1) | JP6620142B2 (enExample) |
| KR (1) | KR102417295B1 (enExample) |
| CN (1) | CN106659699B (enExample) |
| ES (1) | ES2781077T3 (enExample) |
| MX (1) | MX2017001672A (enExample) |
| TW (1) | TWI710548B (enExample) |
| WO (1) | WO2016022408A1 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20210116544A (ko) | 2019-01-18 | 2021-09-27 | 바스프 에스이 | 티오카르보네이트의 제조 방법 |
| CN109880075B (zh) * | 2019-03-06 | 2021-10-08 | 山东益丰生化环保股份有限公司 | 一种高巯基多硫醇固化剂的制备方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2252867A (en) * | 1939-04-21 | 1941-08-19 | Hooker Electrochemical Co | Process for production of alkali metal sulphide and hydrosulphide of high purity and concentration |
| US2894991A (en) * | 1956-12-10 | 1959-07-14 | Pennsalt Chemicals Corp | Fluoroalkyl sulfur compounds |
| US3006964A (en) * | 1959-09-24 | 1961-10-31 | Pennsalt Chemicals Corp | Process for fluoroalkyl sulfides |
| US3088849A (en) * | 1961-12-11 | 1963-05-07 | Minnesota Mining & Mfg | Fluorocarbon-substituted mercaptans |
| DE4333058A1 (de) * | 1993-09-29 | 1995-03-30 | Hoechst Ag | Verfahren zur Herstellung von Trifluorethylschwefelverbindungen aus Thiolaten und 1-Chlor-2,2,2-trifluorethan |
| US6765109B1 (en) * | 1998-06-29 | 2004-07-20 | Roche Colorado Corporation | Preparation of S-aryl-cysteine and its derivatives |
| CN1432566A (zh) * | 2002-01-10 | 2003-07-30 | 王春煜 | 一种二巯基丙磺酸钠的制造及纯化方法 |
| US6680398B1 (en) * | 2002-08-16 | 2004-01-20 | Dow Corning Corporation | Method of making mercaptoalkylalkoxysilanes |
| CN1218939C (zh) * | 2002-12-25 | 2005-09-14 | 南化集团研究院 | 一种制取巯基乙酸的方法 |
| JP2012056898A (ja) * | 2010-09-09 | 2012-03-22 | Sumitomo Seika Chem Co Ltd | アルカンチオールの製造方法 |
-
2015
- 2015-07-31 ES ES15829587T patent/ES2781077T3/es active Active
- 2015-07-31 KR KR1020177003454A patent/KR102417295B1/ko active Active
- 2015-07-31 JP JP2017506657A patent/JP6620142B2/ja active Active
- 2015-07-31 CN CN201580042244.9A patent/CN106659699B/zh active Active
- 2015-07-31 US US15/500,654 patent/US20170210706A1/en not_active Abandoned
- 2015-07-31 EP EP15829587.3A patent/EP3177280B1/en active Active
- 2015-07-31 WO PCT/US2015/043060 patent/WO2016022408A1/en not_active Ceased
- 2015-07-31 MX MX2017001672A patent/MX2017001672A/es unknown
- 2015-08-07 TW TW104125725A patent/TWI710548B/zh active
-
2019
- 2019-01-03 US US16/238,548 patent/US10717707B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2016022408A1 (en) | 2016-02-11 |
| JP2017523217A (ja) | 2017-08-17 |
| CN106659699B (zh) | 2022-10-11 |
| US20170210706A1 (en) | 2017-07-27 |
| EP3177280A4 (en) | 2018-01-03 |
| TWI710548B (zh) | 2020-11-21 |
| KR20170041732A (ko) | 2017-04-17 |
| TW201605781A (zh) | 2016-02-16 |
| MX2017001672A (es) | 2017-08-15 |
| EP3177280B1 (en) | 2020-02-26 |
| EP3177280A1 (en) | 2017-06-14 |
| KR102417295B1 (ko) | 2022-07-07 |
| CN106659699A (zh) | 2017-05-10 |
| US20190135740A1 (en) | 2019-05-09 |
| US10717707B2 (en) | 2020-07-21 |
| ES2781077T3 (es) | 2020-08-28 |
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