JP2017523217A5 - - Google Patents
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- Publication number
- JP2017523217A5 JP2017523217A5 JP2017506657A JP2017506657A JP2017523217A5 JP 2017523217 A5 JP2017523217 A5 JP 2017523217A5 JP 2017506657 A JP2017506657 A JP 2017506657A JP 2017506657 A JP2017506657 A JP 2017506657A JP 2017523217 A5 JP2017523217 A5 JP 2017523217A5
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- msh
- carried out
- group
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims 20
- 239000000203 mixture Substances 0.000 claims 5
- 239000007795 chemical reaction product Substances 0.000 claims 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 3
- 239000006227 byproduct Substances 0.000 claims 3
- 239000012429 reaction media Substances 0.000 claims 3
- 150000005621 tetraalkylammonium salts Chemical group 0.000 claims 3
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 239000003444 phase transfer catalyst Substances 0.000 claims 2
- 239000003495 polar organic solvent Substances 0.000 claims 2
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- XKBGEWXEAPTVCK-UHFFFAOYSA-M methyltrioctylammonium chloride Chemical compound [Cl-].CCCCCCCC[N+](C)(CCCCCCCC)CCCCCCCC XKBGEWXEAPTVCK-UHFFFAOYSA-M 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 229920006395 saturated elastomer Polymers 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- JRMUNVKIHCOMHV-UHFFFAOYSA-M tetrabutylammonium bromide Chemical compound [Br-].CCCC[N+](CCCC)(CCCC)CCCC JRMUNVKIHCOMHV-UHFFFAOYSA-M 0.000 claims 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201462034214P | 2014-08-07 | 2014-08-07 | |
| US62/034,214 | 2014-08-07 | ||
| PCT/US2015/043060 WO2016022408A1 (en) | 2014-08-07 | 2015-07-31 | Synthesis of 2,2,2-trifluoroethanethiol |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017523217A JP2017523217A (ja) | 2017-08-17 |
| JP2017523217A5 true JP2017523217A5 (enExample) | 2018-03-15 |
| JP6620142B2 JP6620142B2 (ja) | 2019-12-11 |
Family
ID=55264366
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017506657A Active JP6620142B2 (ja) | 2014-08-07 | 2015-07-31 | ２，２，２−トリフルオロエタンチオールの合成 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US20170210706A1 (enExample) |
| EP (1) | EP3177280B1 (enExample) |
| JP (1) | JP6620142B2 (enExample) |
| KR (1) | KR102417295B1 (enExample) |
| CN (1) | CN106659699B (enExample) |
| ES (1) | ES2781077T3 (enExample) |
| MX (1) | MX2017001672A (enExample) |
| TW (1) | TWI710548B (enExample) |
| WO (1) | WO2016022408A1 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20210116544A (ko) | 2019-01-18 | 2021-09-27 | 바스프 에스이 | 티오카르보네이트의 제조 방법 |
| CN109880075B (zh) * | 2019-03-06 | 2021-10-08 | 山东益丰生化环保股份有限公司 | 一种高巯基多硫醇固化剂的制备方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2252867A (en) * | 1939-04-21 | 1941-08-19 | Hooker Electrochemical Co | Process for production of alkali metal sulphide and hydrosulphide of high purity and concentration |
| US2894991A (en) * | 1956-12-10 | 1959-07-14 | Pennsalt Chemicals Corp | Fluoroalkyl sulfur compounds |
| US3006964A (en) * | 1959-09-24 | 1961-10-31 | Pennsalt Chemicals Corp | Process for fluoroalkyl sulfides |
| US3088849A (en) * | 1961-12-11 | 1963-05-07 | Minnesota Mining & Mfg | Fluorocarbon-substituted mercaptans |
| DE4333058A1 (de) * | 1993-09-29 | 1995-03-30 | Hoechst Ag | Verfahren zur Herstellung von Trifluorethylschwefelverbindungen aus Thiolaten und 1-Chlor-2,2,2-trifluorethan |
| US6765109B1 (en) * | 1998-06-29 | 2004-07-20 | Roche Colorado Corporation | Preparation of S-aryl-cysteine and its derivatives |
| CN1432566A (zh) * | 2002-01-10 | 2003-07-30 | 王春煜 | 一种二巯基丙磺酸钠的制造及纯化方法 |
| US6680398B1 (en) * | 2002-08-16 | 2004-01-20 | Dow Corning Corporation | Method of making mercaptoalkylalkoxysilanes |
| CN1218939C (zh) * | 2002-12-25 | 2005-09-14 | 南化集团研究院 | 一种制取巯基乙酸的方法 |
| JP2012056898A (ja) * | 2010-09-09 | 2012-03-22 | Sumitomo Seika Chem Co Ltd | アルカンチオールの製造方法 |
-
2015
- 2015-07-31 ES ES15829587T patent/ES2781077T3/es active Active
- 2015-07-31 KR KR1020177003454A patent/KR102417295B1/ko active Active
- 2015-07-31 JP JP2017506657A patent/JP6620142B2/ja active Active
- 2015-07-31 CN CN201580042244.9A patent/CN106659699B/zh active Active
- 2015-07-31 US US15/500,654 patent/US20170210706A1/en not_active Abandoned
- 2015-07-31 EP EP15829587.3A patent/EP3177280B1/en active Active
- 2015-07-31 WO PCT/US2015/043060 patent/WO2016022408A1/en not_active Ceased
- 2015-07-31 MX MX2017001672A patent/MX2017001672A/es unknown
- 2015-08-07 TW TW104125725A patent/TWI710548B/zh active
-
2019
- 2019-01-03 US US16/238,548 patent/US10717707B2/en active Active
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