JP6611735B2 - 空気酸化による３−メチル−２−ニトロ安息香酸の調製プロセス - Google Patents

空気酸化による３−メチル−２−ニトロ安息香酸の調製プロセス Download PDF

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JP6611735B2
JP6611735B2 JP2016569944A JP2016569944A JP6611735B2 JP 6611735 B2 JP6611735 B2 JP 6611735B2 JP 2016569944 A JP2016569944 A JP 2016569944A JP 2016569944 A JP2016569944 A JP 2016569944A JP 6611735 B2 JP6611735 B2 JP 6611735B2
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formula
compound
acid
oxidation
mixture
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JP2017516808A (ja
JP2017516808A5 (enExample
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ステファン・アーネスト・ヤコブソン
ドナルド・ジェイ・デュマス
ルパート・スペンス
ヴェンカテスウァラ・ラオ・スリセッティ
サラ・メイ・クロフォード
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FMC Corp
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FMC Corp
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/49—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by carboxyl groups
    • C07C205/57—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by carboxyl groups having nitro groups and carboxyl groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C237/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
    • C07C237/28—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atom of at least one of the carboxamide groups bound to a carbon atom of a non-condensed six-membered aromatic ring of the carbon skeleton
    • C07C237/30—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atom of at least one of the carboxamide groups bound to a carbon atom of a non-condensed six-membered aromatic ring of the carbon skeleton having the nitrogen atom of the carboxamide group bound to hydrogen atoms or to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/14—Preparation of carboxylic acid nitriles by reaction of cyanides with halogen-containing compounds with replacement of halogen atoms by cyano groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C255/57—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton containing cyano groups and carboxyl groups, other than cyano groups, bound to the carbon skeleton

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
JP2016569944A 2014-05-29 2015-05-29 空気酸化による３−メチル−２−ニトロ安息香酸の調製プロセス Active JP6611735B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201462004459P 2014-05-29 2014-05-29
US62/004,459 2014-05-29
US201462027275P 2014-07-22 2014-07-22
US62/027,275 2014-07-22
PCT/US2015/033131 WO2015184229A1 (en) 2014-05-29 2015-05-29 Process to prepare 3-methyl-2-nitrobenzoic acid by air oxidation

Publications (3)

Publication Number Publication Date
JP2017516808A JP2017516808A (ja) 2017-06-22
JP2017516808A5 JP2017516808A5 (enExample) 2018-07-05
JP6611735B2 true JP6611735B2 (ja) 2019-11-27

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JP2016569944A Active JP6611735B2 (ja) 2014-05-29 2015-05-29 空気酸化による３−メチル−２−ニトロ安息香酸の調製プロセス

Country Status (16)

Country Link
US (2) US9828328B2 (enExample)
EP (1) EP3148962B1 (enExample)
JP (1) JP6611735B2 (enExample)
KR (2) KR20230052989A (enExample)
CN (2) CN106458843A (enExample)
AU (1) AU2015266819B2 (enExample)
BR (1) BR112016027556B1 (enExample)
HU (1) HUE050832T2 (enExample)
IL (1) IL248796B (enExample)
MX (1) MX2016015454A (enExample)
PL (1) PL3148962T3 (enExample)
RU (1) RU2689126C2 (enExample)
SG (2) SG10201810692VA (enExample)
TW (1) TWI678354B (enExample)
WO (1) WO2015184229A1 (enExample)
ZA (1) ZA201607811B (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI678354B (zh) * 2014-05-29 2019-12-01 新加坡商艾佛艾姆希農業新加坡有限公司 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程
CN114560772B (zh) * 2022-02-14 2023-07-28 南昌大学 一种3-甲基-2-硝基苯甲酸的合成方法
CN114560773B (zh) * 2022-02-14 2023-07-28 南昌大学 一种2-硝基-3-甲基苯甲酸的合成方法
TW202346260A (zh) * 2022-04-14 2023-12-01 美商富曼西公司 用於製備5-氯-2-((乙氧基羰基)胺基)-3-甲基苯甲酸之方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4329518A (en) * 1979-09-18 1982-05-11 Fmc Corporation Insecticidal [1,1'-biphenyl]-3-ylmethyl esters
JPH05132450A (ja) 1991-06-21 1993-05-28 Mitsubishi Gas Chem Co Inc ２−ニトロ−３−メチル安息香酸の製造法
US5591890A (en) * 1995-11-03 1997-01-07 E. I. Du Pont De Nemours And Company Process for producing ortho-nitro aromatic acids by oxidation of ortho-nitroalkylaromatic compounds
WO1998016503A2 (en) 1996-10-16 1998-04-23 American Cyanamid Company The preparation and use of ortho-sulfonamido aryl hydroxamic acids as matrix metalloproteinase and tace inhibitors
JP2000290235A (ja) * 1999-04-07 2000-10-17 Fuso Chemical Co Ltd ３−ニトロ−２−メチル安息香酸の製造方法
JP2001011026A (ja) * 1999-07-02 2001-01-16 Fuso Chemical Co Ltd ３−メチル−４−ニトロ安息香酸の製造方法
AR036872A1 (es) 2001-08-13 2004-10-13 Du Pont Compuesto de antranilamida, composicion que lo comprende y metodo para controlar una plaga de invertebrados
WO2004014873A1 (ja) * 2002-08-09 2004-02-19 Kyorin Pharmaceutical Co., Ltd. 4-置換キナゾリン-8-カルボン酸アミド誘導体とその薬理上許容される付加塩
MY140912A (en) 2004-07-26 2010-01-29 Du Pont Mixtures of anthranilamide invertebrate pest control agents
TWI363756B (en) * 2004-12-07 2012-05-11 Du Pont Method for preparing n-phenylpyrazole-1-carboxamides
WO2006080311A1 (ja) * 2005-01-25 2006-08-03 Ishihara Sangyo Kaisha, Ltd. アントラニルアミド系化合物、それらの製造方法及びそれらを含有する有害生物防除剤
JP2006232814A (ja) * 2005-01-25 2006-09-07 Ishihara Sangyo Kaisha Ltd アントラニルアミド系化合物、それらの製造方法及びそれらを含有する有害生物防除剤
JP2009062277A (ja) * 2005-12-27 2009-03-26 Nippon Soda Co Ltd ベンゾイソチアゾリン化合物及び有害生物防除剤
BRPI0713190B1 (pt) 2006-07-19 2016-11-16 Du Pont composto e métodos para preparar compostos
CN100434175C (zh) * 2006-10-17 2008-11-19 郑州大学 一种催化剂及其在合成4-硝基-3-甲基苯甲酸反应中的应用
TWI395728B (zh) 2006-12-06 2013-05-11 Du Pont 製備２-胺基-５-氰基苯甲酸衍生物之方法
TWI415827B (zh) 2006-12-21 2013-11-21 Du Pont 製備２-胺基-５-氰基苯甲酸衍生物之方法
TWI430980B (zh) 2007-06-29 2014-03-21 Du Pont 製備２－胺基－5－氰基苯甲酸衍生物之方法
US8212075B2 (en) 2007-11-08 2012-07-03 E.I. Du Pont De Nemours And Company Process for preparing 2-amino-5-cyanobenzoic acid derivatives
TWI432421B (zh) * 2007-12-19 2014-04-01 Du Pont 製備２－胺基－５－氰基苯甲酸衍生物之方法
TWI431000B (zh) 2008-03-05 2014-03-21 Du Pont 製備２－胺基－５－氰基苯甲酸衍生物之方法
DE102010030629A1 (de) 2010-06-29 2011-12-29 Robert Bosch Gmbh Drehzahlsensor, Fahrdynamikberegelungssteuergerät, Steuergerät und Systeme mit solchen Geräten sowie Verfahren zum Empfang von Daten über eine Funkstelle durch das Steuergerät
HUE025309T2 (en) * 2011-01-28 2016-01-28 Du Pont Process for the preparation of 2-aminobenzamide derivatives
CN103396467B (zh) * 2013-08-05 2015-01-28 上海杏灵科技药业股份有限公司 一种甾醇化合物的制备方法
TWI678354B (zh) * 2014-05-29 2019-12-01 新加坡商艾佛艾姆希農業新加坡有限公司 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程

Also Published As

Publication number Publication date
IL248796A0 (en) 2017-01-31
US10155718B2 (en) 2018-12-18
IL248796B (en) 2020-02-27
AU2015266819A1 (en) 2016-11-24
PL3148962T3 (pl) 2020-12-28
EP3148962B1 (en) 2020-05-13
ZA201607811B (en) 2018-05-30
WO2015184229A1 (en) 2015-12-03
MX2016015454A (es) 2017-03-23
BR112016027556A2 (pt) 2017-08-15
US20180072653A1 (en) 2018-03-15
BR112016027556B1 (pt) 2021-08-10
KR20170013249A (ko) 2017-02-06
JP2017516808A (ja) 2017-06-22
KR20230052989A (ko) 2023-04-20
TWI678354B (zh) 2019-12-01
SG11201609547SA (en) 2016-12-29
TW201602058A (zh) 2016-01-16
US20170197907A1 (en) 2017-07-13
EP3148962A1 (en) 2017-04-05
SG10201810692VA (en) 2018-12-28
HUE050832T2 (hu) 2021-01-28
CN116283596A (zh) 2023-06-23
RU2016151919A3 (enExample) 2018-12-03
KR102720359B1 (ko) 2024-10-23
RU2689126C2 (ru) 2019-05-24
US9828328B2 (en) 2017-11-28
AU2015266819B2 (en) 2019-04-04
RU2016151919A (ru) 2018-07-02
CN106458843A (zh) 2017-02-22

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