JP5953884B2 - サファイア単結晶の製造方法 - Google Patents
サファイア単結晶の製造方法 Download PDFInfo
- Publication number
- JP5953884B2 JP5953884B2 JP2012081574A JP2012081574A JP5953884B2 JP 5953884 B2 JP5953884 B2 JP 5953884B2 JP 2012081574 A JP2012081574 A JP 2012081574A JP 2012081574 A JP2012081574 A JP 2012081574A JP 5953884 B2 JP5953884 B2 JP 5953884B2
- Authority
- JP
- Japan
- Prior art keywords
- crystal
- single crystal
- sapphire single
- sapphire
- crucible
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000013078 crystal Substances 0.000 title claims description 280
- 229910052594 sapphire Inorganic materials 0.000 title claims description 101
- 239000010980 sapphire Substances 0.000 title claims description 101
- 238000004519 manufacturing process Methods 0.000 title claims description 36
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 49
- 238000000034 method Methods 0.000 claims description 43
- 239000007788 liquid Substances 0.000 claims description 34
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 23
- 229910052750 molybdenum Inorganic materials 0.000 claims description 23
- 239000011733 molybdenum Substances 0.000 claims description 23
- 239000000155 melt Substances 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000007872 degassing Methods 0.000 claims description 7
- 230000007547 defect Effects 0.000 description 11
- 239000002994 raw material Substances 0.000 description 9
- 239000000758 substrate Substances 0.000 description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 5
- 229910052741 iridium Inorganic materials 0.000 description 5
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 5
- 229910052710 silicon Inorganic materials 0.000 description 5
- 239000010703 silicon Substances 0.000 description 5
- 239000011810 insulating material Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000006698 induction Effects 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- LTUNNEGNEKBSEH-UHFFFAOYSA-N Prosulfuron Chemical compound COC1=NC(C)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2)CCC(F)(F)F)=N1 LTUNNEGNEKBSEH-UHFFFAOYSA-N 0.000 description 1
- 239000005604 Prosulfuron Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/36—Single-crystal growth by pulling from a melt, e.g. Czochralski method characterised by the seed, e.g. its crystallographic orientation
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/10—Crucibles or containers for supporting the melt
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/20—Controlling or regulating
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/30—Mechanisms for rotating or moving either the melt or the crystal
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/16—Oxides
- C30B29/20—Aluminium oxides
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012081574A JP5953884B2 (ja) | 2012-03-30 | 2012-03-30 | サファイア単結晶の製造方法 |
| KR1020130003851A KR101501036B1 (ko) | 2012-03-30 | 2013-01-14 | 사파이어 단결정 및 그의 제조 방법 |
| CN2013101069673A CN103361727A (zh) | 2012-03-30 | 2013-03-29 | 蓝宝石单晶及其制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012081574A JP5953884B2 (ja) | 2012-03-30 | 2012-03-30 | サファイア単結晶の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013209257A JP2013209257A (ja) | 2013-10-10 |
| JP2013209257A5 JP2013209257A5 (enExample) | 2015-04-09 |
| JP5953884B2 true JP5953884B2 (ja) | 2016-07-20 |
Family
ID=49363950
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012081574A Expired - Fee Related JP5953884B2 (ja) | 2012-03-30 | 2012-03-30 | サファイア単結晶の製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP5953884B2 (enExample) |
| KR (1) | KR101501036B1 (enExample) |
| CN (1) | CN103361727A (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5650869B1 (ja) * | 2013-03-21 | 2015-01-07 | 株式会社アライドマテリアル | サファイア単結晶育成用坩堝およびサファイア単結晶育成方法 |
| KR101532265B1 (ko) | 2013-12-03 | 2015-06-29 | 주식회사 엘지실트론 | 단결정 성장 장치 |
| CN104651935B (zh) * | 2014-10-17 | 2017-06-13 | 洛阳西格马炉业股份有限公司 | 一种坩埚上升法制备高品质蓝宝石晶体的方法 |
| CN109112631B (zh) * | 2018-10-29 | 2021-01-01 | 浙江昀丰新材料科技股份有限公司 | 一种蓝宝石c向长晶方法 |
| CN111394786A (zh) * | 2020-03-25 | 2020-07-10 | 哈尔滨奥瑞德光电技术有限公司 | 一种用于泡生法生长蓝宝石单晶的异形籽晶结构及其生长方法 |
| CN115233299A (zh) * | 2022-07-14 | 2022-10-25 | 露笑新能源技术有限公司 | 一种泡生法生长蓝宝石的引晶方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09278592A (ja) * | 1996-04-18 | 1997-10-28 | Mitsubishi Heavy Ind Ltd | チタンを含む酸化アルミニウム単結晶の製造方法 |
| JP2006151745A (ja) * | 2004-11-29 | 2006-06-15 | Kyocera Corp | 単結晶の製造方法及びそれらを用いた酸化物単結晶 |
| JP4940610B2 (ja) * | 2005-09-29 | 2012-05-30 | 住友金属鉱山株式会社 | サファイア単結晶の育成方法 |
| JP2008007353A (ja) * | 2006-06-28 | 2008-01-17 | Sumitomo Metal Mining Co Ltd | サファイア単結晶育成装置およびそれを用いた育成方法 |
| JP4810346B2 (ja) * | 2006-07-31 | 2011-11-09 | 株式会社信光社 | サファイア単結晶の製造方法 |
| JP4905171B2 (ja) * | 2007-02-14 | 2012-03-28 | 住友金属鉱山株式会社 | 酸化アルミニウム単結晶の製造方法及びこの方法を用いて得られる酸化アルミニウム単結晶 |
| JP4844429B2 (ja) * | 2007-02-26 | 2011-12-28 | 日立化成工業株式会社 | サファイア単結晶の製造方法 |
| JP2008266078A (ja) * | 2007-04-23 | 2008-11-06 | Shin Etsu Chem Co Ltd | サファイア単結晶の製造方法 |
| JP4835582B2 (ja) * | 2007-11-16 | 2011-12-14 | 住友金属鉱山株式会社 | 酸化アルミニウム単結晶の製造方法 |
| JP5004881B2 (ja) * | 2008-06-27 | 2012-08-22 | 京セラ株式会社 | 単結晶育成装置用坩堝、単結晶育成方法、および単結晶育成装置 |
| JP2010143781A (ja) * | 2008-12-17 | 2010-07-01 | Showa Denko Kk | サファイア単結晶の製造方法 |
| JP2010150056A (ja) * | 2008-12-24 | 2010-07-08 | Showa Denko Kk | サファイア単結晶の製造方法 |
| JP2010189242A (ja) * | 2009-02-20 | 2010-09-02 | Showa Denko Kk | サファイア単結晶の製造方法およびサファイア単結晶引き上げ装置 |
| JP2011032104A (ja) * | 2009-07-29 | 2011-02-17 | Showa Denko Kk | サファイア単結晶およびサファイア単結晶の製造方法 |
-
2012
- 2012-03-30 JP JP2012081574A patent/JP5953884B2/ja not_active Expired - Fee Related
-
2013
- 2013-01-14 KR KR1020130003851A patent/KR101501036B1/ko not_active Expired - Fee Related
- 2013-03-29 CN CN2013101069673A patent/CN103361727A/zh active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| JP2013209257A (ja) | 2013-10-10 |
| KR101501036B1 (ko) | 2015-03-10 |
| KR20130111253A (ko) | 2013-10-10 |
| CN103361727A (zh) | 2013-10-23 |
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