JP5322121B2 - 近赤外線の熱入力量を増加させるために使用される酸化タングステン - Google Patents
近赤外線の熱入力量を増加させるために使用される酸化タングステン Download PDFInfo
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- JP5322121B2 JP5322121B2 JP2010532540A JP2010532540A JP5322121B2 JP 5322121 B2 JP5322121 B2 JP 5322121B2 JP 2010532540 A JP2010532540 A JP 2010532540A JP 2010532540 A JP2010532540 A JP 2010532540A JP 5322121 B2 JP5322121 B2 JP 5322121B2
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- tungsten
- nir
- coating
- near infrared
- oxygen
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- B29K2055/00—Use of specific polymers obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in a single one of main groups B29K2023/00 - B29K2049/00, e.g. having a vinyl group, as moulding material
- B29K2055/02—ABS polymers, i.e. acrylonitrile-butadiene-styrene polymers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2067/00—Use of polyesters or derivatives thereof, as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2067/00—Use of polyesters or derivatives thereof, as moulding material
- B29K2067/04—Polyesters derived from hydroxycarboxylic acids
- B29K2067/046—PLA, i.e. polylactic acid or polylactide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2069/00—Use of PC, i.e. polycarbonates or derivatives thereof, as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2077/00—Use of PA, i.e. polyamides, e.g. polyesteramides or derivatives thereof, as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2995/00—Properties of moulding materials, reinforcements, fillers, preformed parts or moulds
- B29K2995/0018—Properties of moulding materials, reinforcements, fillers, preformed parts or moulds having particular optical properties, e.g. fluorescent or phosphorescent
- B29K2995/0026—Transparent
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
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- C01P2004/00—Particle morphology
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Description
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
タングステンブロンズは、EP 1676890に従って製造することができ、ここでは、メタタングステン酸アンモニウムの水溶液を金属塩とともに約300〜700℃に加熱し、そしてこの水性混合物を乾燥させて個体生成物を得ることによって、式MxWO3で表されるタングステンブロンズが製造できるとされている。
・基材
・顔料着色度
・顔料化学物質。
a)近赤外線の損失に起因する低エネルギー効率
b)例えば黒色(FW200)に顔料着色したものと、白色に(TiO2)顔料着色したものとの、硬化速度の差異
c)NIR乾燥は、クリアコート適用のためには使用できない
d)9002、9010&9016のような、特に白色のRALシェードが、NIR硬化の間、エネルギー効率が低い
ということである。
0.4μmのジルコニウムボール240mlを、水450ml中の Osram/ Sylvania社のWO2.7 106.5gの懸濁液に加える。この懸濁液を、Dynomill内で8時間、4500回転/分で粉砕する。得られる懸濁液を濾別し、乾燥させる。粒径は主に、30〜100nmである。
パラタングステン酸アンモニウム粉末((NH4)10W12H20O42・4H2O、Osram Sylvania)を、振動型粉末供給機を10g/分で稼働させてアルゴンキャリアガス中に運んだ。流動化された粉末を、Tekna PL-50プラズマトーチを備えるプラズマ反応器に供給して、出力65kWで稼働させた。反応器のプラズマホットゾーンで通常達成される温度範囲は、5000〜10,000Kである。アルゴン140slpm、水素0.5slpm、及びヘリウム5slpmから成る混合物[slpm=1分あたりの標準リットル;slpmの計算のための標準条件は、次のように定義される:Tn 0℃(32°F)、Pn=1.01bar(14.72psi)]を、シースガスに対して使用した。反応体の蒸気は急冷ガスにより冷却し、そして生成する粉末をバッグフィルタに集めた。生成する水素タングステンブロンズ粉末は、粉末X腺回折、電子顕微鏡、及びUV vis NIR分光分析により分析した。
様々なNIR吸収剤を2P−PU調製物内で、NIR硬化の間の温度吸収量について、並びに最終的なコーティング特性について試験した。NIR吸収剤は、以下の表(値はgで記載)に従って16時間にわたり、ガラスビーズとscandex社の撹拌機を用いてミルベースに組み込んだ。
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
実施例2に記載のIR吸収剤を、射出成形機によってポリカーボネートシート(厚さ2mm)に500ppmの濃度で組み込む。生成するやや青みがかった透明なシートは、250ワットのNd:YAGレーザーを用いて、ポリカーボネートシート(厚さ1mm)と一緒に溶着する。その表面を、20mm/秒の速度でレーザービームによりスキャンした。
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
水ベースの感圧性アクリル接着剤(PSA)(BASF Corp.社のAcronal V 212、固体含分は69%)を、水で希釈した。実施例2に記載のNIR吸収性添加剤を、Ciba社のアクリルコポリマー分散剤EFKA4585を用いてスピードミキサー中で混合した。ステンレス鋼のコーティングバーで、50ミクロンの接着剤層をガラス板に適用した。接着剤の質量は、NIR放射器のもと、複数回にわたる照射(multiple passes)の前、及び後に測定した。
熱で活性化される典型的なホットメルト接着剤(非晶質α−ポリオレフィンベースのもの、APAO)を、シグマブレード混練機内で170℃で1時間混合した。APAPポリマーはEvonik Industries社から、炭化水素樹脂及びスチレンブロックコポリマーはExxon Chemical社から、抗酸化剤はCiba Incから、そしてロジンエステルの粘着性増進剤(tackyfier)はEastman社から得た。これらの接着剤はホットメルトスロットダイコーターを用いて、シリコーン化された紙上にコーティングし、鋼製プレート担体に移した。接着剤試料を近赤外線に被曝し、そして接着剤表面の温度を、レーザー温度計により観察した。その結果、実施例2に従ったNIR吸収性添加剤を含まない接着剤は、対照の鋼製キャリアプレートのような温度にしか到達しないことがわかる。異なる量のNIR吸収性添加剤を加えることにより、接着剤表面温度はそれぞれ、99℃、109℃、及び162℃に急上昇する。
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
Tioxide AH-R(アナターゼ)45質量部、アクリルワニス54.9質量部(Wacker社のVinnapas C501樹脂、酢酸ビニルとクロトン酸とから成る固体コポリマー20質量部と、酢酸プロピル80質量部とを一緒に混合することにより製造される)、及び実施例2から得られる材料0.1質量部から成る無色のインク調製物を、バーコーターを用いてクレーコーティングされた紙に適用する。様々な出力でNd:YAGレーザー(14-25A, 20 kHz, 1500 mms, 4.2-7.6W)を用いたレーザーマーキングにより、コントラストが高い優れたマーキング結果が得られる。
実施例2の材料の代わりにランタンヘキサボライドを用いると、同一のレーザーマーキング性能を得るために、IR吸収剤が10倍以上必要となる(LaB6 1.4質量部)。
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用に関する。
MはNi、Pd、Pt、Au、Ir、Fe、Zn、W、Cu、Mo、In、Mn、Co、Mg、V、Cr及びTiであり、
X1、X2及びX3は、相互に独立して、硫黄又は酸素であり;
R1、R2、R3、R4、R5及びR6は相互に独立して水素、NR7R8、C1〜C18アルキル、アリール、アラルキル、ヘテロアリールアルキルである(この際、R7とR8は相互に独立してC1〜C18アルキル、アリール、アラルキル、ヘテロアリールアルキルである)]
のジチオレン金属錯体を含むブレンドの使用に関する。
Claims (11)
- コーティングのNIR硬化工程、又はコーティングのNIR乾燥工程で、近赤外線の熱入力量を増加させるための、式
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり、
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用。 - タングステン亜酸化物WO2.72、及びH0.3-0.7WO3、Na0.2-0.5WO3、Cs0.2-0.5WO3から選択されるタングステンブロンズが使用される、請求項1に記載の使用。
- Cs0.2-0.5WO3が使用される、請求項1又は2に記載の使用。
- コイルコーティングのNIR硬化工程又はNIR乾燥工程での、請求項1から3までのいずれか1項に記載の使用。
- NIR硬化工程又はNIR乾燥工程における、顔料着色されたコーティング内での、請求項1から4までのいずれか1項に記載の使用。
- 接着剤若しくは封止剤のNIR硬化工程、又は接着剤若しくは封止剤のNIR乾燥工程で、近赤外線の熱入力量を増加させるための、式
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり;
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用。 - タングステン亜酸化物WO2.72、及びH0.3-0.7WO3、Na0.2-0.5WO3、Cs0.2-0.5WO3から選択されるタングステンブロンズが使用される、請求項6に記載の使用。
- Cs0.2-0.5WO3が使用される、請求項6又は7に記載の使用。
- 印刷インキの乾燥工程、又はインクトナーを基材に定着させる工程で、近赤外線の熱入力量を増加させるための、式
WO3−x
[式中、Wはタングステン、Oは酸素、及びxは0.1〜1である]
の酸化タングステンの使用、及び/又は式
MxWyOz
[式中、
Mは、NH4、H、Li、Na、K、Rb、Cs、Ca、Ba、Sr、Fe、Sn、Mo、Nb、Ta、Ni、Pd、Pt、Cu、Ag、Au、Zn、Cd、Al、Ga、In、Tlから選択される1又は1つより多い要素であり;
Wはタングステンであり、
Oは酸素であり、
0.001≦x/y≦1、かつ2.0<z/y≦3.0である]
のタングステン酸塩の使用。 - タングステン亜酸化物WO2.72、及びH0.3-0.7WO3、Na0.2-0.5WO3、Cs0.2-0.5WO3から選択されるタングステンブロンズが使用される、請求項9に記載の使用。
- Cs0.2-0.5WO3が使用される、請求項9又は10に記載の使用。
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EP07119940 | 2007-11-05 | ||
EP07119940.0 | 2007-11-05 | ||
PCT/EP2008/064335 WO2009059900A2 (en) | 2007-11-05 | 2008-10-23 | Tungsten oxides used to increase the heat-input amount of near infrared radiation |
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JP2011503274A JP2011503274A (ja) | 2011-01-27 |
JP2011503274A5 JP2011503274A5 (ja) | 2011-12-01 |
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Family
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JP2010532540A Expired - Fee Related JP5322121B2 (ja) | 2007-11-05 | 2008-10-23 | 近赤外線の熱入力量を増加させるために使用される酸化タングステン |
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US (2) | US8168711B2 (ja) |
EP (4) | EP2244879A2 (ja) |
JP (2) | JP5634871B2 (ja) |
KR (4) | KR101320750B1 (ja) |
CN (4) | CN101848865B (ja) |
BR (1) | BRPI0818911A8 (ja) |
CO (1) | CO6280522A2 (ja) |
EC (1) | ECSP10010198A (ja) |
TW (1) | TWI461368B (ja) |
WO (2) | WO2009059901A2 (ja) |
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KR20100037148A (ko) | 2007-07-18 | 2010-04-08 | 바스프 에스이 | 레이저 감응성 코팅 제제 |
CA2699583C (en) | 2007-09-27 | 2016-04-19 | Francesca Peri | Isolable and redispersable transition metal nanoparticles their preparation and use as ir absorbers |
US8853314B2 (en) | 2008-10-23 | 2014-10-07 | Datalase Ltd. | Heat absorbing additives |
EP2342295A1 (en) | 2008-10-27 | 2011-07-13 | DataLase Ltd | Coating composition for marking substrates |
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JP2011504157A (ja) * | 2007-11-05 | 2011-02-03 | ビーエーエスエフ ソシエタス・ヨーロピア | 断熱添加剤 |
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