JP4424991B2 - ホスゲンを製造するための反応器およびホスゲンの製造方法 - Google Patents

ホスゲンを製造するための反応器およびホスゲンの製造方法 Download PDF

Info

Publication number
JP4424991B2
JP4424991B2 JP2003570972A JP2003570972A JP4424991B2 JP 4424991 B2 JP4424991 B2 JP 4424991B2 JP 2003570972 A JP2003570972 A JP 2003570972A JP 2003570972 A JP2003570972 A JP 2003570972A JP 4424991 B2 JP4424991 B2 JP 4424991B2
Authority
JP
Japan
Prior art keywords
reactor
catalyst
range
heat transfer
catalyst tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2003570972A
Other languages
English (en)
Japanese (ja)
Other versions
JP2005525986A5 (esLanguage
JP2005525986A (ja
Inventor
オルベルト，ゲールハルト
マトケ，トルステン
ヴァンデルヴェーレン，ルク
ネヴェヤンス，フィリップ
ハメネカー，ヤン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2005525986A publication Critical patent/JP2005525986A/ja
Publication of JP2005525986A5 publication Critical patent/JP2005525986A5/ja
Application granted granted Critical
Publication of JP4424991B2 publication Critical patent/JP4424991B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B01J31/28—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/001—Controlling catalytic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B01J12/007—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/0085—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/80—Phosgene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044—Temperature measurement
    • B01J2208/00061—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00513—Controlling the temperature using inert heat absorbing solids in the bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/0061—Controlling the level
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B01J2219/0002—Plants assembled from modules joined together
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00777—Baffles attached to the reactor wall horizontal
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S585/00—Chemistry of hydrocarbon compounds
    • Y10S585/919—Apparatus considerations
    • Y10S585/921—Apparatus considerations using recited apparatus structure
    • Y10S585/922—Reactor fluid manipulating device
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S585/00—Chemistry of hydrocarbon compounds
    • Y10S585/919—Apparatus considerations
    • Y10S585/921—Apparatus considerations using recited apparatus structure
    • Y10S585/924—Reactor shape or disposition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2003570972A 2002-02-27 2003-02-12 ホスゲンを製造するための反応器およびホスゲンの製造方法 Expired - Fee Related JP4424991B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10208398 2002-02-27
PCT/EP2003/001372 WO2003072237A1 (de) 2002-02-27 2003-02-12 Reaktor und verfahren zur herstellung von phosgen

Publications (3)

Publication Number Publication Date
JP2005525986A JP2005525986A (ja) 2005-09-02
JP2005525986A5 JP2005525986A5 (esLanguage) 2009-03-05
JP4424991B2 true JP4424991B2 (ja) 2010-03-03

Family

ID=27762465

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2003570972A Expired - Fee Related JP4424991B2 (ja) 2002-02-27 2003-02-12 ホスゲンを製造するための反応器およびホスゲンの製造方法

Country Status (12)

Country Link
US (2) US8409539B2 (esLanguage)
EP (1) EP1485195B1 (esLanguage)
JP (1) JP4424991B2 (esLanguage)
KR (1) KR100936420B1 (esLanguage)
CN (1) CN1302842C (esLanguage)
AT (1) ATE309856T1 (esLanguage)
AU (1) AU2003208834A1 (esLanguage)
BR (1) BR0307973A (esLanguage)
DE (1) DE50301676D1 (esLanguage)
ES (1) ES2253661T3 (esLanguage)
IN (1) IN237581B (esLanguage)
WO (1) WO2003072237A1 (esLanguage)

Families Citing this family (76)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8409539B2 (en) * 2002-02-27 2013-04-02 Basf Aktiengesellschaft Reactor and method for producing phosgene
JP4145607B2 (ja) * 2002-08-23 2008-09-03 三菱化学株式会社 多管式反応器を用いた気相接触酸化方法
DE102004010383B4 (de) * 2004-03-03 2007-04-12 Man Dwe Gmbh Vorrichtung zur Simulierung des Reaktionsprozesses in und Verfahren zur Optimierung von Mantelrohrreaktoren
DE102004018267B4 (de) * 2004-04-15 2007-05-03 Man Dwe Gmbh Reaktoranordnung zur Durchführung katalytischer Gasphasenreaktionen
DE102004041777A1 (de) * 2004-08-28 2006-03-02 Bayer Materialscience Ag Verfahren und Vorrichtung zur Herstellung von Phosgen
DE102005001952A1 (de) * 2005-01-14 2006-07-27 Man Dwe Gmbh Rohrbündelreaktor zur Durchführung exothermer oder endothermer Gasphasenreaktionen
DE102005032663A1 (de) 2005-07-13 2007-01-18 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102005061626A1 (de) * 2005-12-21 2007-06-28 Basf Ag Verfahren der kontinuierlichen heterogen katalysierten partiellen Dehydrierung wenigstens eines zu dehydrierenden Kohlenwasserstoffs
JP4692351B2 (ja) * 2006-03-29 2011-06-01 Ｊｆｅスチール株式会社 空気分離機に付属するアルゴン精製器
US7504533B2 (en) * 2006-04-24 2009-03-17 Bayer Materialscience Llc Process for the production of isocyanates
DE102006022761A1 (de) * 2006-05-16 2007-11-22 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102006023261A1 (de) 2006-05-18 2007-11-22 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006023581A1 (de) * 2006-05-19 2007-11-22 Bayer Materialscience Ag Verfahren zur Abtrennung von Chlor aus dem Produktgas eines HCI-Oxidationsprozesses
DE102006024506A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006024516A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006024515A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Chlorwasserstoff-Oxidation mit Sauerstoff
DE102006024518A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor aus Chlorwasserstoff und Sauerstoff
DE102006029790A1 (de) * 2006-06-27 2008-01-03 Basf Ag Verfahren der kontinuierlichen heterogen katalysierten partiellen Dehydrierung wenigstens eines zu dehydrierenden Kohlenwasserstoffs
CN101020891B (zh) * 2007-02-07 2011-04-06 秦皇岛领先科技发展有限公司 列管式固定床生物反应器
DE102007020444A1 (de) 2007-04-27 2008-11-06 Bayer Materialscience Ag Verfahren zur Oxidation eines Chlorwasserstoffenthaltenden Gasgemisches
EP2231324B1 (en) * 2007-12-18 2016-06-29 Dow Technology Investments LLC Tube reactor
DE102007061477A1 (de) * 2007-12-20 2009-07-02 Man Dwe Gmbh Rohrbündelreaktor
DE102008009761A1 (de) * 2008-02-19 2009-08-27 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102008012037A1 (de) 2008-03-01 2009-09-03 Bayer Materialscience Ag Verfahren zur Herstellung von Methylen-diphenyl-diisocyanaten
HUE030997T2 (en) * 2008-11-26 2017-06-28 Huntsman Int Llc Process for the preparation of isocyanates
JP5336828B2 (ja) * 2008-12-02 2013-11-06 三井化学株式会社 塩化カルボニルの製造方法および製造装置、ならびに、ポリイソシアネートの製造方法および製造装置
HUE047744T2 (hu) * 2008-12-16 2020-05-28 Basf Se Reaktor és eljárás foszgén elõállítására
ES2656791T3 (es) 2008-12-16 2018-02-28 Basf Se Reactor y procedimiento para la producción de fosgeno
PT2406181T (pt) 2009-03-11 2020-12-24 Basf Se Processo para a produção de fosgénio
DE102009032020A1 (de) 2009-07-07 2011-01-13 Bayer Materialscience Ag Verfahren zur Herstellung von Polycarbonat
SG174714A1 (en) 2010-03-30 2011-10-28 Bayer Materialscience Ag Process for preparing diaryl carbonates and polycarbonates
SG174715A1 (en) 2010-03-30 2011-10-28 Bayer Materialscience Ag Process for preparing diaryl carbonates and polycarbonates
CN101893251B (zh) * 2010-07-26 2011-09-21 王兴军 一种锅炉的吸热器
FR2965490B1 (fr) 2010-09-30 2013-01-11 Aet Group Dispositif et procede pour la phosgenation en continu
EP2586767A1 (de) 2011-10-25 2013-05-01 Bayer MaterialScience AG Verfahren zur Herstellung von Diarylcarbonaten und Polycarbonaten
JP6156860B2 (ja) * 2012-04-04 2017-07-05 住友化学株式会社 多管式反応器および多管式反応器の設計方法
KR101361002B1 (ko) * 2012-05-21 2014-02-12 고등기술연구원연구조합 간접 가열식 ｖｏｃ 반응기
WO2014009346A1 (de) 2012-07-11 2014-01-16 Bayer Materialscience Ag Vorrichtung und verfahren zur herstellung von phosgen
CN105408249A (zh) 2013-07-26 2016-03-16 沙特基础全球技术有限公司 用于生产高纯光气的方法和装置
EP3024783A1 (en) 2013-07-26 2016-06-01 SABIC Global Technologies B.V. Method and apparatus for producing high purity phosgene
JP5667253B2 (ja) * 2013-08-01 2015-02-12 三井化学株式会社 塩化カルボニルの製造装置およびポリイソシアネートの製造装置
CN104415770B (zh) * 2013-08-26 2016-08-31 万华化学集团股份有限公司 一种制备光气的催化剂及制备光气的方法
KR101832864B1 (ko) * 2013-11-06 2018-02-27 와트 퓨얼 셀 코퍼레이션 기체 반응 매질 플로우 관리용 매니폴드를 가지는 화학 반응기
US9180436B1 (en) 2013-11-19 2015-11-10 Emerging Fuels Technology, Inc. Optimized fischer-tropsch catalyst
US9358526B2 (en) 2013-11-19 2016-06-07 Emerging Fuels Technology, Inc. Optimized fischer-tropsch catalyst
JP6316446B2 (ja) * 2014-02-04 2018-04-25 サビック グローバル テクノロジーズ ベスローテン フェンノートシャップ カーボネートの製造方法
CN105960389A (zh) * 2014-02-04 2016-09-21 沙特基础工业全球技术有限公司 用于生产碳酸酯的方法
DE102014202591A1 (de) * 2014-02-13 2015-08-13 Siemens Aktiengesellschaft Umwandlung von Metallcarbonat in Metallchlorid
DE102014202593A1 (de) 2014-02-13 2015-08-13 Siemens Aktiengesellschaft Umwandlung von Metallcarbonat in Metallchlorid
EP2955158B1 (en) 2014-06-11 2020-05-27 Haldor Topsøe A/S A process for safe production of phosgene
CN104190328B (zh) * 2014-08-12 2017-02-01 中国天辰工程有限公司 一种可用于制取气相氰化氢的反应器
JP6567653B2 (ja) 2014-08-20 2019-08-28 バイエル、アクチエンゲゼルシャフトＢａｙｅｒ Ａｋｔｉｅｎｇｅｓｅｌｌｓｃｈａｆｔ ヒドロキシル、チオール、アミノおよび／またはホルムアミド基を有する化合物のホスゲン化方法
US20180214837A1 (en) * 2015-07-29 2018-08-02 Primus Green Energy Inc. Two-stage reactor for exothermal and reversible reactions and methods thereof
DE102015013516B4 (de) * 2015-10-20 2018-01-18 Frank Brucker Rohrbündelwärmeübertrager und Fertigungsverfahren für Rohrbündelwärmeübertrager
DE102016100908A1 (de) 2015-11-06 2017-05-11 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Anlage und Verfahren zur Erzeugung von Fettalkohol
WO2017144584A1 (en) * 2016-02-26 2017-08-31 Shell Internationale Research Maatschappij B.V. Alkane oxidative dehydrogenation (odh)
US10815170B2 (en) * 2016-07-26 2020-10-27 Shell Oil Company Oxidative dehydrogenation (ODH) of ethane
US10752564B2 (en) * 2016-07-26 2020-08-25 Shell Oil Company Oxidative dehydrogenation (ODH) of ethane
EP3421426A1 (de) * 2017-06-29 2019-01-02 Covestro Deutschland AG Energieeffizientes verfahren zur bereitstellung von phosgen-dampf
CN107175056A (zh) * 2017-07-12 2017-09-19 陕西省石油化工研究设计院 高效的液芯光纤光催化反应器
EP3498752A1 (de) 2017-12-18 2019-06-19 Covestro Deutschland AG Verfahren zur herstellung eines polycarbonats unter verwendung eines organischen lösungsmittels auf der grundlage von chlorkohlenwasserstoffen
CN109941965B (zh) * 2019-04-21 2023-05-26 苏州市泰利登净化设备有限公司 一种甲醇制氢设备
US12391557B2 (en) 2019-04-25 2025-08-19 Basf Se Method for producing phosgene
CN113891855B (zh) * 2019-05-20 2025-03-28 巴斯夫欧洲公司 生产光气的方法和反应器
KR20220045150A (ko) 2019-08-08 2022-04-12 코베스트로 인텔렉쳐 프로퍼티 게엠베하 운트 콤파니 카게 폴리카르보네이트를 제조하는 방법
CN112441585B (zh) * 2019-08-30 2022-07-12 万华化学集团股份有限公司 光气合成及盐水蒸发电解一体化处理工艺
EP3862317A1 (de) * 2020-02-06 2021-08-11 Basf Se Verfahren und reaktor zur herstellung von phosgen
KR20230012601A (ko) 2020-05-20 2023-01-26 바스프 에스이 포스겐의 제조를 위한 방법, 반응 혼합물 및 촉매
US12491484B2 (en) * 2021-01-15 2025-12-09 CRI, hf Reactor for synthesis of methanol or other products
WO2022195071A1 (en) 2021-03-19 2022-09-22 Basf Se Apparatus and method for hotspot detection in a tube bundle reactor
EP4326675A1 (en) 2021-04-21 2024-02-28 Basf Se Process for preparing phosgene
KR20240014072A (ko) 2021-05-27 2024-01-31 바스프 에스이 포스겐을 제조하는 방법
WO2023001651A1 (de) 2021-07-23 2023-01-26 Basf Se Verfahren zur herstellung von phosgen
KR20250027815A (ko) 2022-06-30 2025-02-27 바스프 에스이 포스젠의 제조 방법
CN115520868B (zh) * 2022-10-25 2023-11-21 摩珈(上海)生物科技有限公司 一种光气的循环制备方法及其装置系统
KR102840405B1 (ko) * 2022-12-27 2025-07-29 이화여자대학교 산학협력단 포름산염 제조 반응기, 그의 운전방법 및 상기 반응기를 포함하는 포름산 제조장치

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2986454A (en) 1957-07-23 1961-05-30 American Cyanamid Co Tubular catalytic converter
US3518284A (en) 1967-02-20 1970-06-30 Shell Oil Co Partial oxidation of organic compounds
US3807963A (en) * 1972-03-09 1974-04-30 J Smith Reaction apparatus
DE2238851B2 (de) * 1972-08-07 1979-08-30 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung von Acrolein und/oder Acrylsäure unter Vermeidung von Nachreaktionen bei der katalytischen Oxidation von Propylen und/oder Acrolein
US4231959A (en) * 1978-02-15 1980-11-04 Stauffer Chemical Company Phosgene manufacture
JP4024301B2 (ja) * 1996-02-21 2007-12-19 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ホスゲンの製造方法
US6084125A (en) * 1996-02-27 2000-07-04 Praxair Technology, Inc. Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid
EP0998973A1 (de) * 1998-10-27 2000-05-10 Balcke-Dürr Energietechnik GmbH Gekühlter Rohrbündelreaktor
WO2002002220A1 (en) * 2000-06-29 2002-01-10 H2Gen Innovations Inc. Improved system and integrated chemical reactor for hydrogen production through steam reforming of hydrocarbons
JP4092090B2 (ja) * 2001-06-26 2008-05-28 株式会社日本触媒 固体粒子充填反応器およびその反応器を用いた接触気相酸化方法
US8409539B2 (en) * 2002-02-27 2013-04-02 Basf Aktiengesellschaft Reactor and method for producing phosgene

Also Published As

Publication number Publication date
US20130072717A1 (en) 2013-03-21
US8821829B2 (en) 2014-09-02
US20050118088A1 (en) 2005-06-02
EP1485195A1 (de) 2004-12-15
IN2004CH01858A (esLanguage) 2006-06-23
WO2003072237A1 (de) 2003-09-04
CN1302842C (zh) 2007-03-07
ATE309856T1 (de) 2005-12-15
KR20040087326A (ko) 2004-10-13
AU2003208834A1 (en) 2003-09-09
IN237581B (esLanguage) 2010-01-01
BR0307973A (pt) 2004-12-21
JP2005525986A (ja) 2005-09-02
ES2253661T3 (es) 2006-06-01
DE50301676D1 (de) 2005-12-22
EP1485195B1 (de) 2005-11-16
CN1638856A (zh) 2005-07-13
US8409539B2 (en) 2013-04-02
KR100936420B1 (ko) 2010-01-12

Similar Documents

Publication Publication Date Title
JP4424991B2 (ja) ホスゲンを製造するための反応器およびホスゲンの製造方法
CN1321056C (zh) 通过气相氧化氯化氢制备氯
US4714592A (en) Radial flow catalytic reactor including heat exchange apparatus within the bed
US7226567B1 (en) Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions
JP2005525986A5 (esLanguage)
US5520891A (en) Cross-flow, fixed-bed catalytic reactor
JP5378539B2 (ja) ホスゲンを調製するための反応器および方法
US4341737A (en) Apparatus for carrying out catalytic exothermic and endothermic high-pressure gas reactions
EP1839735B1 (en) A transverse tubular heat exchange reactor and a process for catalytic synthesis therein
CA2709887C (en) Tube reactor having an insert for reduced volume outlet head space
CN102316971B (zh) 制备光气的反应器和方法
JP4330537B2 (ja) 塩化水素の気相酸化により塩素を製造する方法
JPH0347134B2 (esLanguage)
CN102458638A (zh) 多级多管壳管式反应器
PL124655B1 (en) Method of operation of reaction between gaseous raw materials and reactor therefor
JPH0376976B2 (esLanguage)
WO2003031050A1 (en) Heat exchange reactor
KR102915553B1 (ko) 포스겐을 제조하기 위한 방법 및 반응기
JPS58112046A (ja) 反応器
JPS61118132A (ja) 触媒反応装置
US20240269634A1 (en) Method for producing phosgene
KR830002469B1 (ko) 입상 촉매층과 접촉하는 기상 원료물질의 발열 반응방법
JP2004518519A (ja) 多数の触媒管を有する長尺反応器
JPS60122036A (ja) 触媒充填反応器

Legal Events

Date Code Title Description
A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20080214

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20080509

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20080819

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20081118

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A821

Effective date: 20081119

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20091110

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20091208

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121218

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121218

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20131218

Year of fee payment: 4

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees