JP4158162B2 - クロロシランの加水分解 - Google Patents

クロロシランの加水分解 Download PDF

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Publication number
JP4158162B2
JP4158162B2 JP2007535673A JP2007535673A JP4158162B2 JP 4158162 B2 JP4158162 B2 JP 4158162B2 JP 2007535673 A JP2007535673 A JP 2007535673A JP 2007535673 A JP2007535673 A JP 2007535673A JP 4158162 B2 JP4158162 B2 JP 4158162B2
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Japan
Prior art keywords
hydrochloric acid
hcl
hydrolysis reactor
weight percent
hydrolyzate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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JP2007535673A
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English (en)
Japanese (ja)
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JP2008516044A (ja
JP2008516044A5 (enExample
Inventor
ゲイミー、アンドリュー・ブルース
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Dow Silicones Corp
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Publication date
Application filed by Dow Corning Corp, Dow Silicones Corp filed Critical Dow Corning Corp
Publication of JP2008516044A publication Critical patent/JP2008516044A/ja
Publication of JP2008516044A5 publication Critical patent/JP2008516044A5/ja
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Publication of JP4158162B2 publication Critical patent/JP4158162B2/ja
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/08—Preparatory processes characterised by the catalysts used

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Silicon Polymers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2007535673A 2004-10-05 2005-08-09 クロロシランの加水分解 Expired - Lifetime JP4158162B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/958,768 US7208617B2 (en) 2004-10-05 2004-10-05 Hydrolysis of chlorosilanes
PCT/US2005/028429 WO2006041561A1 (en) 2004-10-05 2005-08-09 Hydrolysis of chlorosilanes

Publications (3)

Publication Number Publication Date
JP2008516044A JP2008516044A (ja) 2008-05-15
JP2008516044A5 JP2008516044A5 (enExample) 2008-06-26
JP4158162B2 true JP4158162B2 (ja) 2008-10-01

Family

ID=35276465

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2007535673A Expired - Lifetime JP4158162B2 (ja) 2004-10-05 2005-08-09 クロロシランの加水分解

Country Status (8)

Country Link
US (1) US7208617B2 (enExample)
EP (1) EP1809688B1 (enExample)
JP (1) JP4158162B2 (enExample)
KR (1) KR101159520B1 (enExample)
CN (1) CN100577713C (enExample)
AT (1) ATE493460T1 (enExample)
DE (1) DE602005025673D1 (enExample)
WO (1) WO2006041561A1 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7479566B2 (en) * 2005-01-13 2009-01-20 Dow Corning Corporation Method for preparation of alkoxysilanes having reduced halide
JP4388588B2 (ja) 2005-03-29 2009-12-24 ダウ・コーニング・コーポレイション クロロシランの反応蒸留
DE102005048035A1 (de) * 2005-10-06 2007-04-12 Wacker Chemie Ag Verfahren zur Herstellung von OH-endständigen Organohydrogenpolysiloxanen
US8019416B2 (en) * 2006-11-13 2011-09-13 Cardiac Pacemakers, Inc. Reduction of AV delay for treatment of cardiac disease
US7941216B2 (en) * 2006-11-17 2011-05-10 Cardiac Pacemakers, Inc. Method and device for treating myocardial ischemia
CN101323666B (zh) * 2008-07-24 2011-04-27 北京石油化工设计院有限公司 一种甲基氯硅烷浓酸水解连续生产水解物的方法
EP2528928A2 (en) 2010-01-26 2012-12-05 Dow Corning Corporation Method of preparing an organohalosilane
US9296765B2 (en) 2012-08-13 2016-03-29 Dow Corning Corporation Method of preparing an organohalosilane
FR3000070B1 (fr) 2012-12-21 2015-02-06 Bluestar Silicones France Procede de preparation de polyorganosiloxanes fonctionnalises
DE102013201851A1 (de) 2013-02-05 2014-08-21 Wacker Chemie Ag Hydrolyse von Organochlorsilanen im Rohrbündelreaktor
CN105705507B (zh) 2013-11-12 2018-08-31 美国陶氏有机硅公司 制备卤代硅烷的方法
CN103694477B (zh) * 2013-12-03 2016-04-06 中国科学院过程工程研究所 一种硅树脂的清洁制备方法
EP3233731B1 (en) 2014-12-18 2020-08-05 Dow Silicones Corporation Method for producing aryl-functional silanes
DE102015201446A1 (de) * 2015-01-28 2016-07-28 Wacker Chemie Ag Verfahren zur Reinigung von verunreinigtem gasförmigem Chlorwasserstoff
CN105085920A (zh) * 2015-09-24 2015-11-25 唐山三友硅业有限责任公司 低粘度二甲基硅油的连续制备工艺
CN109134865A (zh) * 2018-07-20 2019-01-04 山东东岳有机硅材料股份有限公司 高品质副产物硅油的制备方法
CN110669221B (zh) * 2019-10-31 2021-11-30 河北科盛瑞化工有限公司 一种高沸硅油的水解方法
US12454456B2 (en) 2020-09-04 2025-10-28 John R. CALLAWAY Hydrogen chloride loop fuel reaction
CN113620247A (zh) * 2021-08-26 2021-11-09 浙江新安化工集团股份有限公司 一种有机硅高沸物的处理工艺
CN114768704B (zh) * 2022-04-20 2025-06-17 内蒙古恒星化学有限公司 二甲基二氯硅烷水解产物分离系统
CN116003797B (zh) * 2022-12-08 2024-02-23 唐山三友硅业股份有限公司 高沸硅油生产工艺及生产系统

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4382145A (en) * 1981-09-02 1983-05-03 General Electric Company Method of hydrolyzing organochlorosilanes
JPH028223A (ja) * 1988-06-27 1990-01-11 Toshiba Silicone Co Ltd オルガノクロロシランの加水分解方法
DE4343033A1 (de) * 1993-12-16 1995-06-29 Wacker Chemie Gmbh Verfahren zur Herstellung von Polydimethylsiloxanen
FR2766492B1 (fr) * 1997-07-24 1999-10-22 Rhodia Chimie Sa Procede de preparation de polyorganosiloxanes par hydrolyse d'organohalosilanes
CN100357298C (zh) * 2003-08-10 2007-12-26 蓝星化工新材料股份有限公司江西星火有机硅厂 有机二氯硅烷的连续水解工艺

Also Published As

Publication number Publication date
EP1809688A1 (en) 2007-07-25
JP2008516044A (ja) 2008-05-15
KR101159520B1 (ko) 2012-06-25
KR20070061559A (ko) 2007-06-13
DE602005025673D1 (de) 2011-02-10
US7208617B2 (en) 2007-04-24
CN100577713C (zh) 2010-01-06
WO2006041561A1 (en) 2006-04-20
ATE493460T1 (de) 2011-01-15
US20060074189A1 (en) 2006-04-06
EP1809688B1 (en) 2010-12-29
CN101035838A (zh) 2007-09-12

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