JP2958673B2 - アクリル酸の精製方法と装置、およびその方法により精製されたアクリル酸 - Google Patents
アクリル酸の精製方法と装置、およびその方法により精製されたアクリル酸Info
- Publication number
- JP2958673B2 JP2958673B2 JP6077928A JP7792894A JP2958673B2 JP 2958673 B2 JP2958673 B2 JP 2958673B2 JP 6077928 A JP6077928 A JP 6077928A JP 7792894 A JP7792894 A JP 7792894A JP 2958673 B2 JP2958673 B2 JP 2958673B2
- Authority
- JP
- Japan
- Prior art keywords
- acrylic acid
- crystallization
- static
- purification
- crystallizer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH00922/93-8 | 1993-03-26 | ||
CH92293 | 1993-03-26 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH0748311A JPH0748311A (ja) | 1995-02-21 |
JP2958673B2 true JP2958673B2 (ja) | 1999-10-06 |
Family
ID=4198293
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP6077928A Expired - Lifetime JP2958673B2 (ja) | 1993-03-26 | 1994-03-25 | アクリル酸の精製方法と装置、およびその方法により精製されたアクリル酸 |
Country Status (9)
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007191449A (ja) * | 2006-01-20 | 2007-08-02 | Nippon Shokubai Co Ltd | アクリル酸の製造方法 |
JP2011213735A (ja) * | 2011-07-19 | 2011-10-27 | Nippon Shokubai Co Ltd | アクリル酸の製造方法 |
Families Citing this family (87)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2727061B2 (ja) | 1993-10-13 | 1998-03-11 | 日揮株式会社 | 晶析方法及び晶析装置 |
JP3724864B2 (ja) * | 1995-12-01 | 2005-12-07 | 日揮株式会社 | 晶析方法 |
DE19600955A1 (de) * | 1996-01-12 | 1997-07-17 | Basf Ag | Verfahren zur Herstellung von Acrylsäure und deren Ester |
DE19606877A1 (de) * | 1996-02-23 | 1997-08-28 | Basf Ag | Verfahren zur Reinigung von Acrylsäure und Methacrylsäure |
DE19627679A1 (de) * | 1996-07-10 | 1998-01-15 | Basf Ag | Verfahren zur Reinigung von Roh-Acrylsäure durch Kristallisation |
DE19627847A1 (de) * | 1996-07-10 | 1998-01-15 | Basf Ag | Verfahren zur Herstellung von Acrylsäure |
GB9714632D0 (en) * | 1997-07-12 | 1997-09-17 | Ici Plc | Process for the production of methyl methacrylate |
MY120051A (en) * | 1997-07-30 | 2005-08-30 | Mitsubishi Rayon Co | Process for purification of (meth)acrylic acid |
DE19740252A1 (de) | 1997-09-12 | 1999-03-18 | Basf Ag | Verfahren zur Herstellung von Acrylsäure und Methacrylsäure |
DE19829477A1 (de) * | 1998-07-01 | 2000-01-05 | Basf Ag | Verfahren zur Reinigung von Acrylsäure oder Methacrylsäure durch Kristallisation und Destillation |
DE19833049A1 (de) * | 1998-07-22 | 2000-01-27 | Basf Ag | Verfahren zur Herstellung von Acrylsäure |
DE19904820A1 (de) | 1999-02-05 | 2000-08-10 | Stockhausen Chem Fab Gmbh | Verfahren und Vorrichtung zur Reinigung von Stoffen mittels Kristallisation |
MY122671A (en) | 1999-03-06 | 2006-04-29 | Basf Ag | Fractional condensation of a product gas mixture containing acrylic acid |
DE19923389A1 (de) | 1999-05-21 | 2000-08-17 | Basf Ag | Verfahren zum Lagern und/oder Transportieren von Reinacrylsäure |
US6500982B1 (en) * | 1999-06-28 | 2002-12-31 | Rohm And Haas Company | Process for preparing (meth) acrylic acid |
AU7489300A (en) * | 1999-09-22 | 2001-04-24 | Cognis Corporation | Purification and recovery of dicarboxylic acids using melt crystallization |
FR2799386B1 (fr) * | 1999-10-12 | 2001-12-28 | Befs Prokem | Procede de purification de produits organiques par cristallisation fractionnee a vitesse de circulation variable |
JP3938646B2 (ja) | 2000-01-14 | 2007-06-27 | 株式会社日本触媒 | アクリル酸の製造方法 |
DE10003498A1 (de) * | 2000-01-27 | 2001-08-02 | Basf Ag | Reinigungsverfahren für (Meth)acrylsäure |
WO2001077056A1 (de) * | 2000-04-11 | 2001-10-18 | Basf Aktiengesellschaft | Verfahren zur reinigung einer rohacrylsäureschmelze |
DE10026407A1 (de) | 2000-05-29 | 2001-12-06 | Basf Ag | Verfahren der diskontinuierlichen kristallisativen Reinigung von Roh-Acrylsäure |
JP4673958B2 (ja) * | 2000-06-19 | 2011-04-20 | 株式会社日本触媒 | 固形物除去装置 |
JP5008215B2 (ja) * | 2000-09-29 | 2012-08-22 | 三菱瓦斯化学株式会社 | 晶析方法および装置 |
BR0206396A (pt) * | 2001-01-12 | 2004-02-10 | Degussa | Processo contìnuo para preparação e purificação de ácido (met)acrìlico |
DE10122788A1 (de) * | 2001-05-10 | 2002-06-06 | Basf Ag | Verfahren der kristallisativen Reinigung einer Roh-Schmelze wenigstens eines Monomeren |
DE10122787A1 (de) | 2001-05-10 | 2002-06-06 | Basf Ag | Verfahren zur Herstellung einer gereinigten Schmelze wenigstens eines Monomeren |
EP2311789B1 (en) * | 2001-12-04 | 2015-10-07 | Mitsubishi Chemical Corporation | Process for producing (meth)acrylic acids |
DE10211686A1 (de) * | 2002-03-15 | 2003-10-02 | Stockhausen Chem Fab Gmbh | (Meth)Acrylsäurekristall und Verfahren zur Herstellung und Aufreinigung von wässriger (Meth)Acrylsäure |
DE10221176A1 (de) | 2002-05-13 | 2003-11-27 | Basf Ag | Verfahren zur Herstellung geruchsarmer Hydrogelbildender Polymerisate |
DE10301040B4 (de) | 2003-01-13 | 2005-07-21 | Stockhausen Gmbh | Aufreinigung eines Monomers durch Extraktion mit einem Phasenbildner und Kristallisation |
JP2005247731A (ja) * | 2004-03-03 | 2005-09-15 | Mitsubishi Chemicals Corp | (メタ)アクリル酸組成物及びその製造方法 |
DE102004034316B4 (de) * | 2004-07-15 | 2015-07-16 | Evonik Degussa Gmbh | Ein Verfahren zur Herstellung von (Meth)Acrylsäure |
DE102004044638A1 (de) * | 2004-09-13 | 2006-03-30 | Stockhausen Gmbh | Aufreinigung eines (Meth)Acrylsäure enthaltenen Destillationssumpfprodukts durch Kristallisation |
DE102004044639A1 (de) * | 2004-09-13 | 2006-05-24 | Stockhausen Gmbh | Verfahren zur extraktiven Aufreinigung von (Meth)Acrylsäure unter Einsatz eines Trennmittels |
DE102004058907A1 (de) | 2004-12-07 | 2006-06-08 | Basf Ag | Reinigung von ionischen Flüssigkeiten |
BRPI0607493A2 (pt) * | 2005-03-01 | 2010-04-06 | Basf Ag | processo para remover ácido metacrìlico a partir da fase lìquida p, que compreende ácido acrìlico como um constituinte principal e produto alvo e ácido metacrìlico como um componente secundário |
US7705181B2 (en) | 2005-03-01 | 2010-04-27 | Basf Akiengesellschaft | Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component |
DE102005009890A1 (de) * | 2005-03-01 | 2006-09-07 | Basf Ag | Verfahren zur Abtrennung von Methacrylsäure aus Acrylsäure als Hauptbestandteil sowie Zielprodukt und Methacrylsäure als Nebenkomponente enthaltender flüssiger Phase |
CN101511441B (zh) | 2006-09-12 | 2012-02-22 | 苏舍化学技术有限公司 | 净化离子液体的方法 |
DE102007055086A1 (de) | 2007-11-16 | 2009-05-20 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
DE102007004960A1 (de) | 2007-01-26 | 2008-07-31 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
DE102007014603A1 (de) | 2007-03-23 | 2008-09-25 | Basf Se | Verfahren des Transports einer aus einem Lagerbehälter entnommenen flüssigen Monomerenphase im Tank eines Tankwagens oder eines Tankschiffs |
DE102007014606A1 (de) | 2007-03-23 | 2008-09-25 | Basf Se | Verfahren zur Lagerung einer unter den Bedingungen der Lagerung flüssigen Monomerenphase |
DE102007043748A1 (de) * | 2007-09-13 | 2008-09-11 | Basf Se | Verfahren zur kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat |
JP4822559B2 (ja) * | 2007-09-19 | 2011-11-24 | ローム アンド ハース カンパニー | (メタ)アクリル酸生成物流からのプロピオン酸の選択的減少のための改良された方法 |
EP2085376B1 (en) | 2008-01-30 | 2012-09-05 | Evonik Röhm GmbH | Process for preparation of high purity methacrylic acid |
FR2934264B1 (fr) * | 2008-07-22 | 2012-07-20 | Arkema France | Fabrication d'esters de vinyle a partir de matieres renouvelables, esters de vinyle obtenus et utilisations |
DE102008040799A1 (de) | 2008-07-28 | 2008-12-11 | Basf Se | Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal |
DE102008041573A1 (de) | 2008-08-26 | 2010-03-04 | Basf Se | Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal |
EP2334631B1 (de) | 2008-07-28 | 2017-03-01 | Basf Se | Verfahren zur auftrennung von in einem produktgasgemisch einer partiellen heterogen katalysierten gasphasenoxidation einer c3-vorläuferverbinding der acrylsäure als hauptbestandteil enthaltener acrylsäure und als nebenprodukt enthaltenem glyoxal |
EP2433924B1 (en) * | 2009-05-19 | 2017-09-27 | Nippon Shokubai Co., Ltd. | Process for production of (meth)acrylic acid |
BRPI1011858B1 (pt) * | 2009-06-01 | 2018-03-20 | Nippon Shokubai Co., Ltd. | Método para cristalização de ácido (met)acrílico e método para regular o teor de inibidor de polimerização em ácido (met)acrílico de produto |
US8846977B2 (en) * | 2009-06-30 | 2014-09-30 | Nippon Shokubai Co. Ltd. | Crystallization unit for acrylic acid and method for crystallization of acrylic acid using the same |
US8680331B2 (en) | 2009-07-01 | 2014-03-25 | Nippon Shokubai Co., Ltd. | Process for production of (meth)acrylic acid |
EP2450339B1 (en) * | 2009-07-02 | 2017-07-26 | Nippon Shokubai Co., Ltd. | Process for production of (meth)acrylic acid |
US8859809B2 (en) * | 2009-07-03 | 2014-10-14 | Nippon Shokubai Co., Ltd. | Device and process for crystallizing (meth)acrylic acid |
FR2948365B1 (fr) * | 2009-07-22 | 2011-09-09 | Arkema France | Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol |
FR2948366B1 (fr) | 2009-07-22 | 2012-08-17 | Arkema France | Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol |
DE102010031507A1 (de) | 2010-06-02 | 2011-12-08 | Evonik Stockhausen Gmbh | Verfahren zur Reinigung kristalliner Phasen aus Produktgemischen mittels Schichtkristallisation |
DE102011076931A1 (de) | 2011-06-03 | 2012-12-06 | Basf Se | Wässrige Lösung, enthaltend Acrylsäure und deren konjugierte Base |
US8729299B2 (en) | 2011-10-03 | 2014-05-20 | Celanese International Corporation | Processes for the production of acrylic acids and acrylates |
US8536368B2 (en) | 2011-10-03 | 2013-09-17 | Celanese International Corporation | Processes for the production of acrylic acids and acrylates from a trioxane feed |
US8658822B2 (en) | 2011-10-03 | 2014-02-25 | Celanese International Corporation | Processes for producing acrylic acids and acrylates |
WO2013163806A1 (en) | 2012-05-03 | 2013-11-07 | Evonik Industries Ag | Process for preparation of highly pure, non-yellowing methacrylic acid |
EP2928574B1 (en) * | 2013-01-14 | 2021-09-29 | Sulzer Management AG | Multi-stage crystallisation process and apparatus to purify a compound |
EP2777791A1 (en) | 2013-03-11 | 2014-09-17 | Sulzer Chemtech AG | Process and apparatus for purification of a stream containing a cyclic ester of an alpha-hydroxycarboxylic acid |
US9732023B2 (en) | 2013-03-18 | 2017-08-15 | Evonik Roehm Gmbh | Process for preparation of methacrylic acid and methacrylic acid esters |
US9073846B2 (en) | 2013-06-05 | 2015-07-07 | Celanese International Corporation | Integrated process for the production of acrylic acids and acrylates |
US9120743B2 (en) | 2013-06-27 | 2015-09-01 | Celanese International Corporation | Integrated process for the production of acrylic acids and acrylates |
WO2015036273A1 (de) | 2013-09-12 | 2015-03-19 | Basf Se | Verfahren zur herstellung von acrylsäure |
EP3145965B1 (de) | 2014-05-19 | 2020-02-19 | Basf Se | Verfahren zur kontinuierlichen dehydratisierung von 3-hydroxypropionsäure zu acrylsäure |
WO2016026763A1 (en) | 2014-08-18 | 2016-02-25 | Basf Se | Process for preparing acrylic acid using a heterogeneous alumina catalyst |
EP3012244A1 (en) * | 2014-10-24 | 2016-04-27 | Sulzer Chemtech AG | Process and apparatus for purification of acrylic acid |
DE102014017804A1 (de) | 2014-12-02 | 2016-04-21 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
WO2016135020A1 (de) | 2015-02-24 | 2016-09-01 | Basf Se | Verfahren zur kontinuierlichen dehydratisierung von 3-hydroxypropionsäure zu acrylsäure |
WO2016162175A1 (de) | 2015-04-07 | 2016-10-13 | Basf Se | Verfahren zur dehydratisierung von 3-hydroxypropionsäure zu acrylsäure |
EP3103539A1 (en) * | 2015-06-11 | 2016-12-14 | Sulzer Chemtech AG | Method and apparatus for purifying a mixture comprising oil and wax |
FR3041958B1 (fr) | 2015-10-06 | 2019-06-14 | Arkema France | Procede ameliore de production d’acide (meth)acrylique de grade polymere |
ES2667205T3 (es) * | 2015-11-30 | 2018-05-10 | Evonik Degussa Gmbh | Depuración fina de isoforonanitrilo mediante cristalización por fusión |
WO2017122040A1 (en) | 2016-01-12 | 2017-07-20 | Sabic Global Technologies B.V. | A dynamic melt crystallization process for purifying dicyclopentadiene from a mixed liquid hydrocarbon stream |
US10968160B2 (en) | 2016-12-22 | 2021-04-06 | Eastman Chemical Company | Separation of propionic acid from acrylic acid via azeotropic distillation |
CN110099889B (zh) | 2016-12-22 | 2023-04-04 | 伊士曼化工公司 | 经由分隔壁塔的丙烯酸提纯 |
CN108707072A (zh) * | 2018-05-10 | 2018-10-26 | 宜兴丹森科技有限公司 | 丙烯酸组合物的纯化方法 |
FR3094716B1 (fr) | 2019-04-02 | 2021-06-04 | Arkema France | Production d’acide acrylique de grade polymere |
FR3108906B1 (fr) | 2020-04-06 | 2022-03-04 | Arkema France | Procede de purification d’acide (meth)acrylique |
CN113144660B (zh) * | 2021-02-05 | 2023-03-03 | 成都思达能环保设备有限公司 | 一种结晶方法及系统 |
WO2023006503A1 (de) | 2021-07-28 | 2023-02-02 | Basf Se | Verfahren zur herstellung von acrylsäure |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE521274A (US20020095090A1-20020718-M00002.png) * | 1952-07-11 | |||
US2885431A (en) * | 1954-06-21 | 1959-05-05 | Phillips Petroleum Co | Separation by crystallization |
US2868830A (en) * | 1954-10-18 | 1959-01-13 | Phillips Petroleum Co | Separation by crystallization |
US3050952A (en) * | 1960-10-05 | 1962-08-28 | Phillips Petroleum Co | Separation by crystallization |
DE1620756A1 (de) * | 1966-07-13 | 1970-07-16 | Vickers Zimmer Ag Plangung Und | Verfahren zur Reinigung von stark verunreinigten Lactamen von omega-Aminocarbonsaeuren |
AT279547B (de) * | 1967-04-14 | 1970-03-10 | Buchs Metallwerk Ag | Verfahren und Vorrichtung zur Trennung oder Reinigung schmelzflüssiger, flüssiger oder gelöster Stoffe durch fraktioniertes Kristallisieren |
DE2606364B2 (de) * | 1976-02-18 | 1981-07-30 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Stofftrennung aus einem flüssigen Gemisch durch fraktionierte Kristallisation |
US4230888A (en) * | 1977-12-15 | 1980-10-28 | Standard Oil Company (Ohio) | Process for purification of acrylic acid by fractional crystallization |
US4780568A (en) * | 1984-12-14 | 1988-10-25 | Ashland Oil, Inc. | Purification of methacrylic acid from an oxydehydrogenation by crystallization |
-
1994
- 1994-03-08 TW TW083101994A patent/TW305830B/zh not_active IP Right Cessation
- 1994-03-14 ES ES94810158T patent/ES2086990T3/es not_active Expired - Lifetime
- 1994-03-14 DE DE59400240T patent/DE59400240D1/de not_active Expired - Lifetime
- 1994-03-14 EP EP94810158A patent/EP0616998B1/de not_active Expired - Lifetime
- 1994-03-14 SG SG9606214A patent/SG93785A1/en unknown
- 1994-03-22 US US08/216,162 patent/US5504247A/en not_active Expired - Lifetime
- 1994-03-24 KR KR1019940005927A patent/KR100219943B1/ko not_active IP Right Cessation
- 1994-03-25 JP JP6077928A patent/JP2958673B2/ja not_active Expired - Lifetime
- 1994-03-26 CN CN94103445A patent/CN1058256C/zh not_active Expired - Lifetime
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007191449A (ja) * | 2006-01-20 | 2007-08-02 | Nippon Shokubai Co Ltd | アクリル酸の製造方法 |
JP2011213735A (ja) * | 2011-07-19 | 2011-10-27 | Nippon Shokubai Co Ltd | アクリル酸の製造方法 |
Also Published As
Publication number | Publication date |
---|---|
EP0616998B1 (de) | 1996-05-01 |
EP0616998A1 (de) | 1994-09-28 |
ES2086990T3 (es) | 1996-07-01 |
US5504247A (en) | 1996-04-02 |
CN1105014A (zh) | 1995-07-12 |
KR100219943B1 (ko) | 1999-09-01 |
JPH0748311A (ja) | 1995-02-21 |
DE59400240D1 (de) | 1996-06-05 |
TW305830B (US20020095090A1-20020718-M00002.png) | 1997-05-21 |
SG93785A1 (en) | 2003-01-21 |
CN1058256C (zh) | 2000-11-08 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP2958673B2 (ja) | アクリル酸の精製方法と装置、およびその方法により精製されたアクリル酸 | |
US3621664A (en) | Fractional crystallization process | |
JP4272704B2 (ja) | 精製テレフタル酸の製造法および装置 | |
US7964689B2 (en) | Superabsorbent polymer made from acrylic acid | |
JPH08176045A (ja) | ビスフェノールaの精製法 | |
JP3659507B2 (ja) | アクリル酸の精製方法 | |
US5814231A (en) | Separation of liquid eutectic mixtures by crystallization on cold surfaces and apparatus for this purpose | |
US5264592A (en) | Lactide melt recrystallization | |
CN107750181B (zh) | 半连续结晶方法和装置 | |
EP1173417A1 (en) | Process and apparatus for making ultra-pure dmso | |
JP2003534322A (ja) | 純粋なn−ビニルピロリドンの取得方法 | |
JP4092738B2 (ja) | 晶出により液体混合物から物質を分離する方法 | |
EP0273509A1 (en) | Process- and apparatus for recovering a pure substance from a liquid mixture by crystallization | |
JP2635351B2 (ja) | 冷却結晶層の浄化法 | |
WO2011001891A1 (ja) | (メタ)アクリル酸の製造方法 | |
JP4343423B2 (ja) | メチルメタクリレートの製造方法 | |
US6596862B2 (en) | Purification of N-vinyl-ε-caprolactam | |
JP4188085B2 (ja) | 高濃縮過酸化水素を製造するための連続的方法、高濃縮過酸化水素およびその使用 | |
US20020087029A1 (en) | Purification of acrylic acid by crystallization by means of vacuum evaporation | |
US20240010599A1 (en) | Method for purifying compound | |
JP2004345994A (ja) | N−ビニル−2−ピロリドンの精製方法 | |
JPS59110645A (ja) | 純粋なクロトン酸の製造方法 | |
JP6214156B2 (ja) | メタクリル酸の精製方法 | |
JP4112361B2 (ja) | 晶出による過酸化水素水溶液の濃縮方法 | |
JP2003286228A (ja) | ヒドロキシアルキル(メタ)アクリレートの精製方法、および、ヒドロキシアルキル(メタ)アクリレートの製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20080730 Year of fee payment: 9 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090730 Year of fee payment: 10 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20100730 Year of fee payment: 11 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20100730 Year of fee payment: 11 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20110730 Year of fee payment: 12 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20120730 Year of fee payment: 13 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20120730 Year of fee payment: 13 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20130730 Year of fee payment: 14 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
EXPY | Cancellation because of completion of term |