JP2015517451A5 - - Google Patents
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- JP2015517451A5 JP2015517451A5 JP2015514213A JP2015514213A JP2015517451A5 JP 2015517451 A5 JP2015517451 A5 JP 2015517451A5 JP 2015514213 A JP2015514213 A JP 2015514213A JP 2015514213 A JP2015514213 A JP 2015514213A JP 2015517451 A5 JP2015517451 A5 JP 2015517451A5
- Authority
- JP
- Japan
- Prior art keywords
- growth
- single crystal
- sic single
- sic
- crystal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000859 sublimation Methods 0.000 claims description 20
- 230000008022 sublimation Effects 0.000 claims description 20
- 239000013078 crystal Substances 0.000 claims 40
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 22
- 239000002019 doping agent Substances 0.000 claims 16
- 229910052720 vanadium Inorganic materials 0.000 claims 15
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 15
- 229910052796 boron Inorganic materials 0.000 claims 11
- 238000000034 method Methods 0.000 claims 11
- 229910052757 nitrogen Inorganic materials 0.000 claims 11
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 9
- 238000002109 crystal growth method Methods 0.000 claims 9
- 239000007789 gas Substances 0.000 claims 8
- 239000000463 material Substances 0.000 claims 7
- 125000004429 atom Chemical group 0.000 claims 6
- 239000001257 hydrogen Substances 0.000 claims 6
- 229910052739 hydrogen Inorganic materials 0.000 claims 6
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 4
- -1 boron halide compound Chemical class 0.000 claims 4
- 229910001507 metal halide Inorganic materials 0.000 claims 3
- 150000005309 metal halides Chemical class 0.000 claims 3
- 239000007787 solid Substances 0.000 claims 3
- 230000004913 activation Effects 0.000 claims 2
- 229910052786 argon Inorganic materials 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 150000002431 hydrogen Chemical class 0.000 claims 2
- 239000012535 impurity Substances 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 238000000151 deposition Methods 0.000 claims 1
- 229910052731 fluorine Inorganic materials 0.000 claims 1
- 239000011737 fluorine Substances 0.000 claims 1
- 238000002386 leaching Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 229910052758 niobium Inorganic materials 0.000 claims 1
- 239000010955 niobium Substances 0.000 claims 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- 238000001556 precipitation Methods 0.000 claims 1
- 229910052715 tantalum Inorganic materials 0.000 claims 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261651143P | 2012-05-24 | 2012-05-24 | |
| US61/651,143 | 2012-05-24 | ||
| PCT/US2013/042604 WO2013177496A1 (en) | 2012-05-24 | 2013-05-24 | Vanadium compensated, si sic single crystals of nu and pi type and the crystal growth process thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015517451A JP2015517451A (ja) | 2015-06-22 |
| JP2015517451A5 true JP2015517451A5 (enExample) | 2016-09-01 |
| JP6001768B2 JP6001768B2 (ja) | 2016-10-05 |
Family
ID=49624371
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015514213A Expired - Fee Related JP6001768B2 (ja) | 2012-05-24 | 2013-05-24 | ＮＵ型及びＰＩ型のバナジウム補償型ＳＩＳｉＣ単結晶及びその結晶成長方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9090989B2 (enExample) |
| EP (1) | EP2855741B1 (enExample) |
| JP (1) | JP6001768B2 (enExample) |
| KR (1) | KR101661053B1 (enExample) |
| CN (1) | CN104364428B (enExample) |
| WO (1) | WO2013177496A1 (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9090989B2 (en) | 2012-05-24 | 2015-07-28 | Ii-Vi Incorporated | Vanadium compensated, SI SiC single crystals of NU and PI type and the crystal growth process thereof |
| CN105734672B (zh) * | 2014-12-10 | 2018-11-30 | 北京天科合达半导体股份有限公司 | 一种在含氧气氛下生长高质量碳化硅晶体的方法 |
| US20170321345A1 (en) | 2016-05-06 | 2017-11-09 | Ii-Vi Incorporated | Large Diameter Silicon Carbide Single Crystals and Apparatus and Method of Manufacture Thereof |
| CN109666971B (zh) * | 2017-10-16 | 2020-11-10 | 北京北方华创微电子装备有限公司 | 生长炉 |
| CN108118394B (zh) * | 2017-12-28 | 2020-07-17 | 河北同光晶体有限公司 | 一种降低碳化硅单晶中氮杂质含量的方法 |
| CN107955969A (zh) * | 2017-12-28 | 2018-04-24 | 河北同光晶体有限公司 | 一种持续供料的SiC单晶生长系统 |
| JP7268299B2 (ja) * | 2018-08-08 | 2023-05-08 | 株式会社レゾナック | 遮蔽部材及び単結晶成長装置 |
| CN110055588A (zh) * | 2019-06-05 | 2019-07-26 | 华北电力大学 | 一种碳化硅单晶生长用固气界面可控的坩埚 |
| JP6806270B1 (ja) * | 2019-06-20 | 2021-01-06 | 三菱電機株式会社 | 炭化ケイ素単結晶、半導体素子 |
| CN110408998B (zh) * | 2019-07-29 | 2020-12-22 | 江苏星特亮科技有限公司 | 一种碳化硅单晶连续生长装置及其生长方法 |
| CN110565167A (zh) * | 2019-08-19 | 2019-12-13 | 河北同光晶体有限公司 | 一种用于PVT法生长SiC单晶的装料装置及装料方法 |
| JP7263537B2 (ja) * | 2019-10-31 | 2023-04-24 | 京セラ株式会社 | 配線基板、電子装置及び電子モジュール |
| US12006591B2 (en) * | 2020-03-02 | 2024-06-11 | Ii-Vi Advanced Materials, Llc | Method for preparing an aluminum doped silicon carbide crystal by providing a compound including aluminum and oxygen in a capsule comprised of a first and second material |
| CN111534854B (zh) * | 2020-06-12 | 2021-07-13 | 北京北方华创微电子装备有限公司 | 晶体生长炉 |
| JP2021195301A (ja) | 2020-06-18 | 2021-12-27 | 盛新材料科技股▲ふん▼有限公司Taisic Materials Corp. | 半絶縁性単結晶炭化ケイ素粉末の製造方法 |
| TWI865578B (zh) | 2020-06-18 | 2024-12-11 | 盛新材料科技股份有限公司 | 半絕緣單晶碳化矽塊材以及粉末 |
| US12297561B2 (en) | 2020-06-18 | 2025-05-13 | Taisic Materials Corp. | Semi-insulating single-crystal silicon carbide bulk material and powder |
| TWI766776B (zh) * | 2020-07-27 | 2022-06-01 | 環球晶圓股份有限公司 | 碳化矽晶碇及其製備方法 |
| CN111793821A (zh) * | 2020-08-21 | 2020-10-20 | 哈尔滨科友半导体产业装备与技术研究院有限公司 | 一种精确控制pvt法晶体生长气体压力的系统及方法 |
| CN112853491A (zh) * | 2020-12-31 | 2021-05-28 | 山西烁科晶体有限公司 | 一种掺杂碳化硅单晶及其制备方法 |
| CN113249792B (zh) * | 2021-06-22 | 2021-09-28 | 苏州优晶光电科技有限公司 | 一种调节组分平衡的碳化硅晶体生长方法及设备 |
| EP4206367A4 (en) | 2021-11-15 | 2024-01-17 | Suzhou Uking Photoelectric Technology Co., Ltd. | Synchronous growth method and device for multi-crucible silicon carbide crystal |
| CN114000198B (zh) | 2021-11-15 | 2023-03-10 | 苏州优晶光电科技有限公司 | 一种多坩埚碳化硅晶体同步生长方法及设备 |
| JPWO2023157514A1 (enExample) * | 2022-02-17 | 2023-08-24 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4325804C3 (de) | 1993-07-31 | 2001-08-09 | Daimler Chrysler Ag | Verfahren zum Herstellen von hochohmigem Siliziumkarbid |
| US5611955A (en) | 1993-10-18 | 1997-03-18 | Northrop Grumman Corp. | High resistivity silicon carbide substrates for high power microwave devices |
| US6562130B2 (en) * | 1997-01-22 | 2003-05-13 | The Fox Group, Inc. | Low defect axially grown single crystal silicon carbide |
| US6410433B1 (en) | 1999-04-27 | 2002-06-25 | Tokyo Electron Limited | Thermal CVD of TaN films from tantalum halide precursors |
| US6218680B1 (en) * | 1999-05-18 | 2001-04-17 | Cree, Inc. | Semi-insulating silicon carbide without vanadium domination |
| US6396080B2 (en) * | 1999-05-18 | 2002-05-28 | Cree, Inc | Semi-insulating silicon carbide without vanadium domination |
| US6507046B2 (en) | 2001-05-11 | 2003-01-14 | Cree, Inc. | High-resistivity silicon carbide substrate for semiconductor devices with high break down voltage |
| SE520968C2 (sv) * | 2001-10-29 | 2003-09-16 | Okmetic Oyj | Högresistiv monokristallin kiselkarbid och metod för dess framställning |
| US7063741B2 (en) * | 2002-03-27 | 2006-06-20 | General Electric Company | High pressure high temperature growth of crystalline group III metal nitrides |
| JP4987707B2 (ja) * | 2004-07-07 | 2012-07-25 | トゥー‐シックス・インコーポレイテッド | 低ドーピング半絶縁性ＳｉＣ結晶と方法 |
| US7276117B2 (en) * | 2005-02-09 | 2007-10-02 | Cree Dulles, Inc. | Method of forming semi-insulating silicon carbide single crystal |
| US7608524B2 (en) | 2005-04-19 | 2009-10-27 | Ii-Vi Incorporated | Method of and system for forming SiC crystals having spatially uniform doping impurities |
| US8361227B2 (en) * | 2006-09-26 | 2013-01-29 | Ii-Vi Incorporated | Silicon carbide single crystals with low boron content |
| US8858709B1 (en) * | 2006-04-11 | 2014-10-14 | Ii-Vi Incorporated | Silicon carbide with low nitrogen content and method for preparation |
| WO2008039914A2 (en) * | 2006-09-27 | 2008-04-03 | Ii-Vi Incorporated | Sic single crystals with reduced dislocation density grown by step-wise periodic perturbation technique |
| DE102008063129B4 (de) | 2008-12-24 | 2013-05-16 | Sicrystal Ag | Herstellungsverfahren für einen codotierten SiC-Volumeneinkristall und hochohmiges SiC-Substrat |
| JP5779171B2 (ja) * | 2009-03-26 | 2015-09-16 | トゥー‐シックス・インコーポレイテッド | ＳｉＣ単結晶の昇華成長方法及び装置 |
| WO2011034850A1 (en) * | 2009-09-15 | 2011-03-24 | Ii-Vi Incorporated | Sublimation growth of sic single crystals |
| US20130153836A1 (en) * | 2010-09-02 | 2013-06-20 | Bridgestone Corporation | Method of producing silicon carbide single crystal, silicon carbide single crystal, and silicon carbide single crystal substrate |
| CN102560671B (zh) * | 2010-12-31 | 2015-05-27 | 中国科学院物理研究所 | 半绝缘碳化硅单晶 |
| US9090989B2 (en) | 2012-05-24 | 2015-07-28 | Ii-Vi Incorporated | Vanadium compensated, SI SiC single crystals of NU and PI type and the crystal growth process thereof |
-
2013
- 2013-05-24 US US13/902,016 patent/US9090989B2/en not_active Ceased
- 2013-05-24 JP JP2015514213A patent/JP6001768B2/ja not_active Expired - Fee Related
- 2013-05-24 EP EP13794286.8A patent/EP2855741B1/en active Active
- 2013-05-24 WO PCT/US2013/042604 patent/WO2013177496A1/en not_active Ceased
- 2013-05-24 KR KR1020147033938A patent/KR101661053B1/ko not_active Expired - Fee Related
- 2013-05-24 CN CN201380027241.9A patent/CN104364428B/zh active Active
-
2017
- 2017-05-01 US US15/583,538 patent/USRE48378E1/en active Active
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